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110 2nd Avenue South,#D7,Pacheco CA 94553-5560 McCampbell Analytical, Inc. Tclepbane 925-798-1620 Fax 925-798-1622 —Website www mccampbell cam E inial mamamccampbell come..--w Advanced GeoEnvironmental, Inc Client Project ID Flag City Chevron Date Sampled 01/20/04-01/22/04 . 837 Shaw Road Date Received 01/23/04 Client Contact Tun Cuellar Date Extracted 01/23/04 Stockton,CA 95215 Client P O Date Analyzed 01/24/04-01/28104 Semi-Volatile Organics by GC/MS(Basic Target List)* Extraction Method SW3510C Analytical Method SW9270D Work Order 0401260 Lab ID 0401260-006D 1 - - Client ID - - _ -P40A-47to513- Matrix Water Compound ing Concentration " DF x��s Compound Concentration* DF x`Lmut Arena hthene ND 1 0 10 Acenaphthylene ND 10 10 Anthracene ND 10 10 Benzidine ND 10 50 Benzoic Acid ND l 0 50 Benzo(a)anthracene ND 1 0 10 Benzo(b)fluoranthene ND 10 10 Benzo(k)fluoranthene ND 1 0 10 Benzo( ,h,t)pe!ylene ND 1 0 10 Benzo(a)pyene ND 1 0 10 Ben I Alcohol ND 1 0 20 Bts 2-chloroethox Methane ND to 10 Bis 2-chloroeth l)Ether ND 1 0 10 Bis(2-chloroiso rop 1)Ether ND l 0 10 Bis 2-eth lhex l)Phthalate I ND j 1 0 10 4-Brono hen 1 Phenyl Ether ND l 0 10 Butylbenz.yl Phthalate ND 1 0 10 4-Chloroanilme ND l 0 20 4-Chloro-3-meth 1 henoi ND l 0 10 2-Chlorona hthalene ND 1 0 10 2-Chlorophenol ND 1 0 10 4-Chloro hen l Phenyl Ether ND lo _ 10 Chrysane ND 10 10 Dlben70(a,h)anthracene ND 1 0 10 Dibenzofuran ND 1 0 10 Di-n-but 1 Phthalate ND 1 0 10 1,2-Dichlorobenzene ND 10 10 1,3-Dichlorobenzene ND 10 10 1 4-Dichlorobenzene ND i 0 10 3 3-Dichlorobenzidme ND 10 20 2,4-Dichlorohenol ND I 0 10 Diethyl Phthalate ND 1 0 10 2,4-Dimethylphenol.. ND 10 10 Dimethyl Phthalate ND l 0 10 4,6-Dinitro-2-methyE henol ND 10 50 2 4-Dmrtro henal ND 1 0 50 2,4-Dinitrotoluene ND 10 10 2,6-Dimtrotoluene ND 10 10 -Di-n-octyl Phthalate ND 10 10 1,2-Di hen 1hydramne ND 10 10 Fluoranthene ND 10 10 Fluorene ND 10 10 Hexachlorobenzene ND 10 10 Hexachlorobutadiene ND 10 10 Hexachlorocyclopentadiene ND 10 50 1 Hexachloroethane ND 10 10 Indeno 1,2,3-cd)pyrene ND I to 10 Iso horone ND to 10 2-Methylnaphthalene ND 10 10 2-Meth 1 henol(o-Cresol) ND 1 0 10 J 3&/or 4-Meth 1 henol m -Cresol) ND 10 10 Naphthalene ND l 0 10 2-Nitroanilme ND 10 50 3-Nltroamline ND 10 50 4-Nitroamline ND 10 50 Nitrobenzene ND 10 50 2-Nitrophenol ND 10 50 4-Nttro henol ND 1 0 10 N-Nitrosodi hen lamme ND 10 10 N-Nitrosodi-n- ro lamine ND 1 0 10 Pentachlorophenol ND 101 Phenanthrene ND 1-0 10 Phenol ND 10 10 Pyrene ND 10 10 1,24-Tnehlorobenzene ND E 0 10 2,4,5-Trichlorophenol ND 10 10 2 4 6-Trichlory henol ND l 0 10 Surrogate Recoveries(%) %SSI 921 %SS2 88 8 %SS3 86 7 %SS4 84 7 %SS5 81 5 %SS6 812 Comments t *water samples and all TCLP&SPLP extracts are reported in pg/L soil/sludge/solid samples in mg/kg,wipe samples in ltg/wipe product/oil/non- aqueous liquid samples in mg/L ND means not detected above the reporting limit N/A means analyte not applicable to this analysis #)surrogate diluted out of range,&)law or no surrogate due to matrix interference h)lighter than water immiscible sheen/product is present,i)liquid sample that contains greater than—2 vol %sediment,l)sample diluted due to high organic content,k)reporting limit raised,benzoic acid found in LCS/LCSD samples Benzoic acid found in the method blank at a detectable concentration but under the RL for this compound DHS Certification No 1644 Angela Rydehus, Lab Manager