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110 2nd Avenue South #D7 Pacheco CA 94553-5560 <br /> McCampbell Analytical, Inc. Telephone 925-798-1620 Fax 925-798-1622 <br /> Website www mccampbell cam F-mad main®mccarupbell com <br /> Advanced GeoEnvironmental,Inc Client Project ID Flag City Chevron Date Sampled 01/20/04-01/22104 <br /> 837 Shaw Road Date Received 01/23/04 <br /> Client Contact Tim Cuellar Date Extracted 01/23/04-01/26/04 <br /> Stockton,CA 95215 <br /> Client P O Date Analyzed 01/23/04-01/26104 <br /> Oxygenated Volatile Organics+EDB and 1,2-DCA by P&T and GCIMS* <br /> Extraction Method SW5030B Analytical Method SW8260B Work Order 0401250 <br /> Lab D-) 0401260-021A 0401260-022A 0401260-023A 0401260-024A <br /> r <br /> Client ID P42-15' P42 25' P42-50' P43-15' <br /> Reporting Limit for <br /> Matnx S S J S S DF=1 <br /> 3 <br /> Compound Concentration gg/Kg ug/L <br /> tert-Amyl mcthyl ether(TAME) ND ND ND ND 50 05 <br /> t-Butyl alcohol(TBA) ND ND ND ND 25 50 <br /> 1,2-Dibromoethane(EDB) ND ND ND ND 5 0 05 <br /> 1,2-Dichloroethane(I 2-13CA) ND ND ND ND 50 05 <br /> Diisopropyl ether(DIPS) ND ND ND ND 50 05 <br /> Ethyl tent-butyl ether(ETBE) ND ND ND ND 50 05 <br /> Methyl-t-butyl ether(MTBE) ND ND ND ND 50 05 <br /> Surrogate Recoveries(%} <br /> %SS 935 92 1 937 929 <br /> Comments <br /> "water and vapor samples and all TCLP&SPLP extracts are reported inµg/L,soil/sludgelsolid samples in}ug/kg, wipe samples in lig wipe, <br /> product/oil/non-aqueous liquid samples in mWL <br /> ND means not detected above the reporting limit,N/A means analyte not applicable to this analysts <br /> #surrogate diluted out of range or surrogate coelutes with another peak <br /> h)lighter than water immiscible sheen/product is present,i)liquid sample that contains greater than—2 vol %sediment,,])sample diluted due to high <br /> organic content <br /> DHS Certification No 1644 Angela Rydelius, Lab Manager <br />