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110 2nd Avenue South,4137 Pacheco CA 94$53-5560 <br /> Inc.McCampbell Analytical, Telephone 925-798-1620 Fax 925-798-1622 <br /> _ A_ ___ _ _ _-_ - =_Webgne www inccampbell corn Email mam@mccampbell coni,_ <br /> Advanced GeoEnvironmental, Inc Client Project ID Flag City Chevron Date Sampled 01/20104-01122104 <br /> • 837 Shaw Road Date Received 01/23/04 <br /> Stockton, CA 95215 <br /> Client Contact Tint Cuellar Date Extracted 01/23/04 <br /> Client P O Date Analyzed 01124104-01128/04 <br /> Sena-Volatile Organics by GC/MS(Basic Target List)* ` <br /> Extraction Method SW3510C Analytical Method SW8270D Work Order 0401260 <br /> Lab M 0401260-002D <br /> Client 1D _ - - - P41-37to41 - -- <br /> Matrix Water <br /> RcporCompound Concentration * DF Lunft`g Compound Concentration * DF Repovnmg <br /> Acenaphthene ND 10 10 Acenaphthylene ND 1 0 10 <br /> Anthracene ND 10 10 Benzidine ND 10 50 <br /> Benzoic Acid ND 1 0 50 Benzo(a)anthracene ND to 10 <br /> Benzo(b)fluoranthene ND 1 0 10 Benzo(k)fluoranthene ND to 10 <br /> Benzo{ ,h,r} a lene ND 1 0 10 Benzo(a)pyrene ND 10 10 <br /> Ben I Alcohol ND 1 0 I 20 His 2-chloroethox )Methane ND l 0 10 <br /> Bis(2-chloroeth1)Ether ND 1 0 10 Bis 2-chloroiso ro 1)Ether ND 1 0 to <br /> Bis(2-eth /hex l)Phthalate ND 1 0 ' 10 4-13romo hen 1 Phenyl Ether ND 1 0 io <br /> l3utylbetizyt Phthalate ND 11 0 10 4-Chloroanilme ND 10 20 <br /> 4-Chloro-3-meth (phenol ND t 0 10 2-Chlorona hthalene ND 10 10 <br /> 2-Chloro henot ND 1 0 10 4-Chlorophen 1 Phenyl Ether ND 10 10 <br /> Ch serve ND 1 0 10 1 Dibenzo(a h)anthracene ND 1 0 10 <br /> Dibenzofuran ND 1 0 10 I Di-n-butyl Phthalate I ND I I 0 l0 <br /> 1 2-Dichlorobenzene ND 1 0 10 1,3-Dichlorobenzene ND I to 10 <br /> 1,4-Dichlorobenzene ND 10 to 3,3-Dichlorobenzidme ND l0 20 <br /> 2,4-Dtchloro henol ND 1 0 10 Diethyl Phthalate ND l 0 10 <br /> • <br /> 2,4-Dimethylphenol ND 1 0 10 Dimethyl Phthalate ND 1 0 l0 <br /> 4 6-Dmitro-2-meth l henol ND 1 0 50 2,4-Dmitro lien] ND 1 0 50 <br /> 2 4-Dinitrotoluene ND 1 0 10 2,6-Dmrtrotoluene ND l 0 10 <br /> Di-n-octyl Phthalate ND 1 0 10 1,2-Dlphenylhydrazme ND 10 10 <br /> Fluoranthene ND 10 10 Fluorene ND 10 l0 <br /> Hexachlorobenzene ND 1 0 10 Hexachlorobutadiene ND t 0 I 10 <br /> Hexachloroc clo entadrene ND 1 0 50 Hexachloroethane ND 1 0 10 <br /> lndeno 1,2,3-cdpyrene ND 1 0 10 Iso horone ND I to 10 <br /> 2-Methy1na hthalene ND 1 0 10 2-Meth (phenol(o-Cresol) ND —10 J —10 r <br /> 3 Wor4-Methylphenol m, -Cresol) ND —10 10 Naphthalene ND to I 10 <br /> 2-Nitroantlme ND 10 50 3-Nitroanilme ND10 50 <br /> 4-Nitroantline ND 10 50 Nitrobenzene ND 50 <br /> 2-Nitrophenol ND 10 50 4-Nitrophenol ND :41 <br /> 10 <br /> N-Nitrosodi hen lamme I ND to 10 N-Nitrosodi-n- ro lamme ND 1 0 I 10 <br /> Pentachlorophenol ND I 1 0 50 Phenanthrene ND to 10 <br /> Phenol ND 10 10 Pyrene ND <br /> I lo 10 <br /> 1,2,4-Trichlorobenzene ND to 10 2,4 5-Trichlorophenol ND to 10 <br /> 2 4 6-Tnchlaro hcnol ND 1 0 10 <br /> Surrogate Recoveries(%) <br /> %SSI 949 0/.SS2 i 90 l <br /> %SS3 861 %SS4 820 <br /> %SS5 777 %SS6 81 3 <br /> Comments i <br /> 'water samples and all TCLP&SPLP extracts are reported inµglL,soil/sludge/solid samples in mg/kg wipe samples inµg/wipe,productloil/non- <br /> aqueous liquid samples in mg/L. <br /> ND means not detected above the reporting limit,N/A means analyte not applicable to this analysts <br /> #)surrogate diluted out of range,&)low or no surrogate due to matrix interference <br /> h)lighter than water immiscible sheentproduct is present,i)liquid sample that contains greater than--2 vol %sediment,))sample diluted due to high <br /> organic content,k)reporting limit raised,benzoic acid found in LCSILCSD samples Benzoic acid found in the method blank at a detectable <br /> concentration but under the RL for this compound <br /> DHS Certification No 1644 "'-*y/ y-)6gela Rydehus, Lab Manager <br />