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110 Second Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC. Telephone:925-798-1620 Fax:925-798-1622 <br /> httn://www.mccam2hell.com E-mail:main@mccampbell.com <br /> Date Sampled: 09/22/98 <br /> Advanced GeoEnvironmental CIient Project ID:Emil's Liquors <br /> Date Received: 09/23/98 <br /> 4005 North Wilson Way <br /> Stockton,CA 95205 Client Contact:Gary Dickenson Date Extracted: 09/25/98 <br /> Client P.O: Date Analyzed: 09/26/98 <br /> Oxygenated Volatile Organics By GC/MS <br /> EPA method 8260 modified <br /> Lab ID 95668 <br /> Reporting Limit <br /> Client ID B-1-9.5' <br /> Matrix S S w <br /> Compound Concentration* ug/kg ug/L <br /> Di-isopropyl Ether(DIPS) ND 5.0 1.0 <br /> Ethyl tert-Butyl Ether(ETRE) ND 5.0 1.0 <br /> Methyl-tert Butyl Ether(MTBE) ND 5.0 1.0 <br /> • tert-Amyl Methyl Ether(TAME) ND 5.0 1.0 <br /> tert-Butanol ND 25 5.0 <br /> Surrogate Recoveries(%) <br /> Dibromofluoromethane 97 <br /> Comments: <br /> *water samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/STLC/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit;N/A means surrogate not applicable to this analysis <br /> (h)lighter than water immiscible sheen is present;(i)liquid sample that contains greater than—5 vol.%sediment;0)sample diluted due to <br /> high organic content <br /> DHS Certification No. 1644 // Edward Hamilton,Lab Director <br />