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T 110 2nd Avenue South,#D7 Pacheco CA 94553-5560 <br /> McCampbell Analytical, IIIc. _ Telephone 925 798-1620 Fax 925-798-1622 — — <br /> _—Website wwwmccaiMbell corn-£-niatl main®mccampbell com— <br /> Advanced GeoEnvironinental,Inc Client Project ID Flag City Chevron Date Sampled 01/20/04-01/22/04 <br /> . 837 Shaw Road <br /> Date Received 01/23/04 <br /> Client Contact Tim Cuellar Date Extracted 01/23/04 <br /> Stockton,CA 95215 <br /> [Client P O Date Analyzed 01/24/04-01/28/04 <br /> Serru-Volatile Organics by GCIMS(Basic Target List)* <br /> Extraction Method SW3550C Analytical Method SW8270D Work Order 0401260 <br /> Lab M 0401260-015A <br /> Client 1D P40A-30' '— <br /> Matrix Soil <br /> Reporting <br /> Compound Concentration* DF ReL,mt'g Compound Concentration * DF Lmat <br /> Acenaphthene ND 10 033 Acena hth leve ND 10 033 <br /> Acetochlor ND 1 0 033 Anthracene ND 10 033 <br /> Benzidine ND P10 <br /> 16 Benzoic Acid ND 10 16 <br /> Benzo(a)anthracene ND 033 Benzo )fluoranthene ND 10 033 <br /> Benzo k fluoranthene ND 033 Benzo( ,h,i icnc ND 10 033 <br /> Benzo(a)pyrene ND 033 Benzyl Alcohol ND 10 066 <br /> Bis 2-chloroethox Methane ND 033 His(2-chloroeth l)Ether ND 10 033 <br /> Bis(2-chloroiso ro yl Ether ND 033 Bis 2-eth ihex 1 Adi ate ND 10 033 <br /> Bis 2-eth lhexyl)Phthalate ND 0 33 4-Bromo hen 1 Phenyl Ether ND 10 033 <br /> ButylbenKyl Phthalate ND 1 0 033 4-Chloroaniline ND 10 066 <br /> Nitrobenzene ND 1 0 16 4-Chloro-3-methylphenol ND to 033 <br /> 2-Chlorona hthaiene ND 1 0 033 2-Chlorophenol ND 10 033 <br /> 4-Chloro hen I Phenyl Ether ND 10 033 Ch Bene ND -16 —o33 <br /> Dibenzo(a,h)anthracene ND 10 10 33 Dibenzofuran ND 10 033 <br /> Di-n-butyl Phthalate ND 1 0 033 1,2-Dichlorobenzene ND 10 033 <br /> 1,3-Dichlorobenzene ND 1 0 033 1,4-Dichlorobenzene ND 10 033 <br /> 3,3-Dichlorobenzidme ND 1 0 066 2 4-Dichloro henol ND 10 033 <br /> Diethyl Phthalate ND 1 0 033 2 4-Dimeth 1 henol ND 10 on <br /> Dimethyl Phthalate ND 1 0 033 4,6-Dmrtro-2-melh phenol ND 10 16 <br /> 2,4-Dinitro henol ND 10 16 2,4-Dinitrotoluene ND 10 033 <br /> 2,6-Dinitrotoluene ND 1 4 033D t 1 Phthalate ND l 0 033 <br /> 1 2-Di hen ih drazme ND 1 0 0 33 Flucranthene ND 1 0 033 <br /> Fluorene ND 1 0 0 33 Hexachlorobenzene ND 10 033 <br /> Hexachlorobutadiene ND 1 0 033 Hexachlorocyclo entadiene ND 10 16 <br /> Hexachioroethane ND 1 0 0 33 indeno Q 2 3-cdpyrene ND 10 033 <br /> lso horone ND 1 0 033 2-Methyina hthalene ND 10 033 <br /> 2-Meth 1 henol(a-Cresol) ND 1 0 033 3&lar 4-Meth 1 henol(m, -Cresol) ND 1 0 0 33 <br /> Naphthalene ND 1 0 033 2-Nitroanthne ND 1 0 1 6 <br /> 3-Nttroaniline ND 10 16 4-Nitroaniline ND 10 l6 <br /> 2-Nitrophenol ND 1 0 1 1 6 4-Nitro henot ND 10 033 <br /> N-Nitrosodi hen lamme ND 1 0 03-3 N-Nitrosodi-n-propylamine ND 10 033 <br /> Pentachloro henol ND 1 0 1 6 Phenanthrene ND 10 033 <br /> Phenol ND 1 0 033 n7ene ND 1 0 033 <br /> 1,2,4-Tnchlorobenzene ND 1 0 033 1 2.4,5-Trichlorophenol ND 10 033 <br /> 2,44-Trichlorophenol ND 1 0 033 <br /> Surrogate Recoveries <br /> %SSI 104 %SS2 104 <br /> %SS3 876 %SS4 889 <br /> %SS5 I 928 %SS6 938 <br /> Comments <br /> *water samples and all TCLP&SPLP extracts are reported inµg/L,so11/sludgelsolid samples in mg/kg,wipe samples inµg/wipe,product/oil/non- <br /> aqueous liquid samples in mg/L. <br /> ND means not detected above the reporting limit,NIA means analyte not applicable to this analysis <br /> • #)surrogate diluted out of range,&)low or no surrogate due to matrix interference <br /> h)lighter than water immiscible sheen/product is present,i)liquid sample that contains greater than--2 vol %sediment,j)sample diluted due to high <br /> organic content,k)reporting limit raised,benzoic acid found in LCS/LCSD samples Benzoic acid found in the method blank at a detectable <br /> concentration but under the RL for this com ound <br /> DHS Certification No 1644 'Angela Rydelius, Lab Manager <br />