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110 2nd Avenue South,ND7,Pacheco,CA 94553-5560 <br /> Inc.McCampbell Analytical, Telephone 925-798 1620 Fax 925-798-1622 <br /> Website www rmcarripbell com E mail main®mecampbell corn--=_ - - ---_ <br /> Advanced GeoEnvtronmental,Inc Cltent Project ID Flag City Chevron Date Sampled 01120/04-01/22/04 <br /> $37 Shaw Road <br /> Date Received 01/23/04 <br /> Client Contact Tina Cuellar Date Extracted 01/23/04 <br /> Stockton,CA 95215 <br /> Client P Q Date Analyzed 01/24/04-01/28/04 <br /> Semi-Volatile Organics by GC/MS(Basic Target List)* <br /> Extraction Method SW3550C Analytical Method SW8270D Work Order 0401260 <br /> Lab ID 0401260-016A <br /> Client ID P40A-45' <br /> Matrix Soil <br /> ltcp°nmg <br /> Compound Concentration* DF I RL g Compound Concentration * DF E m,t <br /> Acenaphthene ND 10 033 Acenaphthylene ND 1 0 033 <br /> Acetochlor ND 10 033 Anthracene ND 1 0 033 <br /> Benzidine ND 1 0 16 Benzoic Acid ND 1 0 16 <br /> Benzo(a)anthracene ND l 0 033 Benzo(b)fluoranthene ND 1 0 033 <br /> Benzo k fluoranthene ND 10 033 Benzo( ,h,i) rylene ND 1 0 033 <br /> Benzo(a)pyrene ND 1 0 033 Ben l Alcohol ND 1 0 066 <br /> Bis(2-chloroethoxy)Methane ND 10 033 Bis 2�hloroeth 1)Ether ND 1 0 033 <br /> Bis(2-chlorolso rop 1)Ether ND 1 0 033 Bis 2-ethylhex I Adipate ND 1 0 033 <br /> Bis(2-eth)4hexyl Phthalate ND 10 033 4-Bromo hen 1 Phen I Ether ND 1 0 033 <br /> Butylbenzyl Phthalate ND 10 033 4-Chloroanilme ND 1 0 066 <br /> Nitrobenzene ND 1 0 1 6 4-Chloro-3-meth i henol ND 1 0 033 <br /> 2-Chlorona hthalene ND 10 033 2-Chloro henoI ND 1 0 033 <br /> 4-Chloro hen 1 Phenyl Ether ND 1 0 033 Ch ene ND t 0 033 <br /> Dibenzo(a h)anthracene ND 10 033 Dibenzofuran ND 1 0 033 <br /> Di-n-butyl Phthalate ND 10 033 1 2-Dichlorobenzene ND 10 033 <br /> 1,3-1)ichlorobenzene ND 10 033 1,4-Dichlorobenzene ND 1 0 033 <br /> 3,3-Dichlorobenzidme ND 10 066 2 4-Dichlorophenol ND 1 0 033 <br /> Dicth 1 Phthalate ND 10 033 2,4-Dimethylphenol ND 10 033 <br /> Dimethyl Phthalate ND 10 033 4,6-Dmrtro-2-methyl keno] ND 10 --16 <br /> 2,4-Dinitro henol ND 10 16 2,4-Dinitrotoluene ND 1 0 033 <br /> 2,6-Dinitrotoluene ND 1 0 033 Di-n-oc 1 Phthalate ND 1 0 033 <br /> 1,2-Di hen lh drazine ND 1 0 033 Fluoranthene ND 1 0 033 <br /> Fluorene ND to 033 Hexachlorobenzene ND 1 0 033 <br /> Hexachlorobutadiene ND 1 0 033 Hexachloro clo entadiene ND 1 0 1 6 <br /> Hexachloroethane i ND 1 0 033 indeno 1,2,3-cd}pyrene ND 1 0 033 <br /> Isophoronc ND 1 0 033 2-Methyina hthalene ND l 0 033 <br /> 2-Meth 1 henol(o-Cresol) ND 1 0 033 3&/or 4-Meth 1 henol(m, -Cresol ND l 0 033 <br /> Naphthalene ND l 0 033 , 2-Nitroanilme ND 10 16 <br /> 3-Nitroanilme ND t O 1 6 4-Nitroantlme ND 10 l 6 <br /> 2-Nitro henol ND 1 0 l 6 4-Nitrophenol ND 1 0 033 <br /> N-Nrtrosodi henylamme ND 1 0 033 N-Nitrosodi-n-propytamine ND 1 0 033 <br /> Pentachlorophenol ND 1 0 1 6 Phenanthrene ND 10 033 <br /> Phenol ND 1 0 033 Pyrene ND 10 033 <br /> 1 2,4-Tnehlorobenzene ND 10 033 2,4,5-Tnehlorophenol ND 10 033 <br /> 2 4 6-Tnehlorohenol ND 1 0 033 <br /> Surrogate Recoveries(%) <br /> %SS 1 106 0/.SS2 107 <br /> %SS3 893 %SS4 988 <br /> %SS5 857 %SS6 956 <br /> Comments <br /> *water samples and all TCLP&SPLP extracts are reported in gg(L.,soil/sludge/solid samples in mg/kg,wipe samples inµg/wipe,product/orllnon- <br /> aqueous liquid samples in mg/L <br /> ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis <br /> • #)surrogate diluted out of range,&)low or no surrogate due to matrix interference <br /> h)lighter than water immiscible sheen product is present,i)liquid sample that contains greater than--2 vol %sediment J)sample diluted due to high <br /> organic content,k)reporting limit raised,benzoic acid found in LCS/LCSD samples Benzoic acid found in the method blank at a detectable <br /> concentration but under the RL for this compound <br /> DHS Certification No 1644 �� Angela Rydehus,Lab Manager <br />