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'� _ 110 2nd Avenue South #D7 Pacheco CA 94553-5560 <br /> 4 <br /> McCampbell Analytical, Inc. Telephone 925.798.1620 Fax 925 798-1622 <br /> Website www mccampbell corn E-mail mom@nx campbel!com <br /> Advanced GeoEnviromnental, Inc Client Project ID FIag City Chevron Date Sampled 01/20/04-01122/04 <br /> 837 Shaw Road Date Received 01/23/04 <br /> Client Contact Tim Cuellar Date Extracted 01123104-01/26/04 <br /> Stockton,CA 95215 <br /> Client P O 1 Date Analyzed 01123/04-01/26/04 <br /> Oxygenated Volatile Organics+EDB and 1,2-DCA by P&T and GC/MS* <br /> Extraction Method SW503oB Analytical Method SW8260B Work Order 0401260 <br /> Lab ID 0401260-0090 0401260-OIOC ! 0401260-011 C i 0401260-012C <br /> 3 <br /> Client ID P39-47to51 P43-13to18 ( P43-37to41 P4347to51 Reporting Limit for <br /> Matrix W W W W DF=1 <br /> DF .._.__� 1 __— ---—25 -------- 10 ---- -- - -_1 S W <br /> I <br /> Compound Concentration µg/Kg 1ig/L <br /> tert-Amyl methyl ether(TAME)- ND ND<12 ND<5 0 ND 5 0 0 5 <br /> t-Butyl alcohol(TBA) ND ND<120 ND<50 13 25 5 0 <br /> 1 2-Dibromoethane(EDB) ND ND<12 ND<5 0 ND so 05 <br /> 1,2-Dichloroethane(1,2-DCA) ND ND<12 ND<5 0 ND so 0 5 <br /> • Dusopropyl ether(DIPE) ND ND<12 ND<5 0 ND 5 0 0 5 <br /> Ethyl tert-butyl ether(ETBE) ND ND<12 ND<5 0 ND 5 0 05 <br /> Methyl-t-butyl ether(MTBE) 065 540 210 32 5 0 0 5 <br /> Surrogate Recoveries (%) <br /> %SS 104 93 9 960 102 <br /> Comments <br /> *water and vapor samples and all TCLP&SPLP extracts are reported in pg/L,soillsludge/sohd samples in liglkg, wipe samples in pg/wipe, <br /> product/oil/non-aqueous liquid samples in mg/L <br /> ND means not detected above the reporting limit,NIA means analyte not applicable to this analysis <br /> #surrogate diluted out of range or surrogate coelutes with another peak <br /> Ih)lighter than water immiscible sheen/product is present,i)liquid sample that contains greater than—2 vol %sediment,l)sample diluted due to high <br /> or avec content <br /> •� I <br /> DHS Certification No 1644 4Angela Rydehus,Lab Manager <br />