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110 2nd Avenue South #D7 Pacheco CA 94553-5560 <br /> McCampbell Analytical, Inc. Telephone 925-798-1620 Fax 925-798-1622 <br /> --_ -_—- Website www mecampbell corn E-mail maio@mecarrgkcll com- _ —_---- <br /> Advanced GeoEnviromnental,Inc Client Project ID Flag City Chevron Date Sampled 01/20/04-01/22/04 <br /> 837 Shaw Road Date Received 01/23/04 <br /> Stockton,CA 95215 Client Contact Tian Cuellar Date Extracted 01/23/04 <br /> Client P O Date Analyzed 01124/04-01/28/04 <br /> Semi-Volatile Organics by GUMS(Basic Target List)* <br /> Extraction method SW3550C Analytical Method SW8270D Work Order 0401260 <br /> Lab ID 0401260-016A <br /> - - Client 1D - - P40A-45' f <br /> Matrix Sol] <br /> Compound Concentration * DF a�s Compound Concentration * DF R`t7O�,,;,"g <br /> Acenaphthene ND 10 033 Acenaphthylene ND 1 0 033 <br /> Acetoehlor ND ! 1 0 033 Anthracene ND 1 0 033 <br /> Benzidine ND 1 0 16 Benzoic Acid ND 1 0 16 <br /> Benzo(a)anthracene ND l 0 033 Benzo(b)fluoranthene ND 1 0 033 <br /> Benzo k)fluoranthene ND 1 0 033 Benzo(g,h,i)2erylene ND 1 0 033 <br /> Benzo(a)pyrene ND 1 0 033 Benzyl Alcohol ND l 0 066 <br /> Bis 2-chloroethox )Methane ND 1 0 033 Bis 2-chloroeth I Ether ND l 0 033 <br /> Bis(2-chlorolsopropyl)Ether` ND - 1 0 033 Bis 2-ethylhexyl)Adipate ND 1 0 033 <br /> Bis(2-ethylhex I)Phthalate ND 1 0 033 4-Bromo hen l Phenyl Ether ND 1 0 033 <br /> But lben ]Phthalate ND 1 0 0 33 4-Ch]oroanilme ND 1 0 066 <br /> Nitrobenzene ND 1 0 1 6 4-Chloro-3-meth lhenol ND 1 0 033 <br /> 2-Chlorona hthalene ND 1 0 033 2-Chloro henot ND 1 0 033 <br /> 4-Chlorophen 1 Phenyl Ether ND 1 0 033. 1 Chrysene ND t 0 033 <br /> Dibenzo(a,h)anthracene ND 1 0 033 Dibenzofuran ND 1 0 033 <br /> Di-n-butyll Phthalate ND 1 0 033 1,2-Dichlorobenzene ND 10 033 <br /> . 1 3-Dichlorobenzene ND 1 0 133 1,4-Dichlorobenzene ND 1 0 033 <br /> 3,3-Dichlorobenzidine ND 1 0 066 2 4-Dtchloro heno) ND 1 0 032 <br /> Dieth ]Phthalate ND 1 0 033 2,4-Dimethylphenol ND 1 0 033 <br /> Dimethyl Phthalate ND 1 0 033 4,6-Dinitro-2-methyl heno] ND _10 16 <br /> 2,4-Dinitrn heno] ND 1 0 16 2,4-Dmitrotoluene ND 10 1 033 <br /> 2,6-Dmitrotoluene ND 1 0 033 Di-n-oct 1 Phthalate ND 1 0 1 033 <br /> 1 2-Di hen Ihydrazme ND 1 0 033 Fluoranthene ND l 0 033 <br /> Fluorene ND 1 0 033 Hexachlorobenzene ND 10 033 <br /> Hexachlorobutadiene ND 1 0 0 33 Hexachlorocyclo entadtene ND 10 16 <br /> Hexachloroethane ND 1 0 033 Indeno(1,2,3-cd)pyrene ND 1 0 033 - <br /> Iso horone ND l 0 0 33 2-Meth lna hthalene ND 1 0 033 <br /> 2-Meth l heno/(o-Cresol) ND 1 0 033 3&/or 4-Meth l henal m p-Cresol ND 1 0 033 <br /> Naphthalene ND 1 0 033 2-Nitroanilme ND 1 0 1 6 <br /> 3-Nitroanilme ND 10 16 4-Nitroamline ND <br /> 1 16 <br /> 2-Nitro henot ND 1 0 1 6 4-Nitrophenol ND l 0 033 <br /> N-Nitrosodi hen larnme ND 10 033 N-Nitrosodi-n-propylamine ND 1 0 033 <br /> Pentachlorophenol ND 1 0 1 6Phenanthrene ND 10 1 033 <br /> Phenol ND 10 0 33 Pyrene 71ND 1 0 033 <br /> l,2,4-Trichlorobenzene ND 1 0 033 2,4,5-Trichlorophenol ND 1 0 0 33 <br /> 2 4 6-Trichloro henol ND 1 0 1 033 <br /> Surrogate Recoveries(%) <br /> %SS 1 106 %SS2 107 <br /> %SS3 893 %SS4 888 <br /> %SS5 85 7 %SS6 956 <br /> Comments <br /> 'water samples and all TCLP&SPLP extracts are reported in ltg/L,soil/sludge/solid samples in mg/kg,wipe samples inµg/wipe,product/oil/non- <br /> aqueous liquid samples in mg/L <br /> ND means not detected above the reporting limit,NIA means analyte not applicable to this analysis <br /> #)surrogate diluted out of range,&)low or no surrogate due to matrix interference <br /> h)lighter than water immiscible sheen/product is present 1)liquid sample that contains greater than--2 vol %sediment,j)sample diluted due to high <br /> organic content,k)reporting limit raised,benzoic acid found in LCS/LCSD samples Benzoic acid found in the method blank at a detectable <br /> concentration but under the RL for this compound <br /> DHS Certification No 1644 �� Angela Rydelius, Lab Manager <br />