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1 l0 2nd Avenue South,#137,Pacheco CA 94553-5560 <br /> McCampbell Analytical, Inc. Telephone 925-798-1620 Fax 925-798-1622 <br /> Websue www mecampbellconn-E-mad main@mccampbellcont <br /> Advanced GeoEnvironmental,Inc Client Project ID Flag City Chevron Date Sampled 01/20/04-01122104 <br /> . 837 Shaw Road Date Received 01/23/04 <br /> Client Contact Tim Cuellar Date Extracted 01/23/04 <br /> Stockton„CA 95215 <br /> Client P O Date Analyzed 01/24104-01128104 <br /> Sean-Volatile Organics by GC/MS(Bask Target List)* <br /> Extraction Method SW3510C Analytical Method SW8270D Work Order 0401260 <br /> Lab ID 0401260-005D <br /> _ = Client ID - P40A-14to19 - - - <br /> Matrix Water <br /> Compound Concentration * DF R`port�'s Compound Concentration * D#~ R g <br /> Acena htht,ne ND 1 0 10 Acenaphthylene ND 1 0 i0 <br /> Anthracene ND I0 10 Benzidine ND 10 50 <br /> Benzoic Acid ND 1 0 50 Benzo(a)anthracene ND 10 to <br /> Benzo(b)fluoranthene ND 10 10 Benzo k)tluotailthene ND 10 l0 <br /> Benzo(g,h,i)perylene ND 1 0 10 Benzo a ene ND 1 0 10 <br /> Benzyl Alcohol ND 1 0 20 Bis(2-chloroetli2x Methane ND 1 0 10 <br /> Bis(2-chloroeth 1)Ether ND I 1 0 10 Bis 2-chlorotso ro I)Ether ND 1 0 10 <br /> Bis(2-ethylhex 1 Phthalate - ND I 0 10 4-Broma hen ]Phenyl Ether ND 1 0 10 <br /> Butylben 1 Phthalate ND 1 0 10 4-Chloroanilme ND 10 20 <br /> 4-Chloro-3-meth 1phenol ND 1 0 10 2-Chlorona hthalene ND 1 0 10 <br /> 2-Chlorophenol ND 1 0 IO 4-Chloro henyl 'henyl Ether ND 1 0 10 <br /> Chrysene ND 10 10 Dibenzo(a,h)anthracene ND l0 10 <br /> Dibenzofuran ND I 0 10 Di-n-butyl Phthalate ND 1 0 10 <br /> 1,2-Dichlorobenzene ND I O 10 1,3-Dichlorobenzene ND 10 l0 <br /> 1,4-Dichlorobenzene ND l0 10 3,3-Dichlorobenzidine ND 10 20 <br /> 2,4-Dichloro henol ND 1 0 10 Diethy]Phthalate ND 1 0 10 <br /> 2,4-Dimethyl phenol ND 1 0 10 Dimethyl Phthalate ND 10 10 <br /> 4,6-Dimtro-2-meth t henol ND 1 0 50 2,4-Dinitro henol ND 1 0 50 <br /> 2,4-Dmitrotoluene ND 10 10 2,6-Dmttrotoluene ND 10 ]0 <br /> Di-n-oct 1 Phthalate ND 10 10 1,2-Dr henylh drazine ND 10 10 <br /> Fluoranthene ND 10 10 Fluorene ND 10 10 <br /> Hexachlorobenzene ND 10 10 Hexachlorobutadiene ND i 10 10 <br /> Hexachloroc clo entadiene ND 1 0 50 flexachloroethane ND 1 0 l0 <br /> tndeno(1,2,3-ed)pyrene ND 1 0 10 Iso horone ND 10 10 <br /> 2-Meth lna hthalene ND 1 0 10 2-Methylphenol(o-Cresol) ND 10 t0 --- – <br /> 3&/or 4-Meth 1phenol m, -Cresol) ND 10 10 Naphthalene ND 1 0 10 <br /> 2-Nitroaniltne ND 1 0 50 3-Nitroaniline ND 10 50 <br /> 4-Nitroanilme ND 14 50 1 Nitrobenzene ND <br /> R ! 0 50 <br /> 2-Nitro henol ND l 0 50 1 -Nitrophenol ND 1-0 10 <br /> N-Nitrosodiphenylamine ND 1 0 10 N-Nitrosodi-n-pro ylamine ND 1 0 to <br /> — <br /> Peril henol ND 1 0 50 Phenanthrene ND 1 0 10 <br /> Phenol. ND 10 10 ene ND 10 10 <br /> 1,2,4-Trichlorobenzene ND 1 0 10 2,4,5-Trichloro henol ND 1 0 l0 <br /> 2 4 6-Tnchloro henol ND 1 0 l0 <br /> Surrogate Recoveries(%) <br /> %SS 1 91 7 %SS2 928 <br /> %SS3 875 %SS4 834 <br /> %SS5 940 %SS6 840 <br /> Comments i <br /> *water samples and all TCLP&SPLP extracts are reported in pg/L,soil/sludge/solid samples in mg/kg,wipe samples inµg/wtpe,productloil/non- <br /> aqueous liquid samples in mg/L <br /> ND means not detected above the reporting limit,NIA means analyte not applicable to this analysis <br /> #)surrogate diluted out of range &)low or no surrogate due to matnx interference <br /> . h)lighter than water immiscible sheeniproduct is present,t)liquid sample that contains greater than--2 vol %sediment,3)sample diluted due to high <br /> organic content,k)reporting limit raised,benzoic acid found in LCS/LCSD samples Benzoic acid found in the method blank at a detectable <br /> concentration but under the RL for this compound <br /> DHS Certification No 1644JIAngela Rydehus, Lab Manager <br />