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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCain bell Analylical, Inc. Telephone 925-798 1620 Fax 925-798 1622 ma <br /> -4>�--- -_-- — ——_---- `�- - -- ----- - -- - -- Website www ecampbell corn E-mailE-marl in®mecamphell Com <br /> — —— <br /> Advanced GeoEnviromnental,Inc Client Project ID Flag City Chevron Date Sampled 01/20/04-01122/04 <br /> 837 Shaw Road Date Received 01/23/04 <br /> Client Contact Tum Cuellar Date Extracted 01/23/04 <br /> Stockton,CA 95215 <br /> Chent P O Date Analyzed 01/24104-01/28/04 <br /> Senn-Volatile Organics by GUMS(Basic Target List)* <br /> Extraction Method SW3550C Analyucal Method SW8270D Work Order 0401260 <br /> Lab ID 0401260-017A <br /> Client ID P41-15' <br /> Matrix Soil <br /> R <br /> Compound Concentration * DF �ts Compound Concentration* DF Report <br /> Lana1.arut <br /> Acenaphthene ND 1 0 0 33 Acena hth line ND 1 0 033 <br /> Acetochlor ND 1 0 033 Anthracene ND 1 0 033 <br /> Benzidine ND 10 16 Benzoic Acid ND 10 16 <br /> Benzo(a)anthracene ND 1 0 033 Benzo(b)fluoranthene ND to 033 <br /> Benzo(k)fluoranthene ND 1 0 033 Benzo(g,h,i)perylene ND 1 0 033 <br /> Benzo a e ND 1 0 033 Benzyl Alcohol ND 1 0 066 <br /> Bis 2-chlomethox )Methane ND 1 0 033 Bis 2-chioroeth l)Ether ND 1 0 033 <br /> Bas(2-chloroisopropyi)Ether ND 1 0 033 Bis 2�th lhex l)Adipate ND 10 033 - <br /> Bis(2-eth lhex k)Phthalate ND 1 0 033 1 4-Bromo henyl Phenyl Ether ND 10 033 <br /> Butylbenj Phthalate ND 1 0 033 4-Chloroanlime ND 10 066 <br /> Nitrobenzene ND 1 0 16 4-Chloro-3-meth l henot ND 10 033 <br /> 2-Chlorona hthalene ND E 1 0 033 2-Chlorophenol ND 1 0 033 <br /> 4-Chloro hen t Phenyl Ether ND ! 1 0 033 Ch Bene ND l 0 033 <br /> Dibenzo a,h anthracene ND 1 0 033 Dibenzofuran ND 1 0 033 <br /> Di-n-bit I Phthalate ND 1 0 033 1,2-Dichlorobenzene ND 1 0 033 <br /> 1,3-Dichlorobenzene ND 1 0 033 1,4-Dichlorobenzene ND 1 0 033 <br /> • 3,3-Dwhlorobenzidine ND 1 0 066 2,4-Dichloro henol ND 1 0 033 <br /> Diethyl Phthalate ND 10 0 33 2,4-Dimethyl henol ND 1 0 033 <br /> Dimethyl Phthalate ND 1 0 033 4,6-Dmitro-2-meth 1 henol ND 10 16 <br /> 2,4-Dmitro henol ND l 0 16 2,4-Dinitrotoluene ND 10 033 <br /> 2,6-Dmitrotoluene ND 1 0 033 Di-n-octyl Phthalate ND 10 033 <br /> 1,2-Di hen lh drazme ND 1 0 033 Fluoranthene ND '110 0 33 <br /> Fiuorene ND 1 0 033 Hexachlorobenzene ND 10 033 <br /> Hexachlorobutadiene ND 1 0 033 Hexachlaroc clo entadiene ND 10 16 <br /> Hexachloroethane ND 1 0 033 Indeno 1,2 3-ed e ND 1 0 033 <br /> Iso horone ND 1 0 033 2-Methylnaphthalene ND 1 0 033 <br /> 2-Meth t henol(o-Cresol) ND 1 0 033 3&/or 4-Meth 1 henol(m,p-Cresol) ND 10 033 <br /> Naphthalene ND 1 0 033 2-Nitroanthne ND 1 0 1 6 <br /> 3-Nitroaniline ND l0 16 4-Nitroaniline ND 10 16 <br /> 2-Nitrophenol 1, ND 1 0 1 6 4-Nitro henoi ND 10 033 <br /> N-Nitrosodi hen famine ND 1 0 033 N-Nitrosodi-n- rolamme ND 1 0 033 <br /> Pentachlorophenol ND 1 0 1 6 Phenanthrene ND 1 0 0 33 <br /> Phenol ND 1 0 033 Pyrene ND 1 0 033 <br /> 1,2,4-Trichlorobenzene ND 1 0 033 2,4,5-Trichlorophenol ND 1 0 033 <br /> 2 4 6-TnchlorohenoI ND I 1 0 1 033 <br /> Surrogate Recoveries(%) <br /> %SSI 969 %SS2 90 6 _ <br /> %SS3 883 %SS4 844 <br /> %SS5 72 2 %SS6 880 <br /> Comments <br /> *water samples and all TCLP&SPLP extracts are reported in pg/L,soil/sludge/solid samples in mg/kg,wipe samples in pg/wipe,product/otVnon- <br /> aqueous liquid samples in mg/L <br /> ND means not detected above the reporting limit,NIA means analyte not applicable to this analysis <br /> #)surrogate diluted out of range,&)low or no surrogate due to matrix interference <br /> h)lighter than water immiscible sheen/product is present,t)liquid sample that contains greater than--2 vol %sediment,j)sample diluted due to high <br /> organic content,k)reporting limit raised,benzoic acid found in LCSlLCSD samples Benzoic acid found in the method blank at a detectable <br /> conecntration but under the RL for this compound <br /> DHS Certification No 1644 Angela Rydelius, Lab Manager <br />