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110 2nd Avenue South,#D7 Pacheco,CA 94553-5560 Inc.McCampbell Analytical, Telephone 925-798 1620 Fax 925 798-1622 -- WehSite www mccampbcll coin E mail main@mecampbell coin Advanced GeoEnvironmental, Inc Chent Project ID FIag City Chevron Date Sampled 01/20/04-01/22/04 • 837 Shaw Road Date Received 01/23/04 Client Contact Tim Cuellar Date Extracted 01/23/04 Stockton, CA 95215 - Client P O Date Analyzed 01/24/04-01/28/04 Sethi-Volatile Organics by GC/MS(Baste Target List)* Extraction Method SW3510C Analytical Method. SW8270D Work Order 0401260 Lab ID 0401260-009D - _ f Client ID P39-47to51 - - Matrix Water CompoundConcentration * DF °,,'i„�g Compound Conccntration * DF x�Ltam�g Acenaphthene ND 1 0 30 Acenaphthylene ND 1 0 10 Anthracene ND 10 10 Benzidine ND 10 50 Benzoic Acid ND 1 0 50 Benzo(a)anthracene ND 10 ]0 Benzo(b)fluoranthene ND 1 0 10 Benzo(k)fluoranthene ND 10 10 Benzo(g,h,i)perylcnc ND 1 0 10 Benzo(a)pyrene ND 1 0 I 10 Benzyl Alcohol ND 1 0 20 Bis 2-chloroethox Methane ND 1 0 10 Bis(2-chloroeth l)Ether ND 1 0 10 Bis(2-chlorotsopro l)Ether ND to- t0 Bis 2-eth lhex l)Phthalate ND 1 0 10 4-Bromo hen t Phenyl Ether ND 10 10 Butylbenai Phthalate ND 1 0 10 4-Chloroanihne ND to 20 4-Chloro-3-methyl henoi ND l 0 10 2-Chlorona hthalene ND l 0 10 2-Chloro heriol ND 1 0 10 4-Chloro hen 1 Pheny]Ether ND to 10 Chrysene ND 1 0 10 Dibenzo(a,h)anthracene ND 10 10 Dibenzofuran ND 1 D 10 Di-n-but 1 Phthalate ND to 10 1,2-Dichlorobenzene ND 10 10 1,3-Dichlorobenzene ND 10 10 1 4-Dichlorobenzene ND l 0 10 3 3-Dichlorobenzidme ND 1 0 1 20 2,4-Dichloro henoi ND 1 0 10 Diethyl Phthalate ND 10 1 10 2 4-Dimethylphenol ND 1 0 10 Dimethyl Phthalate ND I O—F l0 4 6-Dmitro-2-meth E henol ND 10 50 2,4-Dinitra henol ND to SD 2,4-Dinitrotoluene ND 1 0 10 2,6-Dmitrotoluene ND l D l0 Di-n-oct l Phthalate ND 1 0 10 1,2-Dihen lh drazme ND 1 0 10 Fluoranthene ND 10 10 Fluorene ND 10 10 Hexachlorobenzene ND 10 10 Hexachlorobutadiene ND 10 10 Hexachloroc clo entadiene ND 1 0 50 Hexachloroethane ND to 10 Indeno 1,2 3-cdpyrene ND l 0 10 Iso borone ND I-1 0--- 10 2-Methylnaphthatene ND _ 1 0 10 2-Meth 1 henoi(o-Cresol) ND 1 0 10 – 3&/or 4-Methylphenol(m, -Cresol) ND 1 0 10 Na hthalene ND 10 10 2-Nitroaniline ND 10 50 3-Nitroanilme ND 10 50 4-Nitroanihne ND 10 50 i Nitrobenzene ND i 10 50 2-Nitrophenol ND 1 0 50 4-Nitrophenol ND l 0 10 N-Nitrosodiphen lamme ND 1 0 10 N-Nitrosodi-n- roylamine ND 10 10 Pentachlorophenol ND 1 0 50 Phenanthrene ND 10 10 Phenol ND 10 10 P ne ND 10 10 1,2,4-Trichlorobenzene ND 1 0 10 2,4,5-Trichlorophenol ND 10 10 5 2 4 -Trichloro henoi ND 1 0 10 Surrogate Recoveries(%) %SSI 91 9 %SS2 955 %SS3 91 4 %SS4 90 4 %SS5 868 %SS6 980 Comments t *water samples and all TCLP&SPLP extracts are reported in pg/L,soil/sludge/solid samples in mg/kg,wipe samples inµg/wipe,product/oillnon- aqueous liquid samples in mg/L ND means not detected above the reporting Limit,N/A means analyte not applicable to this analysts #)surrogate diluted out of range,&)low or no surrogate due to matrix interference • h)lighter than water immiscible sheen/product is present,i)liquid sample that contains greater than–2 vol %sediment,I)sample diluted due to high organic content,k)reporting limit raised,benzoic acid found in LCS/LCSD samples Benzoic acid found in the method blank at a detectable concentration but under the RL for this compound DHS Certification No 1644 qJIML1W Angela Rydehus,Lab Manager