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110 Second Avenue South,#D7,Pacheco,CA 94553-5560 <br /> MCCAMPBELL ANALYTICAL INC. Telephone:925-798-1620 Fax:925-798-1622 <br /> hUp:LMM.mccamobell.com E-mail:main@mccampbell.com <br /> Date Sampled: 09/22/98 <br /> Advanced GeoEnvironmental Client Project ID:Emil's Liquors <br /> Date Received: 09/23/98 <br /> 4005 North Wilson Way <br /> Stockton,CA 95205 Client Contact:Gary Dickenson Date Extracted: 09/23/98 <br /> Client P.O: Date Analyzed: 09/24/98 <br /> Lead* <br /> EPA analytical methods 6010/200.7,239.2* <br /> Lab ID Client ID Matrix Extraction° Lead* %Recovery <br /> Surrogate <br /> 95668 $-1-9.5' S TTLC ND 101 <br /> S TTLC 3.0 mg/kg <br /> Reporting Limit unless otherwise <br /> stated;ND means not detected above W TTLC 0.005 mg/L <br /> the reporting limit <br /> --- STLC,TCLP 0.2 mg/L <br /> *soil and sludge samples are reported in mg/kg,wipe samples in ug/wipe,and water samples and all STLC 1 SPLA/TCLP extracts in mg/L <br /> "Lead is analysed using EPA method 6010 (ICP)for soils, sludges, STLC & TCLP extracts and method 239.2 (AA Furnace) for water <br /> samples <br /> °EPA extraction methods 1311(TCLP),3010/3020(water,TTLC),3040(organic matrices,TTLC),3050(soiids,TTLC);STLC-CA Title 22 <br /> °surrogate diluted out of range;NIA means surrogate not applicable to this analysis <br /> °c reporting limit raised due matrix interference <br /> i) liquid sample that contains greater than 2 vol. % sediment; this sediment is extracted with the liquid, in accordance with EPA <br /> methodologies and can significantly effect reported meta!concentrations. <br /> DHS Certification No. 1644 f/ Edward Hamilton,Lab Director <br />