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110 2nd Avenue South,#137 Pacheco CA 94553-5560 � '1 McCampbell AnalyticalInc. Telephone 925-798 1620 Fax 925-798-1622 l" J _I— — Website www mccampbell com-E nrail main@rnccampbe3l com— p Advanced GeoEnvironmental,Inc Client Project 3D Flag CityChevron Date Sampled 01/20/04-01122/04 • 837 Shaw Road Date Received 01/23/04 Client Contact Tim Cuellar Date Extracted 01/23/04 Stockton,CA 95215 Client P 0 Date Analyzed 01/24104-01/28/04 Seine-Volatile Organics by GC/MS(Basic Target List)* Extraction Method SW3510C Analytical Method SW8270D Work Order 0401260 I.ab ID 0401260-009D Client ID P39-47to51 Matrix Water Compound Concentration * DF Rcpanmg Compound Concentration* DF Reporimg i«rut Aeena hthene ND l 0 10 1Acenaphthylene ND 10 10 Anthracene ND 10 14 1 Benzidine ND 10 50 Benzoic Acid ND t 0 50 Benzo(a)anthracene ND 1 0 10 Benzo(b)fluoranthene ND 1 0 10 Benzo(k)fluoranthene ND 10 10 Benzo( h,i)perylene ND 1 0 10 Benzo(a)pyrene ND to !0 Benzy]Alcohol ND 1 0 20 Bis 2-chloroethox )Methane ND 1 0 10 Bis 2-chloroeth 1 Ether ND 1 0 10 Bis 2-chloroisa ra 1 Ether ND 1 0 !0 Bis 2-eth ihexyl Phthalate ND 1 0 10 4-Bromo hen 1 Phenyl Ether ND to 10 Bui lbenz 1 Phthalate ND 1 0 10 4-Chloroanilme ND 10 20 4-Chloro-3-methylphenol ND 1 0 10 2-Chlorona hthalene ND 1 0 10 2-Chlorophenol ND 1 0 10 4-Chlorophenyl Phenyl Ether ND 1 0 10 Chrysene ND 1 0 10 Dibenzo(a,h)anthracene ND 1 0 10 Dibenzofuran ND 1 0 10 Di-n-but I Phthalate ND 10 10 1,2-Dichlorobenzene ND ( 10 10 1 1,3-Dichlorobenzene ND 10 10 1,4-Dichlorobenzene ND 10 10 3,3-Dichlorobenzidme ND 10 20 2,4-Dichlorophenol ND t 0 10 Diethyl Phthalate ND 1 0 10 2,4-Dimeth 1 henol ND 1 0 10 Dimethyl Phthalate ND to 10 4,6-Dinitro-2-methyl henol ND 1 0 1 50 2 4-Dmitrohenol ND ] 0 50 2,4-Dmitrotoluene ND 1 0 10 2,6-Dinitrotoluene ND ] 0 10 Di-n oct 1 Phthalate ND 1 0 10 1 2-Di hen lh drazme ND 1 0 10 Fluoranthene ND I 10 10 Fluorene ND 10 l0 Hexachlorobenzene ND 1 0 10 Hcxachlorobutadiene ND to 10 Hexachieroc clo entadiene ND l 0 50 Hexachloroethane ND 1 0 10 Indeno 1 2 3-edpyrene ND 1 0 10 Iso horone ND 10 10 2-Methylnaphthalene ND 1 0 10 2-Meth 1 henol o-Cresol} ND 1 0 10 3&/or 4-Meth 1 henol m -Cresol) ND 1 0 10 Naphthalene ND 10 10 2-Nitroanilme ND 10 50 3-Nitroanilme ND 10 50 4-Nitroanilme ND 1 0 50 Nitrobenzene ND to 50 2-Nitrophenol ND 1 0 50 4-Nitrophenol. ND 10 10 N-Nitrosodi hen ]amine ND 1 0 10 N-Nitrosodi-n- ropylarnme ND 10 10 Pentachlorophenol ND 1 0 50 Phenanthrene ND 1 0 10 Phenol ND 1 0 10 EXrene ND 10 10 1,2,4-Trichlorobenzene ND 1 0 10 2,4,5-Trichlorophenol ND 10 10 2,4,6-Trichlorophenol ND t 0 to Surrogate Recoveries(%) %SSI 919 %SS2 95 5 %SS3 914 %SS4 904 %SS5 868 %SS6 880 Comments i *water samples and all TCLP&SPLP extracts are reported inµg/L,soil/sludge/sohd samples in mg/kg wipe samples in lig(wipe product/oil/non- aqueous liquid samples in mg/L ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis #)surrogate diluted out of range,&)low or no surrogate due to matrix interference • h)lighter than water immiscible sheeniproduct is present,i)liquid sample that contains greater than--2 vol %sediment,j)sample diluted due to high organic content,k}reporting limit raised,benzoic acid found in LCS/LCSD samples Benzoic acid found in the method blank ata detectable concentration but under the RL for this compound DHS Certification No 1644 1i�W Angela Rydehus, Lab Manager