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0 0 <br /> Entech Analytical Labs, Inca <br /> 3334 Victor Court e Santa Clara, CA 95054 c (408) 588-0200 a Fax (408) 588-0201 <br /> ECM Group Date: 3/18/03 <br /> P.O.Box 802 Date Received: 3/13/2003 <br /> Benicia,CA 94510 Project Name: PG&E <br /> Project Number: 03400 00 <br /> Attn: Chris Bramer P.O.Number: 03400 00 <br /> Sampled By: Casey Poldino <br /> Certified Analytical Report <br /> Order ID: 33648 Lab Sample ID: 33648-028 Client Sample ID: B6 <br /> Sample Time: 11:30 AM Sample Date: 3113/2003 Matrix: Liquid <br /> Permitter Result Flag DF PQL DLR Units Extraction Analysis QC Batch ID Method <br /> Date Date <br /> Benzene ND 1 0.5 0.5 µg/L N/A 3/14/2003 WGC62783 EPA 8020 <br /> Toluene ND 1 0.5 0.5 pg/L N/A 3/14/2003 WGC62783 EPA 8020 <br /> Ethyl Benzene NO 1 0.5 0.5 µg/L N/A 3/14/2003 WGC62783 EPA 8020 <br /> Xylenes,Total NO I I 1 pg/L N/A 3/14/2003 WGC62783 EPA 8020 <br /> Surrogate Surrogate Recovery Control Limits(%) <br /> 4-BromoOuarobenzene 89.3 65 - 135 <br /> Parameter Result Fing DF PQL DLR Units Extraction Analysis QC Batch ID Method <br /> Data Date <br /> 'rPtl as Diesel ND I 81 BI µ8/L 3/14/2003 3/15/2003 DW4324A EPA 8015 MOD. <br /> (Extractable) <br /> Surrogate Surrogate Recovery Control Limits(%) <br /> o-Terphcnyl 94.0 21 - 142 <br /> Cammenl: Reporting limit increased due to limited sample volume. <br /> Parameter Result Flag DF PQL DLR Units Extraction Analysis QC Batch ID Method <br /> Date Date <br /> TPH as Gasoline NO I 50 50 pg/L N/A 3/14/2003 WGC62783 EPA 8015 MOD. <br /> (Purgeable) <br /> Surrogate Surrogate Recovery Control Limits(%) <br /> 4-Brom0nuorobcnzenc 80.7 65 - 135 <br /> Parameter Result Flag DF PQL DLR Units Extraction Analysis QC Botch ID Method <br /> Date Date <br /> TPH as Motor Oil ND 1 403 403 pgtL 3/14/2003 3/15/2003 DW4324A EPA 8015 MOD. <br /> (Extractable) <br /> Surrogate Surrogate Recovery Control Limits(%) <br /> o-Terphenyl 94.0 32 - 145 <br /> Comment: Reporting limit increased due to limited sample volume. <br /> OF=Dilution Factor ND=Not Detected DLR-Detection Limit Reported PQL=Practical Quantitation Limit <br /> Analysis perrorrned by Entech Analytical Lobs,Inc.(CA ELAP#2346) <br /> atti Sandrock,QA/QC Manager Environmental Analysis Since 1983 <br />