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1534 Willow Pass Road,Pittsburg,CA 94565-1701 <br /> McCam b :II Analytical Inc. Toll Free Telepbone:(877)252.9262/Fax:(925)252-9269 <br /> "When Quality Counts" http://www.mccampbell.com/E-mail:main@mcempbell.com <br /> Quality Control Report <br /> Client: Pander Environmental Services WorkOrder: 1701D08 <br /> Date Prepared: 1/31/17 BatchlD: 133427 <br /> Date Analyzed: 1/31/17-2/1/17 Extraction Method: SW5030B <br /> Instrument: GC10,GCi8 Analytical Method: SW8260B <br /> Matrix: Soil Unit: mg/kg <br /> Project: 17-16039; Pacific Ethanol Spill Sample ID: MB/LCS-133427 <br /> 1701 D36-026AMSIMSD <br /> QC Summary Report for SW8260B <br /> Analyte MB LCS RL SPK MB SS LCS LCS <br /> Result Result Val %REC %REC Limits <br /> Acetone ND - 0.10 - - <br /> tert-Amyl methyl ether(TAME) NO 0.0349 0.0050 0.050 70 53-116- <br /> Benzene NO 0.0437 0.0050 0.050 87 63-137 <br /> Bromobenzene NO - 0.0050 - - - <br /> Bromochloromethane NO 0.0050 - - <br /> Bromodichloromethane NO - 0.0050 - - - <br /> Bromoform NO 0.0050 - - - <br /> Bromomethane NO 0.0050 - - - <br /> 2-Butanone(MEK) NO - 0.020 - <br /> t-Butyl alcohol(TBA) NO 0.126 0.050 0.20 - 63 41-135 <br /> n-Butyl benzene NO - 0.0050 - - - - <br /> sec-Butyl benzene NO - 0.0050 - - <br /> tert-Butyl benzene NO - 0.0050 - - <br /> Carbon Disulfide NO - 0.0050 - _ <br /> Carbon Tetrachloride ND - 0.0050 - - - - <br /> Chlorobenzene ND 0.0464 0.0050 0.050 - 93 77-121 <br /> Chloroethane NO - 0.0050 - - - <br /> Chloroform NO - 0.0050 - <br /> Chloromethane NO - 0.0050 - <br /> 2-Chlorotoluene NO - 0.0050 - <br /> 4-Chlorotoluene NO 0.0050 - - <br /> Dibromochloromethane NO - 0.0050 - <br /> 1,2-Dibromo-3-chloropropane NO - 0.0040 - <br /> 1,2-Dibromoethane(EDB) NO 0.0404 0.0040 0.050 81 67-119 <br /> Dibromomethane NO - 0.0050 - - - <br /> 1,2-Dichlorobenzene NO - 0.0050 - - - <br /> 1,3-Dichlorobenzene NO 0.0050 - - - <br /> 1,4-Dichlorobenzene NO - 0.0050 - <br /> Dichlorodifluoromethane NO - 0.0050 - <br /> 1,1-Dichloroethane NO - 0.0050 - <br /> 1,2-Dichloroethane(1,2-DCA) NO 0.0426 0.0040 0.050 85 58-135 <br /> 1,1-Dichloroethene ND 0.0436 0.0050 0.050 - 87 42-145 <br /> cls-1,2-Dichloroethene NO - 0.0050 - - - - <br /> trans-l,2-Dichloroethene NO - 0.0050 - <br /> 1,2-Dichloropropane NO 0.0050 - - <br /> 1,3-Dichloropropane NO 0,0050 - _ <br /> 2,2-Dichloropropane NO 0.0050 - <br /> (Cont.) <br /> NELAP 4033ORELAP ` QA/QC Officer <br /> Page 40 of 69 <br />