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110 2nd Avenue South #137 Pacheco CA 94553-5560 <br /> McCabmnn <br /> ell Anal�tical,_Ine. Telephone 925-798-1620 Fax 925 798-1622 <br /> — - - - Website www mceanipbell com lrmail rnaui@rnccampbell cam� _�— <br /> Advanced GeoEnvironmental,Inc Client Project ID Flag City Chevron Date Sampled 01/20/04-01/22/04 <br /> 837 Shaw Road Date Received 01/23/04 <br /> Client Contact Tim Cuellar Date Extracted 01/23/04 <br /> Stockton, CA 95215 <br /> Client P O Date Analyzed 01/24/04-01/28/04 <br /> Semi-Volatile Organics by GC/MS(Basic Target List)* <br /> ExtrachonMethod SW3550C Analytical Method SW8270D Work Order 0401260 <br /> Lab ID 0401260-013A <br /> Client ID - P39-45' _ <br /> Matrix Soil <br /> Compound Concentration* DF Re <br /> DFLinut Concentration* DF R`Li,�s <br /> Acenaphthene ND 10 0 U Acena bthylene ND 10 1 033 <br /> Acetochlor ND 1 0 033 Anthracene ND 10 .033 <br /> Benzidine ND 10 16 Benzoic Acid ND 10 1 6 <br /> Benzo a anthracene ND 1 0 033 Benzo(b)fluoranthene ND 1 0 033 <br /> Benzo(k)Iluoranthene ND to 033 Benzo(g,h,i)perylcne ND 1 0 033 <br /> Benzo(a)pyrene ND 10 033 Ben ]Alcohol ND 1 0 066 <br /> Bis 2-chloroethox Methane ND 1 0 033 Bu(2-chloroeth 1)Ether i ND 1 0 033 <br /> Bu(2-chloroiso ro 1)Ether ND 1 0 033 Big(2-eth /hex 1)Adipate ND 1 0 033 <br /> Bis(2-eth lhex 1)Phthalate ND 1 0 033 1 4-Bromophenyl Phenyl Ether ND 1 0 033 <br /> But lbenzyl Phthalate ND 1 0 033 1 4-Chloroanihne ND 1 0 066 <br /> Nitrobenzene ND 10 16 4-Chloro-3-meth 1 henol ND 10 033 <br /> 2-Chlomna hthalene ND 1 0 033 2-Chlorophenol ND 1 0 033 <br /> 4-Chloro hen l Phenyl Ether ND 10 033 Ch Bene ND 10 033 <br /> Dibenzo(a,h)anthracene ND 1 0 033 Dibenzofuran ND 1 0 033 <br /> Di-n-but 1 Phthalate ND 1 0 033 1,2-Dichlorobenzene ND 10 033 <br /> 1 3-Dichlorobenzene ND 1 0 033 1,4-Dichlorobenzene ND 10 033 <br /> 3,3-Dichlorobenzidme ND 10 066 2,4-Dichlorohenol ND 1 0 033 <br /> Diethyl Phthalate ND 10 0 33 ` 2,4-Dimcth 1 heriol ND 10 033 <br /> Dimethyl Phthalate ND 1 0 033 4 6-Dmitro-2-meth 1 henol ND 10 1 6 <br /> 2,4-Dmttro henol ND 10 16 2,4-Dinitrvtoluene ND 10 033 <br /> 2,6-Dinitrotoluene ND 10 033 D a-oc 1 Phthalate ND 1 0 033 <br /> 1,2-Di hen {h drazme ND 1 0 033 Fluoranthene ! ND 10 033 <br /> Fluorene ND 1 0 033 Hexachlarobenzene j ND 10 033 <br /> Hexachlorobutadiene ND 1 0 033 Hexachlorocyclo entadiene ND 10 1 6 <br /> Hexachloroethane ND to 033 Indena 1,2,3 c d)pyrene ND 10 033 <br /> Iso horone ND 1 0 033 2-Methylnaphthalene ND 10 033 <br /> 2-Meth t henol(a-Cresol) ND 1 0 033 3&/or 4-Meth /phenol m, -Cresol ND 10 033 <br /> Naphthalene ND 10 033 2-Nttroantline E ND 10 16 <br /> 3-Nttroanilme ND 10 16 4-Nttroanilme ND 10 16 <br /> 2-Nitro henol ND 1 0 16 4-Nitrophenol ND 10 033 <br /> N-Nitrosodt hen lamme ND 1 0 033 N-Nitrosodi-n-propylamine ND 10 033 <br /> Pentachlorophenol.. ND 10 1 6 Phenanthrene ND 10 033 <br /> Phenol ND 10 0 33 P ne ND 10 033 <br /> 1,2,4-Tnchlorobenzene ND 1 0 033 2,4,5-Trichlorophenol ND 10 033 <br /> 2 4 6-Tnchlorohenol ND 1 0 1 033 <br /> Surrogate Recoveries(%) <br /> %SSI 946 %SS2 928 <br /> %SS3 861 %SS4 869 <br /> %SS5 823 %SS6 874 <br /> Comments <br /> *water samples and all TCLP&SPLP extracts are reported inµgfL,SOLI/sludge/solid samples to mg/kg,wipe samples in pg/wipe,product/otl/non- <br /> aqueous liquid samples in mg1L <br /> ND means not detected above the reporting limit,NIA means analyte not applicable to this analysts <br /> #)surrogate diluted out of range,&)low or no surrogate due to matrix interference <br /> h)lighter than water immiscible sheen/product is present,i)liquid sample that contains greater than-2 vol %sediment,j)sample diluted due to high <br /> organic content,k)reporting limit raised,benzoic acid found in LCS/LCSD samples Benzoic acid found in the method blank at a detectable <br /> concentration but under the RL for this compound <br /> DHS Certification No 1644 r*�l Angela Rydelius, Lab Manager <br />