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Entech Analyfocal Labs, Mico <br /> 3334 Victor Court m Santa Clara, CA 95054 0 (408) 588-0200 o Fax (408) 588-0201 <br /> ECM Group Date: 3/18/03 <br /> P.O.Box 802 Date Received: 3/13/2003 <br /> BProject Name:PG&E <br /> Benicia,CA 94510 <br /> ProjectNumber. 03400 00 <br /> Attn: Chris Bramer P.O.Number: 03400 00 <br /> Sampled By: Casey Poldino <br /> Certified Analytical Report <br /> Order ID: 33648 Lab Sample ID: 33648-020 Client Sample ID: B17-6 <br /> Sample Time: 3:05 PM Sample Date: 3/13/2003 Matrix: Solid <br /> Parameter Result Flag DF PQL DLR Units Extraction Analysis QC Batch ID Method <br /> Date Date <br /> Benzene ND 1 0.025 0.025 mglkg 3/14/2003 3/142003 SGC42784 EPA 8020 <br /> Toluene ND 1 0.025 0.025 mg1kg 3/14/2003 3/14/2003 SGC42784 EPA 8020 <br /> Ethyl Benzene ND 1 0.025 0.025 mg/kg 3/14/2003 3/1412003 SGC42784 EPA 8020 <br /> Xylenes,Total ND 1 0.05 0.05 mg/kg 3/14/2003 3/14/2003 SGC42784 EPA 10020 <br /> Surrogate Surrogate Recovery Control Limits I%) <br /> 4-Bromolluombcnzene 96.3 65 - 135 <br /> Parameter Result Flag DF PQL DLR Units Extraction Analysis QC Batch ID Method <br /> Date Date <br /> TPI I as Diesel 450 x 100 1 100 mg/Kg 3/13/2003 3/17/2003 DS4259A EPA 8015 MOD. <br /> (Extractable) <br /> Surrogate Surrogate Recovery Control Limits(%) <br /> o-Terphenyl 91.0 50 - 126 <br /> Comment: Not a TPII as Diesel pattern:Value due to overlap Dam the Motor Oil mnge into the Diesel quantitation range. <br /> Parameter Result Flag DF 1'QL DLR Units Extraction Analysis QC Batch ID Method <br /> Data Date <br /> TPII as Gasoline NO 1 2.5 2.5 mg/kg 3/14/2003 3/14/2003 SGC42784 EPA 8015 MOD. <br /> (Purgcable) <br /> 8urrugme Surrogate Recovery Control Limits I%) <br /> 4-Bromofluorobenzene 91.1 65 - 135 <br /> Pnrmnuter Result Flag OF PQL DLR Units Extraction Analysis QC Batch ID Method <br /> Date Date <br /> TPII as Motor Oil 2200 100 13 1300 mg/Kg 3/13/2003 3/17/2003 DS4259A EPA 8015 MOD. <br /> (Extractable) <br /> Surrogate Surrogate Recovery Control Limits(h) <br /> o-Terphenyl 91.0 40 - 128 <br /> OF=Dilution rector ND Not Detected DLR=Detection Limit Reported PQL=Practical Quantitation Limit <br /> Analysis performed by Entech Analytical Lobs,Inc.(CA ELAP#2346) <br /> Patti Sandrock,QA/QCManager Environmental Analysis Since 7983 <br />