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110 2nd Avenue South #137,Pacheco CA 94553-5560 <br /> I <br /> McCampbell Analytical, nC. Telephone 925 798 1620 Fax 925-798 1622 <br /> Websrle www mecampbell com E-mail main@mccampbell cam -- - - — <br /> Advanced GeoEnvironmental, Inc Client PrRlect ID Flag City Chevron Date Sampled 01120104-01/22/04 <br /> . 837 Shaw Road Date Received 01/23/04 <br /> Stockton,CA 95215 <br /> Client Contact Tim Cuellar Date Extracted 01/23/04 <br /> - <br /> Client P O Date Analyzed 01124104-01/28/04 <br /> Semi-Volatile Organics by GC/MS(Basic Target List)* <br /> Extraction Method SW3550C Analytical Method SW8270D Work Order 0401260 <br /> Lab ID 0401260-019A <br /> Client ID - P41-45' i- <br /> Matrix Soil <br /> DFR�"O"N& ReCom ound Concentration t Compound Concentration DF Lmt <br /> Acena hthene ND 1 0 0 33 Acena hthylene ND 10 0 33 <br /> Acetochlor ND 1 0 033 Anthracene ND 1 0 033 <br /> Benzidine ND 1 0 1 6 Benzoic Acid ND 1 0 16 <br /> Benzo(a)anthracene ND 1 0 0 33 Benzo fluoranthene ND 1 0 033 <br /> Benzo(k)fluoranthene ND 1 0 033 Benzo(g,h,i)perylene ND 1 0 033 <br /> Benzo(a)pyrene ND 1 0 0 33 Benzy[Alcohol ND 1 0 1 066 <br /> Bis(2-chloroethox )Methane ND 1 0 033 Bis 2-chloroethyl)Ether ND I 0 0 33 <br /> Brs 2-chloroiso ro 1 Ether ND 1 0 033 Bis 2-eth lhex 1)Adipate ND 1 0 033 <br /> Bis(2-ethylhexyl)Phthalate ND 1 0 033 4-Bromophen l Phenyl Ether ND 1 0 033 <br /> Butylbenzyl Phthalate ND 1 0 033 4-Chloroanilme ND 1 0 066 <br /> Nitrobenzene ND 1 0 1 6 4-Chloro-3-methyl henol ND 1 0 033 <br /> 2-Chlorona hthalene ND 1 0 033 2-Chloro henol ND 1 0 0 33 <br /> 4-Chloro hen ]Phenyl Ether ND 1 0 033 Chrysene ND 1 0 033 <br /> Dibenzo(a,h)anthracene ND 1 0 033 Dibenzo£uran ND 1 0 -033 <br /> Di-n-but ]Phthalate ND 1 0 033 1,2-Dtchlorobenzene ND k 1 0 033 <br /> 1,3-Dichlorobenzene ND l 0 033 1,4-Du,hlorobenzene ND 1 0 033 <br /> 3 3-Dichlorobenzidme ND 1 0 066 2,4-Dichlorophenol ND 1 0 033 <br /> Diethyl Phthalate ND 1 0 033 2,4-Dimethylphenol ND 1 0 033 <br /> Dimethyl Phthalate ND 1 0 033 4,6-Dmrtro-2-meth 1 hetsol ND 1 0 1 6 <br /> 2,4-Dmrtro henol ND 1 0 1 6 2,4-Dtnrtrotoluene ND 1 0 033 <br /> 2,6-Dinitrotoluene ND 1 0 033 Di-n-oct 1 Phthalate ND 11 0 033 <br /> 1 2-Di henyih drazine ND 1 0 033 Fluoranthene ND 1 0 033 <br /> Fluorene ND 1 0 033 Hexachlorobenzene ND 1 0 033 <br /> Hexachlorobutadiene ND 1 0 033 Hexachloroc clopentadiene ND 1 0 16 <br /> Hexachlomethane ND — 10 0 33 Indeno 1,2 3-cd) ne ND 11 0 033 <br /> iso horone ND 1 0 033 2-Meth Ina hthalene ND 1 0 033 <br /> 2-Methyl henol(o-Cresol) ND 1 0 033 3 Wor 4-Meth 1 henol(m, -Cresol) ND 1 0 033 <br /> Naphthalene ND 10 0 33 2-Nitroaniline ND 1 0 1 6 <br /> 3-Nitroanilme ND 10 16 4-Natroanrime ND I 10 16 <br /> 2-Nitrohenol ND 1 0 1 6 1 4-Nitro henol ND 1 0 033 <br /> N-Nitrosodl here lamme ND 10 033 N-Nitrosodt-n-pr9pXlamme ND l 0 033 <br /> Pentachlorophenol ND 10 16 Phenanthrene ND 1 0 033 <br /> Phenol ND 10 033 Pyrene ND 1 0 033 <br /> 1,2,4-Tnchlorobenzene ND 1 0 033 2,4,5-Tnchloro henol ND 1 6 0 33 <br /> 2 4 6-Tnchloro henol ND 10 0 33 <br /> Surrogate Recoveries(%) <br /> %SSI 95 9 %SS2 I 85 8 <br /> %SS3 884 %SS4 85 0 <br /> %SS5 85$ %SS6 892 <br /> Comments <br /> "water samples and all TCLP&SPLP extracts are reported inµg/L,soillsludge/solid samples in mg/kg,wipe samples to jig/wipe,productlod/non- <br /> aqueous liquid samples in mg/L <br /> ND means not detected above the reporting limit,NIA means analyte not applicable to this analysis <br /> #)surrogate diluted out of range,&)low or no surrogate due to matrix interference <br /> h)lighter than water immiscible sheen/product is present,i)liquid sample that contains greater than—2 vol %sediment,j)sample diluted due to high <br /> organic content,k)reporting limit raised,benzoic acid found in LCS/LCSD samples Benzoic acrd found in the method blank at a detectable <br /> concentration but under the RL for this compound <br /> DHS Certification No 1644 Angela Rydelius, Lab Manager <br />