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110 2nd Avenue South,#137,Pacheco,CA 94553-5560 <br /> McCampbell Analytical, Inc. Telephone 925-798 1620 Fax 925-798-1622 <br /> Website www mccampbell corn E mail masn®mccanipbell com <br /> • Advanced GeoEnvironmental,Inc Client Project ID Flag City Chevron Date Sampled 01120/04-01/22/04 <br /> 837 Shaw Road Date Received 01/23/04 <br /> Client Contact Tim Cuellar Date Extracted 01/23/04-01/26/04 <br /> Stockton,CA 95215 <br /> Client P O Date Analyzed 01/23/04-01/26/04 <br /> Oxygenated Volatile Organics+EDB and 1,2-DCA by P&T and GC/MS* <br /> Extraction Method SW5030B Analyucal Method SW 8260B Work Order 0401260 <br /> Lab ID 0401260-OOIC 0401260-002C 0401260-003C 0401260-004C <br /> Client ID P41-15to20 P41-37to41 P42-11to]6 P42-40to44 Reporting Limit for <br /> Matrix W W W W DF-1 <br /> i <br /> Compound Concentration pp,/Kg lip/L <br /> tent-Amyl methyl ether(TAME) ND ND<25 ND ND<2 5 50 05 <br /> t-Butyl alcohol(TBA) ND ND<250 ND ND<25 25 50 <br /> 1,2-Dibromoethane(EDB) ND ND<25 ND ND<2 5 50 05 <br /> 1,2-Dichloroethane(1 2-DCA) ND ND<25 ND ND<2 5 50 05 <br /> • Dusopropyl ether(DIPF) ND ND<25 I ND ND<2 5 50 05 <br /> Ethyl tent-butyl ether(ETRE) ND ND<25 ND ND<2 5 50 05 <br /> Methyl-t-butyl ether(MTBE) 079 1900 ND 240 50 0 5 <br /> Surrogate Recoveries(%) <br /> %SS 100 942 994 982 <br /> Comments i i i i <br /> *water and vapor samples and all TCLP&SPLP extracts are reported in lig/L sail/sludge/solid samples in Ag/kg, wipe samples in Pg/wipe, <br /> product/oil/non-aqueous liquid samples in mglL <br /> ND means not detected above the reporting limit,NIA means analyte not applicable to this analysis <br /> #surrogate diluted out of range or surrogate coelutes with another peak <br /> h)lighter than water immiscible sheentproduct is present,i)liquid sample that contains greater than—2 vol %sediment,j)sample diluted due to high <br /> organic content <br /> DHS Certification No 1644 LAW ' _Angela Rydelius,Lab Manager <br />