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, E,. AJ McCampbell Analytical, Inc. t10Telephone AvenueSouth, 5 798-1620 dFax�925-798CA 51 22560 __ ----Web www mccampbel!cam-E-mail mom r�i niccarrq)tiell cam— -- — — =- Advanced Geo>~nvlronmental,Inc CliejCLontact ID Flag City Chevron Date Sampled 01/20/04-01/22104 837 Shaw Road Date Received 01/23/04 Stockton, CA 95215 ClieTim Cuellar Date Extracted 01/23/04 ClieDate Analyzed 01/24/04-01/28/04 Serru-Volatile Organics by GC/MS(Basic Target List)* $xtracnon Method. SW3510C Analytical Method SW8270D Work Order 0401260 Lab ID 040I260-006D Client ID P40A-47to51 Matrix Water FBcnzo(b)flUOrantheneND pound Concentration * DF a`°°"mg Compound Concentration * DF Reportingt ND 1 0 IO Acena lith leve ND 10 10 ND IO 10 —Benzidine ND 10 50 Acid ND 1 0 50 Benza(a anthracene ND 10 10 Benzo 10 10 Benzo k fluoranthene ND t 0 10 ( )per lene ND 10 10 Benzo(a)p ene ND 10 to Ben I Alcohol ND 1 0 20 Bis(2-chloroethux Methane ND 1 Q 10 Bis 2-ehloroeth 1)Ether ND 1 0 10 Bis 2 chlorotso ra 1)Ether ND Bis(2-eth ]hexyl)Phthalate ND 10 10 1 0 10 4-$tomo hen l Phenyl Ether ND 10 10 But lb 1 Phthalate ND 1 0 t0 4-Chloroaniline ND 10 20 4-Chloro-3-meth l henol ND 10 10 2-Chloronaphthalene ND 2-Chloro henol ND 1 0 ]0 4 Chloro hen 1 Phen I Ether1 0 10 Ch sentND 10 10 ND [ 0 10 Dibenzo(a,h}anthracene ND to 10 Dibenzofuran ND 1 0 10 Di-n-but 1 Phthalate 12-Dichlorobenzene ND t 0 10 ND ] 0 10 1,3-Dichlorobenzene ND to I l0 1,4-Dichlorobenzene ND 10 10 3,3-Dichlorobenzidine ND l0 20 2,4-Dichloro hent ND 10 10 Dteth E Phthalate ND 10 to 2,4-Dimethyl henol ND 10 10 Dimethyl Phthalate ND 10 4,6-17initro-2-mn ethyl lie [ ND 1 0 50 2,4-Dinitro henol 10 2,4-Dmitrotoluene ND ] 0 50 ND ] 0 10 2 6-Dmitrotoluene ND 1 10 1 10 Di-n-octyl Phthalate ND 1 0 10 1,2-Dt hen th drazine ND 1 0 10 Fluoranthene ND 1 0 10 Fluorene ND 10 10 Hexachlorobenzene ND 1 0 10 Hezachlorobutadiene ND 1 U 10 Hexachloroc clo entadiene ND 1 0 50 Hexachlorcethane Indeno(1,2,3-ed p ene ND 1 0 10 ND ] 0 to � Iso horone ND ]0 10 2-Meth ]na hthalene ND 1 0 10 2-Meth ]phenol o-Cresol) ND l 0 10 3 Wor 4-Meth 1 henol m, -Cresol) ND 1 0 10 Na hthalene 2-NitroanthneI O 50 ND 10 10 ND 3-Nitraamline ND 10 50 2-Nitrop 4-NitronND t 0 50 Nitrobenzene henol ol ND 1 0 50 4-Nitro henol ND1 0 50 N-Nitrosodt hen lamine ND 10 1 10 ND 1 0 IQ N-Nitrosodt-n- ro lamme ND 10 I0 Phenol lard heno! PND 1 0 50 Phenanthrene ND 1 0 10 Phenol ND 10 10 P ene ND ] 0 10 1 2,4-Tnchlorobenzene ND 10 10 2,4,5-Trhenol 2 4 6-TrichlorohentND 10 10 ND 1 0 10 Surrogate Recoveries(%) %SS 1 %553 971 %S32 888 %SS5 867 %SS4 84 7 Comments i 81 5 %SS6 L�E� 81 2 *water samples and all TCLP&SPLP extracts are reported inµg/L,sotl/sludge/solid samples tomg/kg, in aqueous liquid samples in mg/Lwipe P samples P Ag/wipe,product/oillnon- ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis #)surrogate diluted out of range,&)low or no surrogate due to matrix interference . h)lighter than water immiscible sheen/product is present,i)liquid sample that contains greater than--2 vol %sediment,3)sample diluted due to high organic content,k)reporting limit raised,benzoic acid found in LCS/LCSD samples Benzoic acid found in the method blank at a detectable `' concentration but under the RL for this com ound DHS Certification No I644 ^- Arl ela � � g Rydeltus, Lab\M,4