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110 2nd Avenue South #D7 Pacheco CA 94553-5560 <br /> I <br /> McCampbcll Analytical, n C. Telephone 925-798 1620 Fax 925 798-1622 <br /> M- �;-- -24 -.„- —,-- - -___ -,- _ ,,- .- -Website wwwmccampbellcom Ismail main®inccampbellconi�- „ <br /> Advanced GeoEnvironmental, Inc Client Project ID Flag City Chevron Date Sampled 01/20/04-01/22/04 <br /> • 837 Shaw Road Date Received 01/23/04 <br /> Stockton,CA 95215 <br /> Chent Contact Tim Cuellar Date Extracted 01/23/04 <br /> CIient P O Date Analyzed 01/24104-01128104 <br /> Sema-Volatile Organics by GC/MS(Basic 1 arget List)* <br /> Extractinn Method Sw3510C Analytical Method SW8270D Work Order 0401260 <br /> Lab ID 0401260-008D <br /> -€ - - Client ID - P39-36to41 - - - - - - <br /> Matrix Water <br /> Compound Concentration* DF R`�°=t s Compound Concentration* DF R�l+s <br /> Acena hthenc ND 1 0 10 Acena hthylenc ND 1 0 10 <br /> Anthracene ND 10 10 Benzidine ND 10 50 <br /> Benzoic Acid ND l 0 50 Benzo a anthracene ND 10 10 <br /> Benzo b fluoranthene ND 1 0 10 Benzo(k)fluoranthene ND 10 10 <br /> Rcnzo(g,h,i)perylenc. ND 1 0 10 Benzo(a)pyrene ND 10 10 <br /> Ben 1 Alcohol ND ] 0 20 Bis(2-chioroethox Methane ND 10 10 <br /> Bis(2-chloroeth 1)Ether ND 1 0 101 Bis(2-chloroiso rop I)Ether ND to 10 <br /> Bis(2-eth /hex l)Phthalate ND 1 0 10 4-Bromophenyl Phony]Ether ND 10 10 -- <br /> Butylbenz 1 Phthalate ND l 0 10 4-Chioroanilme ND <br /> 10 20 <br /> 4-Chloro-3-mesh /phenol ND 1 0 10 2-Chlorona hthalene ND l 0 10 <br /> 2-Chlorophenol ND 1 0 10 4-Chloro henyl Phenyl Ether ND 1 0 10 <br /> Chrysene ND 10 l0 Dibenzo(a,h)anthracene ND 10 10 <br /> Dibenzoturan ND 1 0 10 Di-n-butyl Phthalate ND 1 0 10 <br /> l2-Dichlorobenzene ND 1010 1,3-Dichloroben7ene ND 10 10 <br /> 1,4-Dichlorobenzene ND 1 0 10 3 3-Dlchlorobenzidme ND 10 20 <br /> 2,4-Drc1loro henol ND to 10 Diethyl Phthalate ND 1 0 10 <br /> . <br /> 2,4-Dimethylphenol ND lo ]0 Dimeth i Phthalate ND 1 0 10 <br /> 4,6-Dmitro-2-methyl henoi ND 1 050 2,4-Dmitro henoi ND 1 0 50 <br /> 2,4-Dimtrotoluene ND <br /> 10 10 2 6-Dmrtrotoluene ND 1 0 10 <br /> Di-n-oct I Phthalate ND 10 10 1,2-Di hen [h drazine ND 1 0 10 <br /> Fluoranthene ND 10 10 Fluorene ND IO 10 <br /> Hexachlorobenzene ND 10 10 hlexachlorobutadiene ND IO 1 10 <br /> Hexachloroc clo entadiene ND 10 50 Hexachloroethane ND 1 0 10 <br /> Indeno(1,2,3-cdpyrene ND 10 10 Iso horone ND 1 0 l0 <br /> 2-Meth ina hthalene ND l0 10 2-Meth 1 henoi(o-Cresol) ND 1 0 10 - — <br /> 3&/or 4-Methyl henoi(m, -Cresol) ND 1 0 10 Naphthalene ND l 0 10 <br /> 2-Nitroaniime ND 10 50 3-Nitroamlme ND 10 50 <br /> 4-Nitroamline ND 10 50 Nitrobenzene ND 10 50 <br /> 2-Nitr2henoi ND 1 0 50 4-Nitrophenol ND 1 0 10 <br /> N-Nitrosodi hen [amine ND 1 0 10 N-Nitrosodi-n-propylamine ND 1 0 10 <br /> Pentachlorophenol ND l 0 50 1 Phenantbrene ND l 0 10 <br /> Phenol ND l0 10 Pyrene ND l0 10 <br /> 1,2,4-Tnchlorobenzene ND 10 10 2,4 5-Trichlorophenol ND 1 0 10 <br /> 2 4 6-Trichlorohenol ND 110 10 <br /> Surrogate Recoveries(%) <br /> %SSI 94 1 %SS2 98 7 <br /> %SS3 92 4 %SS4 97 2 <br /> %SS5 867 %556 88 9 <br /> Comments i <br /> *water samples and all TCLP&SPLP extracts are reported in gg/L soil/sludgelsolid samples in mg/kg,wipe samples inµg/wipe,product/oil/non- <br /> aqueous liquid samples to mg/L <br /> ND means not detected above the reporting limit,N/A means analyte not applicable to this analysts <br /> #)surrogate diluted out of range,&)low or no surrogate due to matrix interference <br /> • h)lighter than water immiscible sheen/product is present,i)liquid sample that contains greater than—2 vol %sediment,J)sample diluted due to high <br /> organic content,k)reporting limit raised,benzoic acid found m LCS/LCSD samples Benzoic acid found to the method blank at a detectable <br /> concentration but under the RL for this compound <br /> DHS Certification No 1644 C`A�Angela Rydelms, Lab Manager <br />