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ry' 110 2nd Avenue South,#D7 Pacheco,CA 94553-5560 <br /> Inc.McCampbell Analytical, Telephone 925-798-1620 Fax 925-798-1622 <br /> Website www mccampbell corn E-mail roam@mccampbeU corn <br /> Advanced GeoEnvironmental,Inc Client Project ID Flag City Chevron Date Sampled 01/20/04-01/22/04 <br /> 837 Shaw Road Date Received 01/23/04 <br /> Client Contact Tim Cuellar Date Extracted 01/23/04-01/26/04 <br /> Stockton,CA 95215 <br /> Client P O 1 Date Analyzed 01/23/04-01/26/04 <br /> Oxygenated Volatile Organics+EDB and 1,2-DCA by P&T and GC/MS* <br /> Extraction Method SW5030B Analytical Method SW8260B Work Order 0401260 <br /> Lab ID 0401260-005C 0401260-006C 10401260-007C I 0401260-008C <br /> i <br /> Client ID P40A-14tol9 P40A-47to51 P39-15to20 I P39-36to41 <br /> Reporting Limit for <br /> Matrix W W I W I W DF=1 <br /> I <br /> Compound Concentration Ng/Kg µg/L <br /> tent-Amyl methyl ether(TAME) ND<2 5 ND ND ND<25 5 0 05 <br /> t-Butyl alcohol(TBA) ND<25 NO ND ND<250 25 50 <br /> 1,2-Dibromoethane(EDB) ND<2 5 ND ND ND<25 50 05 <br /> 1,2-Dichloroethane(1,2-DCA) ND<2 5 ND ND ND<25 50 05 <br /> Dusopropyl ether(RIPE) ND<2 5 ND ND ND<25 50 05 <br /> Ethyl tert-butyl ether(ETRE.) ND<2 5 ND ND ND<25 50 05 <br /> Methyl-t-butyl ether(MTBE) 120 15 ND 570 50 05 <br /> Surrogate Recoveries <br /> %SS 976 999 977 930 <br /> Comments <br /> *water and vapor samples and all TCLP&SPLP extracts are reported in gg/L,soil/sludge/solid samples to jig/kg, wipe samples inµg/wipe, <br /> product/oil/non-aqueous liquid samples in mg/L <br /> ND means not detected above the reporting limit,N/A means analyte not applicable to this analysts <br /> #surrogate diluted out of range or surrogate coelutes with another peak <br /> h)lighter than water immiscible sheen/product is present,i)liquid sample that contains greater than—2 vol %sediment,j)sample diluted due to high <br /> organic content <br /> DHS Certification No 1644 Angela Rydelius,Lab Manager <br /> �f <br />