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h 110 2nd Avenue South,#D7 Pacheco CA 94553-5560 <br /> McCampbell Analytical, Inc. Telephone 925-798-1620 Fax 925-798-1622 <br /> Website www mccampliell com E-mail mam a tnccampbell cam <br /> Advanced GeoEnvironmental, Inc Client Project ID Flag City Chevron Date Sampled 01120/04-01/22/04 <br /> 837 Shaw Road Date Received 01/23/04 <br /> Client Contact Tian Cuellar Date Extracted 01/23/04-01/26/04 <br /> Stockton,CA 95215 <br /> Client P O Date Analyzed 01/23/04-01126104 <br /> Oxygenated Volatile Organics+EDB and 1,2-DCA by P&T and GC/MS* <br /> Extraction Method SW5030B Analytical Method SW8260B Work Order 0401260 <br /> Lab ID 0401260-009C 0401260-0 I OC 0401260-011 C 0401260-012C <br /> I ' <br /> Client ID P39-47to51 P43-13tol8 P43-37to41 P43-47to51 Reporting Limit for <br /> Matnx W W W W DF=1 <br /> DF 1 25 10 1 S W <br /> Compound Concentration Vg/Kg µg/L <br /> tert-Amyl methyl ether(TAME) ND ND<12 ND<5 0 ND 50 05 <br /> t-Butyl alcohol(TBA) ND ND<120 ND<50 13 25 50 <br /> 1,2-Dibromoethane(EDB) ND ND<12 ND<5 0 ND 50 05 <br /> 1,2-131ehlorocthane(1,2-DCA) ND ND<12 ND<5 0 I ND 50 05 <br /> . Dnsopropyl ether(DIPS) ND ND<12 ND<5 0 ND 5 0 05 <br /> Ethyl tert-butyl ether(ETRE) ND ND<12 ND<5 0 ND 5 0 05 <br /> Methyl-t-butyl ether(MTBE) 065 540 210 32 5 0 0 5 <br /> Surrogate Recoveries(%) <br /> %SS 104 93 9 960 102 <br /> LComments t t t t <br /> "water and vapor samples and all TCLP&SPLP extracts are reported in ug/L soil/sludge/solid samples inµg/kg wipe samples in Rg/wipe <br /> productloil/non-aqueous liquid samples in mg/L <br /> ND means not detected above the reporting limit NIA means analyte not applicable to this analysts <br /> #surrogate diluted out of range or surrogate coelutes with another peak <br /> I)lighter than water immiscible sheen/product is present,i)liquid sample that contains greater than--2 vol %sediment,j)sample diluted due to high <br /> r antc content <br /> DHS Certification No 1644 C' j0 ngela Rydelius, Lab Manager <br />