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Entech Analytical Labs, Inc© <br /> 3334 Victor Court Santa Clara, CA 95054 a (408) 588-0200 a Fax (408) 588-0201 <br /> ECM Group Date: 3/18/03 <br /> P.O.Bos 802 Date Received: 3/13/2003 <br /> Project Name:PG&E <br /> Benicia,CA 945I0 Project Number: 03400 00 <br /> Attn: Chris Bramer P.O.Number: 03400 00 <br /> Sampled By: Casey Poldino <br /> Certified Analytical Report <br /> Order ID: 33648 Lab Sample D): 33648-019 Client Sample ID: B16-6 <br /> Sample Time: 3:00 PM Sample Date: 3/13/2003 Matrix: Solid <br /> Parameter Result Ping DF PQL DLR Units Extraction Analysis QC Batch ID Methad <br /> Dale Date <br /> Benzene NO 1 0.025 0.025 mg/kg 3/14/2003 3/14/2003 SGC42784 EPA 8020 <br /> Toluene ND 1 0.025 0.025 mp/kg 3/14/2003 3/14/2003 SGC42784 EPA 8020 <br /> Ethyl Benzene ........ND, 1 0.025 0.025 mg/kg 3/14/2003 3/14/2003 SGC42784 EPA 8020 i <br /> Xylenes,Total ND 1 0.05 0.05 mg/kg 3/14/2003 3/14/2003 SGC42784 EPA 8020 <br /> Surrogate Surrogate Recovery Control Limits(%) <br /> 4-Bromolluorobenzcne 96.0 65 - 135 <br /> Parautcter Result Flag DF 1'QL DLR Unils Extraction Analysis QC Batch ID Method <br /> Date Date <br /> TPM as Diesel NO I 1 I mgtKg 3/13/2003 3/142003 DS4259A EPA 8015 MOD. <br /> (Extractable) <br /> Surrogate Surrogate Recovery Control Limits(%) <br /> o-Tcrphenyl 72.0 50 - 126 ', <br /> Parameter Result Flag DF PQL DLR Units Extraction Analysis QC Batch ID Metimd <br /> Date Date <br /> TPM as Gasoline ND 1 2.5 2.5 mg/kg 3/14/2003 3/1412003 SGC42784 EPA 8015 MOD. <br /> (Purgeable) <br /> Surrogate Surrogate Recovery Control Limits(%) <br /> 4-BromoOuombenzene 90.3 65 - 135 <br /> Parameter Result Fing DF PQL DLR Units Extraction Analysis QC Balch ID Malhod <br /> Date Dale <br /> TPhI as Motor Oil ND 1 13 13 mg/Kg 3/13/2003 3114/2003 DS4259A EPA 8015 MOD. <br /> (Extractable) <br /> Surrogate Surrogate Recovery Control Limits(%) <br /> o-Terphcnyl 72.0 40 - 128 <br /> it <br /> DF=Dilution Factor ND m Not])elected DLR=Detection Limit Reported PQL-Practical Quantimtion Limit <br /> Analysis perrar ed by Entech Analytical Labs,Inc.(CA ELAP 112346) <br /> atti an rock,QA/QC Manager Environmental Analysis Since 1983 <br />