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0 0 <br /> Enttech Analytical Labs, Dnco <br /> 3334 Victor Court o Santa Clara, CA 95054 m (408) 588-0200 n Fax (408) 588-0201 <br /> ECM Group Date: 3/18/03 <br /> P.O.Bos 802 Date Received: 3/13/2003 <br /> Project Name: PG&E <br /> Benicia,CA 94510 Project Number: 0340000 <br /> Attn: Chris Bramer P.O.Number: 03400 00 <br /> Sampled By: Casey Poldino <br /> Certified Analytical Report <br /> Order ID: 33648 Lab Sample ID: 33648-029 Client Sample ED: B7 <br /> Sample Time: 12:00 PM Sample Date: 3/13/2003 Matrix: Liquid <br /> Parameter Result Flab DF PQL DLR Units Extraction Analysis QC Batch ID Method <br /> Date Date <br /> Benzene ND 1 0.5 0.5 pg/L N/A 3/14/2003 WGC62783 EPA 8020 <br /> Toluene ND 1 0.5 0.5 pg/L N/A 3/14/2003 WGC62783 EPA 8020 <br /> Ethyl Benzene NO 1 0.5 0.5 pg/L N/A 3/14/2003 WGC62783 EPA 8020 <br /> Xylenes,Total NO I I 1 pg/L N/A 3/14/2003 WGC62783 EPA 8020 <br /> Surrogate Surrogate Recovery Control Limits I%) <br /> 4-Bromalluorobenzene 97.3 65 - 135 <br /> Parameter Result Flag DF PQL DLR Units Extraction Analysis QC Batch ID Method <br /> Date Date <br /> TPI-1 as Diesel ND 1 56 56 pg/L 3/14/2003 3/15/2003 DW4324A EPA 8015 MOD. <br /> (Extractable) <br /> Surrogate Surrogate Recovery Control Limits(%) <br /> c-Terphenyl 92.0 21 - 142 <br /> Comment: Reporting limit increased due to limited sample volume. <br /> Parameter Result Flag DF PQL DLR Units Extraction Analysis QC Batch ID Method <br /> Dale Date <br /> TPM as Gasoline ND 1 50 50 pg/L N/A 3/14/2003 WGC62783 EPA 8015 MOD. <br /> (Purgeable) <br /> Surrogate Surrogate Recovery Control Limits I%) <br /> 4-Bromatluorobenzene 83.0 65 - 135 <br /> Parameter Result Flag DF PQL DLR Units Extraction Analysis QC Batch ID Method <br /> Date Date <br /> 7"PH as Motor Oil ND 1 281 281 pg/L 3/14/2003 3/15/2003 DNV4324A EPA 8015 MOD. <br /> (Extractable) <br /> Surrogate Surrogate Recovery Control Limits(%) <br /> o-Terphenyl 92.0 32 - 145 <br /> Comment: Reporting limit increased due to limited sample volume. <br /> OF-Dilution Factor NO=Not Detected DLR=Detection Limit Reported PQL=Pmcdcul Quantitation Limit <br /> Analysis performed by Emech Analytical Labs,Inc.(CA FLAP 112346) <br /> 1 atti Sandrock,QA/QCManager Environmental Analysis Since 1983 <br />