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110 2nd Avenue South #D7,Pacheco CA 94553 5560 <br /> IncMcCampbell Analytical, . Telephone 925-798-1620 Fax 925-798-1622 <br /> Website www ntecantpbell cont E mail mamQmccampbell corn <br /> Advanced GeoEnvironrnental, Inc Client Project ID Flag City Chevron Date Sampled 01/20/04-01/22/04 <br /> • 837 Shaw Road Date Received 01/23/04 <br /> Client Contact Tim Cuellar Date Extracted 01/23/04 <br /> Stockton,CA 95215 <br /> Client P Q Date Analyzed 01/24/04-01/28/04 <br /> Semi-Volatile Organics by GC/MS(Basic Target List)* <br /> Extraction Method SW3510C Analytical Method SW8270D Work Order 0401260 <br /> Lab lD 0401260-007D <br /> Client 1D - P39-15to20 <br /> Matnx Water <br /> Compound Concentration* DF Re <br /> 1°°mt Compound Concentration* DF x L s <br /> Acenaphthene ND 10 10 Acenaphthylene ND 1 0 10 <br /> Anthracene ND 10 10 Benzidine ND 10 50 <br /> Benzoic Acrd ND 10 50 Benzo a anthracene ND 1 0 10 <br /> Benzo b fluoranthene ND 1 0 10 Benzo(k fluomnthene ND 1 0 10 <br /> Benzo( ,h,r)perylene ND 1 0 10 Benzo apyrene ND 1 0 10 <br /> Beng]Alcohol ND 1 0 20 Bis(2-chloroethox )Methane ND 1 0 10 <br /> Bis 2-chloroeth 1 Ether ND 1 0 10 Bis(2-chlorotso rot)Ether ND 1 0 10 <br /> Bis(2-eth ihexyl)Phthalate ND 1 0 10 4-Bromo hen I Phenyl Ether ND 1 0 10 <br /> Butylbenzyl Phthalate ND 10 10 4-Chloroaniltne ND 1 0 20 <br /> 4-Chloro-3-meth i henoi ND 1 0 10 2-Chlorona hthalene ND l 0 10 <br /> 2-Chlorophenol ND 1 0 10 4-Chloro hen 1 henyl Ether ND 1 0 10 <br /> Ch sent ND 10 10 Dibenzo(a,h)anthracene ND l0 10 <br /> Dibenzofuran ND 10 10 Di-n-but I Phthalate ND 1 0 10 <br /> 1,2-Dichlorobenzene ND 10 10 1,3-Dichlorobenzene ND 10 10 <br /> 14-Dichlorobenzene ND 10 10 3,3-Dichlorobenzidme ND 10 20 <br /> 2,4-Dichloro henol ND 1 0 10 Diethyl Phthalate ND 1 0 10 <br /> 2 4-Dimethylphenol ND 10 10 Dimethyl Phthalate ND 1 0 to <br /> 4,6-Dmitro-2-meth i henoi ND 10 50 2,4-Dmitrohenoi ND 1 0 50 <br /> 2,4-Dinitrotoluene ND f 0 10 2,6-Dinitrotoluene ND 1 0 10 <br /> Di-n-oct I Phthalate ND 10 10 l 2-Dr henxlh drazine ND 1 0 10 <br /> Fluoranthene ND 10 10 Fluorene ND 10 10 <br /> Hexachlorobenzene ND 10 10 Hexachlorobutadiene ND 10 10 <br /> Hexachloroc clo entadiene ND 10 50 Hexachloroethane ND 1 0 10 <br /> Indeno 1,2,3-cd)pyrene ND 1 0 10 Iso horone ND 1 0 10 <br /> 2-Methylnaphthalene ND 10 10 2-Meth I henoi(o-Cresol) ND 1 0 10 <br /> 3&/or4-Methyl henoi(m, -Cresol) ND 10 10 Naphthalene ND 1 D 1 10 <br /> 2-Nitroanrhne ND 10 50 3-Nitroanilme ND 10 50 <br /> 4-Nitroanilme ND 10 50 Nitrobenzene ND 10 50 <br /> 2-Nitro henol ND 1 0 50 1 4-Nitrophenol ND 1 0 10 <br /> N-Nitrosodi hen lamme ND 1 0 10 N-Nitrosodi-n- ro lamme ND 1 0 10 <br /> Pentachlorophenol ND 1 0 50 Phenanthrene ND 1 0 10 <br /> Phenol ND 10 10 P ene ND 10 10 <br /> 1,2,4-Tnchlorobenzene ND 1 0 10 2,4,5-Tnchloro henoi ND 1 0 10 <br /> 2 4 6-Tnchloro henoi ND to-1. 10 <br /> Surrogate Recoveries <br /> %SS1 lot %SS2 905 <br /> %SS3 988 %SS4 930 <br /> %SS5 93 8 %SS6 895 <br /> Comments i <br /> *water samples and all TCLP&SPLP extracts are reported inµg/L,soil/sludge/solid samples in mg/kg,wipe samples in pg/wipe,product/oil/non- <br /> aqueous liquid samples in mg/L. <br /> ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis <br /> #)surrogate diluted out of range,&)low or no surrogate due to matrix interference <br /> . h)lighter than water immiscible sheetilproduct is present,i)liquid sample that contains greater than---2 vol %sediment,l)sample diluted due to high <br /> organic content,k)reporting limit raised,benzoic acid found in LCS/LCSD samples Benzoic acid found in the method blank at a detectable <br /> concentration but under the RL for this compound <br /> DHS Certification No 1644 Angela Rydelius, Lab Manager <br />