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M c Campbell A n�l y t i�a l Inc. Toll 1534 Willow Pass Road,Pittsburg,CA 94565-1701 Free Telephone:(877)252-4262/Fax:(925)252-9269 ` "When Qualio,Counts" hup:llwww.mccampbeil.com/E-mail:mainrr=campbell.com Quality Control Report Client: Ponder Environmental Services WorkOrder: 1701D08 Date Prepared: 1/31/17 BatchlD: 133427 Date Analyzed: 1/31/17-2/1/17 Extraction Method: SW5030B Instrument: GC10,GC18 Analytical Method: SW8260B Matrix: Sol] Unit: mg/kg Project: 17-16039;Pacific Ethanoi Spill Sample ID: MB/LCS-133427 1701 D36-026AMS/MSD QC Summary Report for SW8260B Analyte MB LCS RL SPK MB SS LCS LCS Result Result Val %REC °/REG Limits 1,1-Dichloropropene ND 0.0050 cis-1,3-Dichloropropene ND 0.0050 - trans-1,3-Dichloropropene ND - 0.0050 - - Diisopropyl ether(DIPE) ND 0.0370 0.0050 0.050 74 52-129 Ethylbenzene ND - 0.0050 _ - _ Ethyl tert-butyl ether(ETBE) ND 0.0376 0.0050 0.050 75 53-125 Freon 113 ND - 0.0050 - - - Hexachlorobutadiene ND - 0.0050 - - - - Hexachloroethane ND - 0.0050 - - 2-Hexanone ND - 0.0050 - - - - lsopropylbenzene ND - 0.0050 - - - 4-Isopropyl toluene ND - 0.0050 - - - Methyl-t-butyl ether(MTBE) ND 0.0382 0.0050 0.050 - 76 58-122 Methylene chloride ND - 0.0050 - - - - 4-Methyl-2-pentanone(MIBK) ND - 0.0050 - - Naphthalene ND - 0.0050 - - - n-Propyl benzene ND - 0.0050 - - Styrene ND - 0.0050 - - 1,1,1,2-Tetrachloroethane ND - 0.0050 - - 1,1,2,2-Tetrachloroethane ND - 0.0050 - Tetrachloroethene ND - 0.0050 - - - Toluene ND 0.0465 0A050 0.050 93 76-130 1,2,3-Trichlorobenzene ND - 0,0050 - - - 1,2,4-Trichlorobenzene ND - 0.0050 - 1,1,1-Trichloroethane ND - 0.0050 - 1,1,2-Trichloroethane ND - 0.0050 - - Trichloroethene ND 0.0484 0.0050 0.050 97 72-132 Trichlorofluoromethane ND - 0.0050 - - - 1,2,3-Ttichloropropane ND 0.0050 - 1,2,4-Trimethylbenzene ND 0.0050 - - - 1,3,5-Trimethylbenzene ND 0.0050 - Vinyl Chloride ND 0.0050 - Xylenes,Total ND - 0.0050 - - (Cont) NELAP 4033ORELAP -- QA/QC Officer Page 41 of 69