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110 2nd Avenue South,#177 PaCheco,CA 94553-5560 <br /> McCampbell Analytical, Inc. Telephone 925-798-1620 Fax 925-796-1622 <br /> - — - - -- - Website www mccampbell com F-mail main®mccainpbell corn- <br /> Advanced <br /> om Advanced GeoEnvironniental,Inc Client Project ID Flag City Chevron Date Sampled 01/20/04-01/22/04 <br /> 837 Shaw Road Date Received 01/23/04 <br /> Client Contact Tim Cuellar Date Extracted 01/23/04 <br /> Stockton,CA 95215 <br /> [Chen�tP O Date Analyzed 01124/04-01128104 <br /> Semi-Volatile Organics by GC/MS(Basic Target List)* <br /> Extraction Method SW351oC Analytical Method SW8270D Work Order 0401260 <br /> Lab ID 0401260-002D <br /> Client ID - P41-37to41 <br /> Matrix Water <br /> Compound Concentration* DF0,��8 Compound Concentration* DFncng <br /> Acenaphthene ND 1 0 10 Acena hth lene ND 1 0 10 <br /> Anthracene ND I 10 10 Henzidine ND 10 50 <br /> Benzoic Acrd ND 1 0 50 Benzo a anthracene ND 1 0 10 <br /> Benzo(b)fluoranthene ND 10 10 Benzo(k)fluoranthene ND 10 10 <br /> Benzo(g,h,i)perylcne ND 1 0 10 Benzo(a)pyrene ND 10 10 <br /> Benzyl Alcohol ND 1 0 20 Bis 2�hloroethox Methane ND 10 10 <br /> Bis(2-ehloroeth I)Ether ND 1 0 10 Bis 2-chloroiso ro 1 Ether ND 1 0 to <br /> Bis(2-eth lhex l)Phthalate ND 1 0 1 10 4-Bromo hen 1 Phenyl Ether ND 10 10 <br /> But lben 1 Phthalate ND 1 0 10 4-Chloroantline ND 10 20 <br /> 4-Chloro-3-methyl henol ND 1 0 10 1 2-Chiorona hthalene ND 1 0 10 <br /> 2-Chlorophenol ND 1 0 10 4-Chlorophenyl Phenyl Ether ND 1 0 10 <br /> Ch Bene ND 1 0 10 Dibenzo(a,h)anthraccne ND 1 0 10 <br /> Dibenzofuran ND 1 0 10 Dt-n-butyl Phthalate ND 1 0 10 <br /> 1,2-Dichlorobenzene ND 10 10 13-Dichlorobenzene ND 10 10 <br /> 14-Dichlorobenzene ND 10 10 3,3-Dichlorobenzidme ND 10 20 <br /> 2,4-Dichloro henol ND 1 0 10 Diethyl Phthalate ND 1 0 10 <br /> • 2,4-Dimeth l henol ND 1 0 10 Dimethyl Phthalate ND 1 0 10 <br /> 4,6-Dmitro-2-methyl henol ND l 0 50 2,4-Dinitro henol ND 1 0 50 <br /> 2,4-Dmitrotoluene ND t4fo ! <br /> 10 2,6-Dimtrotoluene ND 10 l0 <br /> Di-n-oct l Phthalate ND 1 2-Di hen 1h drazine ND 1 0 10 <br /> Fluoranthene ND Fluorene ND 10 10 <br /> Hexachlorebenzene ND l0 HexachJorobutadiene ND 10 10 <br /> Hexachlorocyctopentadiene ND 1 0 50 Hexachloroethane ND 1 0 10 <br /> Indeno 1,2,3-cdpyrene ND 1 0 10 1 Iso horone ND 1 0 t0 <br /> 2-Meth Ina hthalene ND 1 0 10 2-Methylphenol(o-Cresol) - ND 1 0 10 - <br /> 3&/or 4-Meth ] henol m, -Cresol ND 1 0 10 Naphthalene ND [ 0 10 <br /> 2-Nitroanilme ND 10 50 3-Nitroamhne ND 10 50 <br /> 4-Nitroaniiine ND 10 50 Nitrobenzene ND 10 50 <br /> 2-Nitro henol ND 1 0 50 4-Nitrophenol ND 1 0 10 <br /> N-Nitrosodt hen lamine ND 10 10 N-Nitrosodi-n- ro lamme ND 1 0 10 <br /> Pentachlorophenol ND 1 0 50 Phenanthrene ND 1 0 10 <br /> Phenol ND 10 10 Pyrene ND 10 10 <br /> 1,2,4-Trichlorobenzene ND 1 0 10 2,4 5-Trrchloro hent ND l 0 10 <br /> 2 4 6-Trichlorohenol ND 1 0 1 10 <br /> Surrogate Recovenes(%) <br /> %SS 1 94 9 %SS2 90 1 <br /> %SS3 86 1 %SS4 82 0 <br /> %SS5 777 %SS6 813 <br /> Comments i <br /> *water samples and all TCLP&SPLP extracts are reported in gg/L,soil/sludge/solid samples in mg/kg,wipe samples inµg/wipe,product/oil/non- <br /> aqueous liquid samples in mg/L <br /> ND means not detected above the reporting limit,NIA means analyte not applicable to this analysts <br /> #)surrogate diluted out of range,&)low or no surrogate due to matnx interference <br /> h)lighter than water immiscible sheen/product is present,i)liquid sample that contains greater than--2 vol %sediment,l)sample diluted due to high <br /> organic content,k)reporting limit raised,benzoic acid found in LCS/LCSD samples Benzoic acid found in the method blank at a detectable <br /> concentration but under the RL for this compound <br /> DHS Certification No 1644 V gela Rydelius, Lab Manager <br />