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Castle Analytical Laboratory, Atwater, CA <br /> Lab Report No.: H3121802 Date: 12/29/2003 Page: 4 <br /> Project Name: OLIVAREZ PROPERTY Analysis: Volatile Organic Compounds by GC/MS Fuel <br /> Project No: NA Method: 8260FA <br /> Prep Meth: SW50303 <br /> Field ID: MW-3 Lab Samp ID: 8447-3W <br /> Descr/Location: MW-3 Rec'd Date: 12/18/2003 <br /> Sample Date: 12/17/2003 Prep Date: 12/22/2003 <br /> Sample Time: 0945 Analysis Date: 12/22/2003 <br /> Matrix: Water QC Batch: VWMS-D223 <br /> Basis: Not Filtered Notes: <br /> Analyte Det Limit Rep Limit Note Result Units Pvc Dil <br /> Methyl-tert-butyl ether(MTBE) 0.289 0.5 MRL ND UG/L 1 <br /> Ethyl telt-butyl ether(ETRE) 0.084 0.5 MRL ND UG/L 1 <br /> tert-Amyl methyl ether(TAME) 0.067 0.5 MRL ND UG/L 1 <br /> Di-isopropyl ether(DIPS) 0.155 0.5 MRL ND UG/L 1 <br /> tert-Butyl alcohol (TBA) 8.79 20. MRL ND UG/L 1 <br /> 1,2-Dichloroethane 0.081 0.5 MRL 3.7 UG/L 1 <br /> 1,2-Dibromoethane 0.092 0.5 MRL ND UG/L 1 <br /> SURROGATE AND INTERNAL STANDARD RECOVERIES: <br /> Toluene-d8 76-129 SLSA 111% 1 <br /> 1,2-Dichloroethane-d4 53.141 SLSA 93.8% 1 <br /> i <br /> Approved by: Date: -zl/o <br /> t <br />