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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCampbell Analytical, Inc. Telephone 925-798-1620 1-ax 925-798-1622 <br /> Website www mccampbOl com E-mail main@mccampbell com-= - -- <br /> Advanced GeoEnvlronmental, Inc Client Project ID Flag City Chevron Date Sampled 01/20104-01122104 <br /> 837 Shaw Road Date Received 01/23/04 <br /> Stockton, CA 95215 Client Contact Tim Cuellar Date Extracted 01/23/04 <br /> Client P O Date Analyzed 01/24104-01/28/04 <br /> Sent-Volatile Organics by GC/MS(Basic Target List)* <br /> Extraction Method SW3550C Analytical Method SW8270D Work Order 0401260 <br /> Lab ID 0401260-020A <br /> Client ID - P42-10' <br /> Matrix Soil <br /> Compound Concentration * DF x s Compound Concentration * DP Urmt <br /> Remg <br /> bAcetocblor <br /> hthene ND 1 0 0 33 Acena hth lene ND 10 -033 <br /> ND 1 0 033 Anthracene ND 10 033 <br /> ine ND 1 0 1 6 Benzoic Acid ND 10 16 <br /> )anthracene ND 1 0 033 Benzo(b)tluoranthene ND 10 033 <br /> Benzo(k)fluoranthene ND 1 0 0 33 Benzo(Y_hj)perylene ND 10 033 <br /> Benzo(a)pyrcne ND 1 0 0 33 Benzyl Alcohol ND 10 066 <br /> Bis 2-chloroethox Methane ND 1 0 033 Bis 2�hloroeth l Ether ND 10 033 <br /> Bis 2-chlorotso ra I)Ether ND 1 0 033 Bis(2-eth Ihex1 Adi ate ND 1 0 0 33 <br /> Bis 2 eth the I)Phthalate ND 1 0 0 33 4-Bromo hen I Phenyl Ether ND 10 033 <br /> But lbenzyl Phthalate ND 1 0 033 4-Chloroanilme ND 1 0 066 <br /> Nitrobenzene ND i 1 0 1 6 4-Chloro-3-methylphenol ND <br /> 10 033 <br /> 2-Chloronaphthalene ND 1 0 033 2-Chlorophenol ND 1 0 033 <br /> 4-Chloro henyl Phenyl Ether ND 1 0 033 Ch serve ND 10 033 <br /> Dibenzo(a,h)anthracene ND 1 0 1 033 Dibenzofuran ND 10 033 <br /> Di-n-butyl Phthalate ND 1 0 0 33 1,2-Dichlorobenzene ND to 033 <br /> 1 3-Dichlorobenzene ND 1 0 033 1,4-1)ichlorobenzene ND 10 033 <br /> 3 3-Dichlorobenzidine ND 1 0 066 2,4-Dichloro henol ND 10 033 <br /> Diethyl Phthalate ND 1 0 033 2,4-Dimethylphenol ND 10 033 <br /> Dimethyl Phthalate ND —to 033 4,6-Dinitro-2-methyl henol ND 1 0 16 <br /> 2 4-Dmitro henol ND l 0 16 2,4-Dmitrotoluene ND 10 033 <br /> 2,6-Dmitrotoluene ND 1 0 1 033 Di-n-oct 1 Phthalate ND 10 033 <br /> 1 2-15i hen lb dtazme ND 1 0 033 Fluoranthene ND 10 033 <br /> Fluorene ND 1 0 033 1-Iexachlorobenzene ND 10 —033 <br /> Hexachlorobutadiene ND l 0 033 Hexachloroc clo entadiene ND 1 0 16 <br /> Hexachloroethane ND 1 0 033 Indeno(1,2 3-cdpyrene ND 1 0 033 <br /> Iso horone ND 1 0 033 2-Methylnaphthalene ND 10 033 <br /> 2-Meth 1 henol o-Cresol ND 1 0 033 3 Wor 4-Mcth ]phenol m p-Cresol ND 1 0 033 <br /> Naphthalene NO 1 0 033 2-Nitroaniline ND 10 16 <br /> 3-Nitroandme ND 10 16 4-Nilroamline ND 10 16 <br /> 2-Nitro henol ND 1 0 1 6 4-Nitro hent ND 1 0 033 <br /> N-Nitrosodt hen lamme ND 1 0 033 N-Nitrosodi-n- ro lamine ND 1 0 033 <br /> Pentachlorophenol ND 1 0 16 Phenanthrene ND 10 033 <br /> Phenol ND 1 0 033 Pyrenc ND 10 033 <br /> 1,2,4-Trichlorobenzene ND 1 0 033 2,4,5-Tnchlora henol ND 1 0 033 <br /> 2 4 6-Tnchlorohenol ND 1 0 033 <br /> Surrogate Recoveries(%) <br /> %SS 1 81 8 %SS2 842 <br /> %SS3 81 1 %SS4 788 <br /> %SS5 800 %SS6 <br /> 797 <br /> Comments <br /> *water samples and all TCLP&SPLP extracts are reported in 994,soil/sludge/solid samples in mg(kg,wipe samples inµg/wipe,product/oil/non- <br /> aqueous liquid samples in mg/L. <br /> ND means not detected above the repotting limit,N/A means analyte not applicable to this analysis <br /> #)surrogate diluted out of range,&)low or no surrogate due to rriatnx interference <br /> h)lighter than water immiscible sheen/product is present,i)liquid sample that contains greater than-2 vol %sediment,j)sample diluted due to high <br /> organic content,k)reporting limit raised,benzoic acid found in LCS/LCSD samples Benzoic acid found in the method blank at a detectable <br /> concentration but under the RL for this compound <br /> DHS Certification No 1644 C\�WyAngela Rydelius,Lab Manager <br />