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110 2nd Avenue South,#tD7 Pacheco CA 94553-5560 <br /> McCain bell Anal XcW Inc. Telephone 925-798-1620 Fax 925 798-1622 <br /> `� —— •—-- —-- -- — --- Website www r ccampbell corn E mail main@twcampbell coin - -- — —--- <br /> Advanced GeoEnvlronmental,Inc Client Project ID Flag City Chevron Date Sampled 01/20/04-01122104 <br /> 837 Shaw Road Date Received 01/23/04 <br /> Client Contact Tim Cuellar Date Extracted 01/23/04 <br /> Stockton, CA 95215 <br /> Client P O Date Analyzed 01124/04-01/28/04 <br /> Semi-Volatile Organics by GC/MS(Basic Target List)* <br /> Extraction Method SW3550C Analytical Method SW8270D Work Order 0401260 <br /> Lab ID 0401260-021 A <br /> Client ID P42-15' <br /> Matrix Soil <br /> Compound Concentration* DF xepar <br /> r�;& Compound Concentration* DF `�,�;'e <br /> Acenaphthene ND 1 0 033 Acenaphthylene ND 10 033 <br /> Acetochlor ND 1 0 033 Anthracene ND 1 0 033 <br /> Benzidine ND 1 0 1 6 Benzoic Acid ND 10 1 6 <br /> Benzo(a)anthracene ND 1 0 033 Benzo b fluoranthene ND 1 0 033 <br /> Benzo(k)fluoranthene ND 1 0 033 Bcnzo(g,h,i)perylene ND 1 0 033 <br /> Benzo a ene ND 1 0 033 Benzyl Alcohol ND 1 0 066 <br /> Bis 2-chloroethox Methane ND 1 0 033 Bis(2-chloroethyi)Ether ND 1 0 033 <br /> Bis(2-chloroiso ro 1)Ether ND 10 033 Bis(2-eth lhex l)Adipate ND 1 0 033 <br /> Bis 2-eth [hex 1 Phthalate ND l 0 033 4-Bromo hen t Phenyl Ether ND 1 0 033 <br /> But ]ben 1 Phthalate ND 10 1 033 4-Chloroanilme ND 1 0 066 <br /> Nitrobenzene ND 10 16 4-Chloro-3-methyl henoI ND 1 0 033 <br /> 2-Chlorona hthalene ND 1 0 033 2-Chlorophenol I ND 10 033 <br /> 4-Chiorohen I Phenyl Ether ND 1 0 1 0 33 Ch sere ND 1 0 033 <br /> Dibenzo a,h anthracene ND 1 0 033 Dibenzofuran ND 1 0 033 <br /> Di-n-butyl Phthalate ND 1 0 033 1 2-Dichlorobenzene ND 1 0 033 <br /> 1,3-Dichlorobenzene ND 1 0 033 1,4-Dichlorobenzene ND 1 0 033 <br /> 3,3-Dichiorobenzidine ND 1 0 066 2,4-Dichlorohenol ND 1 0 033 <br /> Diethyl Phthalate ND 10 033 2,4-Dimeth iphenol ND 1 0 033 <br /> Dimethyl Phthalate ND 1 0 033 4,6-Dinitro-2-meth I henol ND 1 0 1 6 <br /> 2,4-Dinitrohenol ND 10 16 2,4-Dinitrotoiuene ND 1 0 033 <br /> 2,6-Dinitrotoluene ND 10 033 Di-n-octyl Phthalate ND 1 0 033 <br /> 1,2-Di hen lh drazine ND 10 033 Fluoranthene ND 1 0 033 <br /> Fluorene ND 1 0 033 Hexachlorobenzene ND 1 0 033 <br /> Hexachlorobutadiene ND 1 0 033 Hexachloroc clo entadiene ND 1 0 1 6 <br /> Hexachlornethane ND 1 0 033 Indeno(1,2,3-cd)pyrene ND 1 0 033 <br /> Iso horone ND 1 0 033 2-Methylnaphthalene ND 10 0 33 <br /> 2-Meth I henol(o-Cresol) ND 1 0 033 3&Jar 4-Meth 1 henot(m -Cresol) ND l 0 033 <br /> Naphthalene ND 1 0 033 2-Nitroaniline ND 1 0 16 <br /> 3-Nitroanrhne ND 1 0 1 6 4-Nitroanilme ND 1 0 t 6 <br /> 2-Nitro hcnol ND 1 0 1 6 4-Nitrophenol ND 1 0 0 33 <br /> N-Nitrosodt hen lamme ND l 0 0 33 N-Nitrosodi-n-pEopylamine ND 1 0 033 <br /> Pentachlorophenol ND 1 0 1 6 Phenanthrene ND 10 0 33 <br /> Phenol ND 1 0 033 Pyrene ND 1 0 033 <br /> 1 2,4-Trichlorobenzene ND 1 0 033 2,4,5-Tnchlora henol ND 1 0 4 33 <br /> 2 4 6-Tnehlorohenol I ND 1 0 0 33 <br /> Surrogate Recoveries(%) <br /> %SSI 979 %SS2 85 6 <br /> %SS3 883 %SS4 905 <br /> %SSS 810 %SS6 90 8 <br /> Comments <br /> *water samples and all TCLP&SPLP extracts are reported inµSIL,soil/studge/sohd samples in mg/kg,wipe samples toµg/wipe,product/oil/non- <br /> aqueous liquid samples in mg/L <br /> ND means not detected above the reporting limit,NIA means analyte not applicable to this analysis <br /> #)surrogate diluted out of range,&)low or no surrogate due to matrix interference <br /> h)lighter than water immiscible sheen/product is present,i)liquid sample that contains greater than—2 vol %sediment,j)sample diluted due to high <br /> organic content,k)reporting limit raised,benzoic acid found in LCS/LCSD samples Benzoic acid found in the method blank at a detectable <br /> concentration but under the RL for this compound <br /> DHS Certification No 1644 CAngela Rydehus, Lab Manager <br />