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McCampbell Analytical, Inc. 110 2nd 925 798-16 Pacheco CA 98 1622560 <br /> Telephone 925 798-]fi20 Fax 925-798 1622 <br /> -Website www=campbcll coin E mail main@rnccarnpbell corn- - _- I <br /> I <br /> Advanced GeoEnvironmental,Inc Client Project ID Flag City Chevron Date Sampled 01/20/04-01/22/04 <br /> 837 Shaw Road Date Received 01/23/04 <br /> Client Contact Tun Cuellar Date Extracted 01/23/04 <br /> Stockton,CA 95215 <br /> Client P O Date Analyzed 01/24/04-01/28/04 <br /> Seini-Volatile Organics by GC/MS(Banc Target List)* <br /> Extraction Method SW3550C Analytical Method SW8270D WDrk Order 0401260 <br /> Lab ID 0401260-025A <br /> Li�7 Client ID - P43-30' <br /> Matrix Soil <br /> mg <br /> Compound I Concentration * DF R`p0m s Compound Concentration* DF x LLmmut <br /> Acena hthene ND 1 0 033 Acenaphthylene ND 1 0 T-033 <br /> Acetochlor ND 1 0 033 Anthracene ND 1 0 033 <br /> Senzidine ND 1 0 1 6 Benzoic Acid ND 1 0 1 6 <br /> Benzo(a)anthracene ND 1 0 033 Benzo(b)fluotanthene ND 1 0 033 <br /> Benzo(k)fluoranthene ND 10 033 Benzo( ,h,i)perXlene ND 1 0 033 <br /> Benzo(a)pyrene ND 10 033 Benzyl Alcohol ND 1 0 066 <br /> Bis(2-chloroethox Methane ND 1 0 033 Bis(2-chloroeth 1)Ether ND 1 0 033 <br /> Bis 2-chlomiso rap 1)Ether ND 1 0 033 Bis(2-eth lhex 1)Adipate ND 1 0 033 <br /> Bis 2-ethylhex l Phthalate ND 1 0 1 033 4-Bromophenyl Phenyl Ether ND 1 0 033 <br /> Butylbenz 1 Phthalate ND 1 0 033 4-Chloroanilme ND 1 0 066 <br /> Nitrobenzene ND 10 1 6 4-Chloro-3-meth l henol ND 1 0 033 <br /> 2-Chlorona hthalene ND 10 033 2-Chlorophenol ND 1 0 033 <br /> 4-Chlorophe_n 1 Phenyl Ether ND 10 033 Chrysene ND 1 0 033 <br /> Dibenzo(a h)anthracene ND 1 0 033 Dibenzofuran ND 1 0 033 <br /> Di-n-but 1 Phthalate ND 1 0 033 1,2-Dichlorobenzene ND 1 0 033 <br /> 1 3-Dichlorobenzene ND 10 033 1,4-Dichlorobenzene ND 10 033 <br /> . 3,3-Dichlorobenzidme ND 10 066 2,4-Dichloro henoi ND 10 033 <br /> Diethyl Phthalate ND I 10 033 2,4-1)imethylphenol I ND 1 0 033 <br /> Dimethyl Phthalate ND 10 033 4,6-Dmitro-2-meth ]phenol ND 1 0 16 <br /> 2,4-Dmitro henoi ND 10 1 6 2,4-Dmrtrotoluene ND 1 0 033 <br /> 2,6-Dinitrotoluene ND 1 0 033 Di-n-oct 1 Phthalate ND 1 0 033 <br /> l,2-Di hen Eh drazme ND 1 0 033 Fluoranthene ND 1 0 033 <br /> Fluorene ND 10 033 Hexachlorobenzene ND 1 0 033 <br /> Hexachlorobutadtene ND 1 0 033 Hexachloroc clo entadiene ND 1 0 16 <br /> Hexachloroethane ND 1 0 033 Indeno 1,2,3 d ne ND 1 0 033 <br /> Iso horone ND 1 0 033 2-Methylnaphthalene ND 1 0 033 <br /> 2-Meth i henol(o-Cresol) ND 10 033 3&lar 4-Meth l henoi(m, -Cresol) ND 1 0 033 <br /> Naphthalene ND to 033 2-Nitroaniltne ND 1 0 1 6 <br /> 3-Nitroarulme ND 10 1 16 4-Nitroantline ND l0 16 <br /> 2-Nitrophenol ND 1 0 16 4-Nitrophenol ND 1 0 033 <br /> N-Nitrosodt hen lamme ND 1 0 033 N-Nitrosodi-n-propXlamme ND 1 0 033 <br /> Pentachlorophenol ND 10 1 6 Phenanthrene ND 1 0 033 <br /> Phenol ND 10 0 33 ene ND 10 0 33 <br /> 1,2 4-Trtchlorobenzene ND 10 033 2,4,5-Trichlorophenol ND 1 0 0 33 <br /> 2 4 6-Tnchloro henoi ND 10 033 <br /> Surrogate Recoveries <br /> %SSI 107 %SS2 927 <br /> %SS3 929 %SS4 983 <br /> %SS5 81 1 %SS6 106 <br /> Comments <br /> •water samples and all TCLP&SPLP extracts are reported inµg/L,soilisludgelsolid samples in mg/kg,wipe samples inµg/wipe,product/oitinon- <br /> aqueous liquid samples in mg/L <br /> ND means not detected above the reporting limit,NIA means analyte not applicable to this analysis <br /> #)surrogate diluted out of range,&)low or no surrogate due to matrix interference <br /> h)lighter than water immiscible sheen/product is present,i)liquid sample that contains greater than--2 vol %sediment,j)sample diluted due to high <br /> organic content,k)reporting limit raised,benzoic acid found in LCS/LCSD samples Benzoic acid found in the method blank at a detectable <br /> concentration but under the RL for this compound <br /> DHS Certification No 1644 Angela Rydehus, Lab Manager <br /> r <br />