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110 2nd Avenue South #D7 Pacheco CA 94553 5560 <br /> McCampbell Analytical, Inc. Telephone 925-798 1620 Fax 925 798 1622 <br /> �-*— _ __ �� _- _—— _ - _ _ _ =Weh$de www rmcampbell com E-mail mainr@mccampbell com__. <br /> Advanced GeoEnvironmental,Inc Client Project ID Flag City Chevron Date Sampled 01/20/04-01/22104 <br /> 837 Shaw Road Date Received 01/23/04 <br /> Client Contact Tim Cuellar Date Extracted 01/23/04 <br /> Stockton,CA 95215 <br /> Client P O Date Analyzed 01/24/04-01128104 <br /> Semi-Volatile Organics by GC/MS(Basic Target List)* <br /> 7E%t=ra-1i--M7.1hod SW3510C Analytical Method SW8270D Work Order 0401260 <br /> Lab ID 0401260-003D <br /> Client ID P42-1 1to16 <br /> Matrix Water <br /> Compound Concentration* DF Re <br /> DF Compound Concentration* DF >z L`�,M1 s <br /> Acenaphthene ND l 0 10 Acenaphth lene ND 1 0 I 10 <br /> Anthracene ND 10 10 Benzidine ND 10 50 <br /> Benzoic Acid ND 1 0 50 Benzo(a)anthracene ND 1 0 10 <br /> Benzo Atio-rithene ND 10 I0 Benzo fluoranthene ND 10 10 <br /> Benzo h,0prrylene ND 1 0 10 Bcnzo(a)pyrene ND 1 0 10 <br /> Benzyl Alcohol �� ND 1 0 20 Bis(2-chloroethox Methane ND l 0 10 <br /> Bis(2-chloroeth 1)Ether ND 1 0 10 Bis 2-chloroiso ro t)Ether ND I 0 to <br /> Bis 2-ethylhexyl Phthalate ND 1 0 10 4-Bromophen l Phenyl Ether ND 1 0 10 u <br /> Butylbenz t Phthalate ND 1 0 10 4-Chloroaniline ND 1 0 20 <br /> 4-Chloro-3-methylphenol ND 1 0 10 2-Chlorona hthalene ND 1 0 l0 <br /> 2-Chlorophenol ND 1 0 10 4-Chloro hen l Phenyl Ether ND 1 0 10 <br /> Clisone ND 1 0 10 Dibenzo a,h anthracene { ND t 0 10 <br /> Dibenzofuran ND 1 0 10 Dt-n-but I Phthalate ND 1 0 t0 <br /> 1,2-Dichlorobenzene ND 10 10 1,3-Dichlorobenzene ND 10 10 <br /> 14-Dichlorobenzene ND 1 0 10 3,3-Dichlorobenzidme ND t 0 20 <br /> 2,4-Dichloro henol ND 1 0 10 Diethyl Phthalate ND 1 0 10 <br /> 2,4-Dimethylphenol ND I 0 10 Dimethyl Phthalate N❑ l 0 10 <br /> 4 6-Dtnitro-2-meth [phenol I ND 1 0 50 2,4-Dmitro henol ND l 0 50 <br /> 2,4-Dmitrotoluene ND l0 10 2,6-Dimtrotolilene ND 10 10 <br /> Di-n-octyl Phthalate ND 1 0 10 1,2-Dt hen lhydrazine ND 1 0 10 <br /> F'luoranthene ND 10 10 Fluorene ND 10 10 <br /> Hexachlorobenzene ND 10 10 Hexachlorobutadiene ND 10 10 <br /> Hexachloroc clo entadiene ND 1 0 50 Hexachioroethane ND 1 0 1 10 <br /> lndeno(1,2,3-cd)p) ene ND 1 0 10 Isopborone ND 1 0 1 10 <br /> 2-Meth ina hthalene ND 1 0 10 2-Meth 1 henol(o-Cresol) ND 1 0 10 _ <br /> 3 Wor 4-Meth 1 henol(m, -Cresol) ND 10 10 Naphthalene ND 1 0 10 <br /> 2-Nitroaniline ND 10 50 3-Nitroaniline ND 10 50 <br /> 4-Nitroanilme ND 10 50 Nitrobenzene ND 10 50 <br /> 2-Nitro henol ND 1 0 50 4-Nitrophenol ND 1 0 10 <br /> N-Nitrosodt hen [amine ND 1 0 10 N-Nitrosodi-n- rolamme ND —LL-1 10 <br /> Pentachlorophenol ND 1 0 50 Phenanthrene ND 1 0 10 <br /> Phenol ND 10 10 Pyrene ND 10 10 <br /> 1 2,4-Trichlorobenzene ND 1 0 10 2,4 5-Tnchloro henol ND 1 0 10 <br /> 2 4 6-Tnchloro henol ND 1 0 10 <br /> Surrogate Recoveries(%) <br /> %SSI 842 %SS2 85 1 <br /> %SS3 73 9 %SS4 420 <br /> %SS5 787 %SS6 797 <br /> Comments i <br /> *water samples and all TCLP&SPLP extracts are reported inµg/L,soil/sludgeisolid samples in mg/kg,wipe samples in gg/wipe,product/oil/non- <br /> aqueous liquid samples in mg/L <br /> ND means not detected above the reporting limit.NIA means analyte not applicable to this analysis <br /> #)surrogate diluted out of range,&)low or no surrogate due to matrix interference <br /> h)lighter than water immiscible sheeniproduct is present,i)liquid sample that contains greater than—2 vol %sediment,I)sample diluted due to high <br /> organic content,k)reporting limit raised,benzoic acid found in LCSILCSD samples Benzoic acid found in the method blank at a detectable <br /> concentration but under the RL for this com ound <br /> DHS Certification No 1644 C W►WW'yr/Angela Rydelius,Lab Manager <br />