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0 0 <br /> Entech Ana yytic 0 Labs, Deco <br /> 3334 Victor Court e Santa Clara, CA 95054 a (408) 588-0200 o Fax (408) 588-0201 <br /> ECM Group Date: 3/18/03 <br /> P.O.Bos 802 Date Received: 3113/2003 <br /> BProject Name: PG&E <br /> Benicia,CA 94510 <br /> Project Number: 0340000 <br /> Attn: Chris Bramer P.O.Number: 0340000 <br /> Sampled By: Casey Poldino <br /> Certified Analytical Report <br /> Order ID: 33648 Lab Sample ID: 33648-023 Client Sample ED: BI <br /> Sample Time: 9:00 AM Sample Date: 3/13/2003 Matrix: Liquid <br /> Parameter Result Flag DF PQL DLR Units Extraction Analysis QC Butch ID Method <br /> Date Date <br /> Benzene ND 1 0.5 0.5 pp/L N/A 3/14/2003 WGC62783 EPA 8020 <br /> Toluene NO I 0.5 0.5 pg/L N/A 3/14/2003 WGC62783 EPA 8020 <br /> Ethyl Benzene ND 1 0.5 0.5 pF/L N/A 3/1412003 WGC62783 EPA 8020 <br /> Xylenes,Total NO I I 1 pg/l, N/A 3/142003 WGC62783 EPA 8020 <br /> Surrogate Surrogate Recovery Control Limits I%) <br /> 4-Bramolluorobenzene 88.2 65 - 135 <br /> Parameter Result Flag DF PQL DLR Units Extraction Analysis QC Balch ID Method <br /> Dale Date <br /> TPFI as Diesel NO 1 60 60 ag/L 3/14/2003 3/152003 DW4324A EPA 8015 MOD. <br /> (Extractable) <br /> Surrogate Surrogate Recovery Control Limits(%) <br /> o-Tcrphcnyl 95.0 21 - 142 <br /> Comment: Reporting limit increased due to limited sample volume. <br /> Parameter `i Result Flag DF PQL DLR Units Extraction Analysis QC Bateb ID Method <br /> Date Date <br /> Tpn as Gasoline NO I 50 50 pg/L N/A 3/14/2003 WGC62783 CPA 8015 MOD. <br /> (Purgeable) <br /> Surrogate Surrogate Recovery Control Limits I%) <br /> 4-8mmoRuorobenune 79.7 65 - 135 <br /> Parameter Result Flag DF PQL DLR Units Extraction Analysis QC Balch ID Method <br /> Date Date <br /> TPFI as Motor Oil ND 1 298 298 pp/L 3/14/2003 3/1512003 DW4324A EPA 8015 MOD. <br /> (Extractable) <br /> Surrogate Surrogate Recovery Control Limits(%) <br /> a-Terphenyl 95.0 32 - 145 <br /> Comment: Reporting limit increased due to limited sample volume. <br /> OF=Dilution Factor ND=Not Detected DLR=Detection Limit Reported PQL-Practical Quantitation Limit <br /> Analysis perromred by Entech Analytical labs,Inc.(CA CLAP 12346) <br /> Panum rw QA/QC Manager Environmental Analysis Since 1983 <br />