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Castle Analytical Laboratory, Atwater, CA <br /> Lab Report No.: H3121802 Date: 12/29/2003 Page: 3 <br /> Project Name: OLIVAREZ PROPERTY Analysis: Volatile Organic Compounds by GC/MS Fuel <br /> Project No: NA Method: 8260FA <br /> Prep Meth: SW5030B <br /> Field ID: MW-2 Lab Samp ID: 6447-2W <br /> Descr/Location: MW-2 Rec'd Date: 12/18/2003 <br /> Sample Date: 12/17/2003 Prep Date: 12/22/2003 <br /> Sample Time: 1511 Analysis Date: 12/22/2003 <br /> Matrix: Water QC Batch: VWMS-D223 <br /> Basis: Not Filtered Notes: DF <br /> Analyte Det Limit Rep Limit Note Result Units Pvc Dil <br /> Methyl-tert-butyl ether(MTBE) 2-89 5. MRL 160L UG/L 10 <br /> Ethyl tert-butyl ether(ETBE) 0.840 5. MRL ND UG/L 10 <br /> tert-Amyl methyl ether(TAME) 0.670 5. MRL ND UG/L 10 <br /> Di-isopropyl ether(DIPE) 1.55 5. MRL ND UG/L 10 <br /> tert-Butyl alcohol (TBA) 87.9 200. MRL NO UG/L 10 <br /> 1,2-Dichloroethane 0.810 5. MRL 16Q UG/L 10 <br /> 1,2-Dibromoethane 0.920 S. MRL 22 UG/L 10 <br /> SURROGATE AND INTERNAL STANDARD RECOVERIES: <br /> Toluene-d8 76-129 SLSA 88.8% 1 <br /> 1,2-Dichloroethane-d4 53-141 SLSA 96.0% 1 <br /> DF: Reporting limits elevated due to matrix interferences <br /> • <br /> Approved by: IAk�, Date: <br />