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1 io 2nd Avenue South #137 Pacheco,CA 94553 5560 <br /> McCampbell Analytical, Inc. Telephone 925 798-1620 Fax 925-798-1622 <br /> Website www niccampbell com E mail main®mecaii>Qbell coin <br /> Advanced GeoEnvirownental, Inc Client Project ID Flag City Chevron Date Sampled 01/20/04-01/22104 <br /> n <br /> Date Received 01/23/04 <br /> 837 Shaw Road <br /> Client Contact Tum Cuellar Date Extracted 01/23/04-01/26/04 <br /> Stockton, CA 95215 Client P O 1 Date Analyzed 01/23/04-01/26/04 <br /> Oxygenated Volatile Organics+EDB and 1,2-DCA by P&T and CC/MS* <br /> Extraction Method SW5030B Analytical Method SW8260B Work Order 0401260 <br /> Lab ID 0401260-017A 0401260-018A 0401260-019A ! 0401260-020A _ <br /> Client ID P41-15' P41-30' P41-45' P42-10* Reporting Limit for <br /> Matrix S S S S DF=1 <br /> I � <br /> Compound Concentration pg/Kg lig/L <br /> T tert-Amyl methyl ether(TAME) ND ND ND' ND ' so 05 <br /> t-Butyl alcohol( BA) ND ND ND ND 25 50 <br /> 12-Dibromoethane(EDB) ND ND ND ND 50 05 <br /> 1,2-Dichloroethane(1,2-DCA) ND ND ND ND 50 05 <br /> Dusopropyl ether(DIPS) ND ND ND ND 50 05 <br /> Ethyl tert-butyl ether(ETBE) ND ND ND ND 50 05 <br /> Methyl-t-butyl ether(MTBE) ND 52 I ND ND 5 0 05 <br /> Surrogate Recoveries(%) <br /> %SS =94$ 944 952 975 <br /> Comments <br /> *water and vapor samples and all TCLP&SPLP extracts are reported in}ig/L,soil/sludge/solid samples inµg/kg, wipe samples in lig/wipe, <br /> product/oil/non-aqueous liquid samples in mg/L <br /> ND means not detected above the reporting limit N/A means analyte not applicable to this analysis <br /> #surrogate diluted out of range or surrogate coelutes with another peak <br /> h)lighter than water immiscible sheen/product is present,i)liquid sample that contains greater than--2 vol %sediment,l)sample diluted due to high <br /> organic content <br /> t <br /> 1. <br /> DHS Certification No 1644 'Angela Rydelius, Lab Manager <br />