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110 2nd Avenue South,#D7 Pacheco,CA 94553-5560 ell McCain bAnal�7tical? Inc. Telephone 925-798-1620 Fax 925-798 1622 -=i „t - P= -- = J=_ - ---- —- - - Website www mecampbell corn E-mail main©mecampbell com - - - ---- Advanced GeoEnvirotimental, Inc Client Project ID Flag City Chevron Date Sampled 01120104-01122104 837 Shaw Road Date Received 01/23104 Client Contact Tun Cuellar Date Extracted 01/23/04 Stockton,CA 95215 Client P O Date Analyzed 01124/04-01/28104 Semi-Volatile Organics by GUMS(Basic Target List)* Extraction Method SW3510C Analytical Method SW8270D Work Order 0401260 Lab 1D 0401260-001 D Client 1D P41-15to20 - Matrix Water Compound Concentration* DF R°L°im� Compound Concentration* DF ReLimt& Acenaphthene ND 1 0 1 10 Acenaphthylene ND — 10 10 Anthracene ND 10 10 Benzidine ND 10 50 Benzoic Acid ND 10 50 Benzo a anthracene ND 10 10 Benzo b fluoranthene ND 1 0 10 Benzo(k)fluoranthene ND 10 10 Benzo(g,h,i)perylene ND 1 0 10 Benzo(a)pyrene ND 10 t0 Benzyl Alcohol ND 1 0 20 Bis 2-chloroethox )Methane ND to 10 Bis(2-chloroeth 1)Ether ND 1 0 10 BEs(2-chloroiso rol)Ether ND 1 0 10 Bis 2-ethylhex 1)Phthalate ND 1 0 10 4-Bromo hen l Phenyl Ether ND 10 10 But lbenz ]Phthalate ND 1 0 10 4-Chloroaniline ND 1 0 20 4-Chloro-3-meth 1phenol ND 1 0 10 2-Chlomna hthalene ND 1 0 l0 2-Chlorophenol ND 1 0 10 4-Chloro hen l Phenyl Ether ND 1 0 10 chrysene ND l 0 10 Dibcnzo a,h anthracene ND to 10 Dibenzofuran ND to 10 Di-n-but 1 Phthalate ND 1 0 10 12-Dichlorobenzene ND l0 10 1,3-Dichlorobenzene ND 10 10 1,4-Dichlorobenzene ND I 10 10 3,3-Dichlorobenzidine ND 10 20 2,4-Dichlorophenol ND 1 0 10 I Diethyl Phthalate ND to 10 • 2 4-Dimethylphenol ND 10 10 Dimethyl Phthalate I ND 11 0 10 4,6-Dmttro-2-methyl henol ND 1 0 50 1 2,4-Dinitrohenol ND to 50 2 4-13tnttrotoluene ND 1 0 10 2,6-Dmitrotoluene ND 1 0 10 Di-n-octyl Phthalate I ND 10 10 1,2-Di hen lhydrazme ND to 10 _Fluoranthene ND 10 10 Fluorene ND 10 10 Hexachlaroberizene ND 10 10 Hexachlorobutadiene ND 10 10 Hexachloroc clo entadiene ND 1 0 50 Hexachloroethane ND 1 0 _ 10 Indeno(1,2,3-cd)pyrene ND 10 10 Iso horotie ND to 10 2-Meth Ina hthalene ND 10 10 2-Meth l henol(o-Cresol) ND 1 0 10 3&/or 4-Meth l henol m,p-Cresol) ND 10 10 Naphthalene ND 11 0 10 2-Nitroaniline ND 10 50 3-Nitroanilme ND 10 50 4-Nitroaniline ND 10 50 Nitrobenzene ND 10 50 2-Nitrophenol ND 10 50 4-Nitro henol ND 10 10 N-Nitrosodi hen lamme ND 1 0 10 I N-Nitrosodi-n-propylamine ND 10 10 Pcntachloro henol ND 1 0 50 Phenanthrene ND 10 10 Phenol ND ] 0 10 Pyrene ND 1 0 10 1,2,4-Trichlorobenzene ND 10 10 2,4,5-Tnchlorn henot ND I 1 0 10 2 4 6-Tnchloro henol ND 10 10 Surrogate Recoveries %SS 1 I 994 %SS2 107 %SS3 I 952 %SS4 81 5 %SS5 I 90 1 %SS6 958 Comments t "water samples and all TCLP&SPLP extracts are reported inµg/L,soil/sludge/solid samples in mglkg,wipe samples in Ag/wipe product/oil/non- aqueous liquid samples in mg/L ND means not detected above the reporting limit,N/A means analyte not applicable to this analysts #)surrogate diluted out of range,&)low or no surrogate due to matrix interference h)lighter than water immiscible sheen/product is present,i)liquid sample that contains greater than-2 vol %sediment,l)sample diluted due to high organic content,k)reporting limit raised,benzoic acid found in LCS/LCSD samples Benzoic acid found in the method blank at a detectable concentration but under the RL for this compound DHS Certification No 1644 Angela Rydelius, Lab Manager i