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110 2nd Avenue South,ND7,Pacheco,CA 94553 5560 <br /> Inc.McCampbell Analytical, ITelephone 925-798-1620 Fax 925 798 1622 <br /> --� -— > _ - -- - -- -- _--—T-- - — --=--Website www McCampbell Loin E-mall maui(a mccarWbel]Loin - <br /> Advanced GeoEnvironmental,Inc Client Protect ID Flag City Chevron Date Sampled 01/20/04-01/22/04 <br /> 837 Shave Road Date Received 01/23/04 <br /> Client Contact Tim Cuellar Date Extracted 01/23/04 <br /> Stockton,CA 95215 1 1 - <br /> Client P O Date Analyzed 01124104-01/28/04 <br /> Semi-Volatile Organics by GC/MS(Basic Target List)* <br /> Extraction Method SW3550C Analytical Method SW8270D Work Order 0401260 <br /> Lab ID 0401260-026A <br /> Client ID P43-45' <br /> Matrix Soil <br /> Compound Concentration* DF R��ms Compound Concentration " DF R`Lmcia <br /> Acenaphthene ND l 0 033 Acenaphthylene ND 10 033 <br /> Acetochlor ND 1 0 033 Anthracene ND 1 0 033 <br /> Benzidine ND 10 16 Benzoic Acid ND 1 0 1 6 <br /> Benzo(a)anthracene ND 10 033 Benzo fluoranthene ND 1 0 033 <br /> Benzo(k)fluoranthene ND 1 0 033 Benzo(g,h,i)pSrylcne ND 1 0 033 <br /> Benzo(a)pyreiic ND 1 0 033 Ben 1 Alcohol ND 10 066 <br /> Bis 2-chloroethox Methane ND 1 0 033 Bis 2-chloroethyl)Ether ND 10 033 <br /> Bis(2-chloroiso ro1)Ether ND 1 0 033 Bis(2-eth Ihex I Adipate ND 1 0 033 - <br /> Brs(2-eth lhex 1)Phthalate ND 1 0 033 4-Bromo hen 1 Phenyl Ether ND 1 0 033 <br /> Bu!ylbcnzyi Phthalate ND l 0 033 4-Chloroanilme ND 1 0 066 <br /> Nitrobenzene ND 10 16 4-Chloro-3-methylphenol ND 1 0 033 <br /> 2-Chlorona hthalene ND 1 0 033 2-Chlorophenol ND 1 0 033 <br /> 4-Chloro hen 1 Phenyl Ether ND 10 033 Chrysene ND 1 0 —033 <br /> Dibenzo(a h)anthracene ND 10 033 Dibenzofuran ND E to 033 <br /> Di-n-butyl Phthalate ND 1 0 033 1 2-Dichlorobcn2ene ND 10 033 <br /> 1,3-Dichlorobenzene ND 1 0 033 1,4-Dichlorobenzene ND 1 0 033 <br /> • 3,3-Dichlorobenzidme ND 10 066 2 4-Dichlorohenol ND 1 0 033 <br /> Diethyl Phthalate ND 10 0 33 2,4-Dimethylphenol ND 1 0 —033 <br /> Dimethyl Phthalate ND 10 033 4,6-Dinitro-2-meth 1 henol ND 10 1 6 <br /> 2,4-Dmitro henol ND 10 16 2,4-Dmrtrotoluene ND 10 o33 <br /> 2,6-Dmitrotoluene ND Elo <br /> 033 Di-n-0c 1 Phthalate ! ND 1 0 033 <br /> 1,2-Di henylh drazine ND 033 Fluoranthene ND 1 0 033 <br /> Fiuorene ND 10 0 33 Hexachlorobenzene I ND 1 0 033 <br /> Hexachlorobutadiene ND 10 1 033 Hexachloroclo entadiene ND 1 0 16 <br /> Hexachloroethane ND --1-0-7-033 Indeno 1,2,3-cdpyrene ND 1 0 033 - <br /> Iso horone ND 1 0 033 2-Methylnaphthalene ND 1 0 033 <br /> 2-Meth 1 henol(o-Cresol) ND 10 033 3 Wor 4-Meth I henol m, -Cresol) ND 10 033 <br /> Naphthalene ND 1 0 033 2-Nitroanilme ND 1 0 16 <br /> 3-Nitroanilme ND 10 16 4-Nitroamlme ND 10 16 <br /> 2-Nitrophenol ND 10 16 4-Nitrohenol ND 1 0 033 <br /> N-Nitrosodr hen lamine ND 10 0 33 N-Nitrosadi-n-pTpylarnine ND 1 0 033 <br /> Pentachlorophenol ND 10 1 1 6 Phenanthrene ND 1 0 033 <br /> Phenol ND 10 033 ne ND 1 0 033 <br /> 1,2,4-Tnchlorobenzene ND 10 033 2,4,5-Trichlorophenol ND 1 0 033 <br /> 2.4,6-Trichlorophenol ND 10 033 <br /> Surrogate Recoveries(%) <br /> %SSI 93 2 %SS2 863 <br /> %SS3 83 2 %SS4 83 7 <br /> %SS5 80 6 %SS6 909 <br /> Comments <br /> "water samples and all TCLP&SPLP extracts are reported in pg/1L soil/sludge/solid samples in mg/kg,wipe samples inµg/wipc,product/oil/non- <br /> aqueous liquid samples in mg/L <br /> ND means not detected above the reporting limit,NIA means analyte not applicable to this analysis <br /> #)surrogate diluted out of range,&)low or no surrogate due to matrix interference <br /> h)lighter than water immiscible sheen/product is present,i)liquid sample that contains greater than-2 vol %sediment,j)sample diluted due to high <br /> organic content,k)reporting limit raised,benzoic acid found m LCS/LCSD samples Benzoic acid found in the method blank at a detectable <br /> concentration but under the RL for this compound <br /> DHS Certification No 1644 Angela Rydehus, Lab Manager <br />