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1102nd Avenue South #D7 Pacheco CA 94553-5560 <br /> I <br /> McCampbell Analytical, In C. Telephone 925-798-1620 Fax 925-798 1622 <br /> -f _-- - -- - ------ --_—- -- - ---_ -- - -Website www inccanipbell com E mail mainta mccampbell cam---- <br /> Advanced GeoEnvironmental,Inc Client Project ID Flag City Chevron Date Sampled 01120104-01122104 <br /> 837 Shaw Road Date Received 01/23/04 <br /> Client Contact 'Tim Cuellar Date Extracted 01/23/04 <br /> Stockton, CA 95215 <br /> =Clicnt Date Analyzed 01124104-01128104 <br /> Septi-Volatile Organics by GUMS(Basic Target List)* <br /> Extraction Method SW3550C Analytical Method SW8270D Work Order 0401260 <br /> Lab ID 0401260-024A <br /> Client ID P43-15' <br /> Matrix Soil <br /> Compound Concentration* DF a L=t Compound Concentration * DF R`L°mt rting <br /> Arena hthene ND 1 0 033 Acenaphthylene ND 10 033 <br /> Acetochlor ND 1 0 033 Anthracene ND 10 033 <br /> Benzidine ND to 1 6 Benzoic Acid ND 10 16 <br /> Benzo(a)anthracene ND 1 0 033 Benzo(b)fluoranthene ND 1 0 033 <br /> Benzo(k)fluoranthene ND 1 0 033 Benzo(S,h,i)perylene ND 1 0 033 <br /> Benzo(a) yrene ND 1 0 033 Benzyl Alcohol ND 10 066 <br /> Bis(2-chloroethox Methane ND 1 0 033 Bis(2-chloroeth l)Ether ND 1 10 033 <br /> Bis 2-chloroiso ropyi)Ether ND 1 0 033 Bis 2-ethylhexyl Adipate ND 1 0 033 <br /> Bis(2�th lhcx 1)Phthalate ND 10 033 4-Bromo henyl Phenyl Ether ND 1 0 033 <br /> But ]be 1 Phthalate ND 1 0 033 4-Chloroaniline ND 1 0 066 <br /> Nitrobenzene ND l 10 16 4-Chloro-3-meth 1 henol ND 1 0 033 <br /> 2-Chlorona hthalene ND 1 0 033 2-Chlorophenol ND 10 033 <br /> 4-ChlorophenyI Phenyl Ether ND 1 0 033 Ch Bene ND 1 0 033 <br /> Dibenzo a,h anthracene ND 10 033 Dibenzofuran ND 10 033 <br /> Dt-n-but 1 Phthalate ND 1 0 033 1,2-Dichlorobenzene ND 1 0 033 <br /> 1,3-Dichlorobenzene ND 10 033 1,4-Dichlorobenzene ND 1 0 033 <br /> 3 3-Dichlorobenzidine ND 1 0 066 2 4-Dichloro henol ND 1 0 033 <br /> Diethyl Phthalate ND 1 0 033 2,4-Dimethy]phenol ND 1 0 1 033 <br /> Dimethyl Phthalate ND 1 0 033 4,6-Dmitro-2-meth l henol ND 1 0 1 6 <br /> 2,4-Dmitro henol ND 10 16 2,4-Dmitrotoluene ND 10 033 <br /> 2,6-Dinitrotoluene ND 1 0 033 Dl-n-oct 1 Phthalate ND 1 0 033 <br /> 1,2-Di hen lhydrazine ND l 0 033 Fluoranthene ND 1 0 033 <br /> Fluorene ND 10 033 Hexachlorobenzene ND —10 -033 <br /> Hexachlorobutadiene ND 10 033 Hexachloroc clo entadiene ND 10 16 <br /> Hexachloroethane ND 140 0 33 Indeno 1,2 3-cd ne ND i 0 033 <br /> Iso horone ND 033 2-Meth ina hthalene ND 1 0 033 <br /> 2-Meth 1 henol(o-Cresol) ND 033 3&/or 4-Meth I henol(m -Cresol) ND l 0 033 <br /> Na hthalene ND 0 33 2-Nitroaniline ND 1 0 16 <br /> 3-Nitroamlme ND 10 16 4-Nitroantline ND 10 16 <br /> 2-Nitrophenol ND 10 1 6 4-Nitrophenol ND 10 033 <br /> N-Nitrosodi hen iamme ND 10 033 N-Nitrosodi-n-propylamLne ND to 0 33 <br /> Pentachlorophenol ND 10 16 1 Phenanthrene ND J. 0 033 <br /> Phenol ND 10 033 Pyrene ND 10 033 <br /> 1 2 4-Tnchlorobenzene ND 10 033 2,4,5-Tnchloro henol ND 1 0 033 <br /> 2 4 6-Tnchlorohenol ND 10 033 <br /> Surrogate Recoveries(%) <br /> %SS 1 842 %SS2 858 <br /> %SS3 974 %SS4 881 <br /> %SS5 886 %SS6 839 <br /> Comments <br /> *water samples and all TCLP&SPLP extracts are reported in gg/L,soil/sludge/solid samples in mglkg,wipe samples in gg/wipe,product/otl/non- <br /> aqueous liquid samples in mg/L <br /> ND means not detected above the reporting limit,NIA means analyte not applicable to this analysis <br /> #)surrogate diluted out of range,&)low or no surrogate due to matnx interference <br /> h)lighter than water immiscible sheen/product is present,i)liquid sample that contains greater than—2 vol %sediment,j)sample diluted due to high <br /> organic content,k)reporting limit raised,benzoic acid found to LCSILCSD samples Benzoic acid found in the method blank at a detectable <br /> concentration but under the RL for this compound <br /> DHS Certification No 1644 Angela Rydehus, Lab Manager <br />