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0 0 <br /> Entech Ana8y ical Labs® Inc. <br /> 3334 Victor Court e Santa Clara, CA 95054 o (408) 588-0200 a Fax (408) 588-0201 <br /> ECM Group Date: 3/18103 <br /> P.O.Box 802 Date Received: 3/13/2003 <br /> BProject Name: PG&E <br /> Benicia,CA 94510 <br /> Project Number: 03400 00 <br /> Attn: Chris Bramer P.O.Number: 03400 00 <br /> Sampled By: Casey Poldino <br /> Certified Analytical Report <br /> Order ID: 33648 Lab Sample ID: 33648-018 Client Sample ED: B15-9 <br /> Sample Time: 2:45 PM Sample Date: 3/13/2003 Matrix: Solid <br /> Parameter Result Flag DF PQL DLR Units Extraction Analysis QC Batch ID Method <br /> Dote Date <br /> Benzene NO 10 0.025 0.25 mg/kg 3/14/2003 3/14/2003 SGC42784 EPA 8020 <br /> Toluene NO 10 0.025 0.25 mg/kg 3/1412003 3/14/2003 SGC42784 EPA 6020 <br /> Ethyl Benzene NO 10 0.025 0.25 mg/kg 3/1412003 3/14/2003 SGC42784 EPA 8020 <br /> xylenes,Total NO 10 0.05 0.5 mg/kg 3/14/2003 3/14/2003 SGC42784 EPA 8020 <br /> Surrogate Surrogate Recovery Control Linins(%) <br /> 4-Bromolluorobenume 95.3 65 - 135 <br /> Parameter Result Flag DF PQL DLR Units Extraction Analysis QC Batch ID Method - <br /> Dale Date <br /> TPI'I as Diesel 220 x 20 1 20 mg/Kg 3113/2003 3/16/2003 DS4259A EPA 6015 MOD. <br /> (aaracmble) <br /> Surrogate Surrognte Recovery Control Limits I%) <br /> o-Terphenyl 77.0 50 - 126 <br /> Comment: Not a TPH as Diesel paltem;Value due to an unknmvn hydrocarbon(CIO-C34),overlapping into the Diesel quantitation range. <br /> Parameter Result Flog DF PQL DLR Units Extraction Analysis QC Batch ID Method <br /> Date Date <br /> TPH as Gasoline 130 x 10 2.5 25 mg/kg 3/14/2003 3/14/2003 SGC42784 EPA 8015 MOD. j <br /> (Purgeable) <br /> Surrogate Surrogate Recovery Control Limits I%) <br /> 4-Bromo0uerobenzcne 105.6 65 - 135 <br /> Comment: Reported TPIi as Gasoline value is the result of heavy end hydrocarbons within the TPH as Gasoline quantitation range but not <br /> typical of TPH as Gasoline. <br /> Parameter Result Flag DF PQL DLR Units Extraction Analysis QC Batch ID Method <br /> Date Date <br /> TPI/as Motor Oil ND 20 13 260 mg/I(g 3/13/2003 3/16/2003 DS4259A EPA 8015 MOD. <br /> (Extractable) <br /> Surrogate Surrogate Recovery Control Limits(%) <br /> o-Terphenyl 77.0 40 - 128 <br /> DF=Dilution Factor ND=Not Detected DLR=Detection Limit Reported PQL-Practical Quantitation Limit <br /> Analysis performed by Enicch Analytical Labs.Inc.(CA ELAP 02346) <br /> atti <br /> Sau�&64 QA/QC Manager Environmental Analysis Since 1983 <br />