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1102nd Avenue South 01137 Pacheco CA 94553-5560 <br /> McCampbell Analytical, Inc. Telephone 925-798 1620 Fax 925-798-1622 <br /> Weblite www niccanipbell cum Emil main©mccampbell com- - <br /> Advanced GeoEnvironmental, Inc Client Project ID Flag City Chevron Date Sampled 01/20104-01/22/04 <br /> 837 Shaw Road Date Received 01/23/04 <br /> Stockton,CA 95215 <br /> Client Contact Tim Cuellar Date Extracted 01/23/04 <br /> - <br /> CIient P O --fDatc Analyzed 01124104-01128/04 <br /> Semi-Volatile Organics by GC/MS(Basic Target List)* <br /> Extraction Method SW3550C Analytical Method SW8270D Work Order 0401260 <br /> Lab ID 0401260-015A <br /> Client ID - - P40A-30' - <br /> Matrix Soil <br /> Compound CORCentratlon * DF Reporting « RcpOfvig <br /> Gom <br /> P Lima Compound Concentration DF (amrt <br /> Arena hthene ND 1 0 0 33 Acena hthylene ND 1 0 033 <br /> Acetochlor ND 1 0 0 33 1 Anthracene ND 1 0 033 <br /> Benzidine ND 10 16 Benzoic Acid ND 1 0 16 <br /> Benzo(a)anthracene ND 1 0 0 33 Benzo(b)fluoranthene ND 1 0 033 <br /> Benzo(k)fiuoranthene ND l 0 033. Benzo(S,h,i)perylene ND 1 0 033 <br /> Benzo(a) enc ND 1 0 033 Benzyl Alcohol ND 1 0 066 <br /> Bis(2�hloroethoxy)Methane ND 1 0 033 Bis 2-chloroeth 1 Ether ND 1 0 033 <br /> Bis 2-chlomisoprop 1)Ether ND - 1 0 033 Bis(2-ethylhexyl)Adipate ND 10 033 <br /> Bis(2-eth ]hex l)Phthalate ND 1 0 033 4-Bromo hen 1 Phenyl Ether ND 1 0 033 <br /> Butylbenzyl Phthalate ND 1 0 033 4-Chloroanelme ND 1 0 066 <br /> Nitrobenzene ND 1 0 1 6 4-Chloro-3-methyl --1 ND 1 0 033 <br /> 2-Chlorona hthalene ND l 0 033 2-Chloropheno1 i ND 1 0 I 033 <br /> 4-Chloro henyl Phen 1 Ether ND 1 0 0 33 Ch sene ND 1 0 033 <br /> Dibenzo a,h anthracene ND 1 0 033 Dibenzofuran ND <br /> I 10 033 <br /> Di-n-butyl Phthalate ND 1 0 033 1 2-Dichlorobenzene ND 1 0 033 <br /> 1,3-Dichlorobenzene ND 10 033 1,4-Dichlorobenzene ND 10 033 <br /> 3,3-Ditihlorobenzidine ND 1 0 1 066 2,4-Dichlorophenol ND 1 0 033 <br /> Deethyi Phthalate ND l 0 1 033 2 4-Dimeth Ephenol ND 1 0 033 <br /> Dimethyj Phthalate ND 1 0 033 4,6-Dinitro-2-meth 1 henol ND 1 0 16 <br /> 2 4-Dmttro henol ND 1 0 1 6 2,4-Denetrotoluene ND 1 0 033 <br /> 2,6-Dinitrotoluene ND 1 0 033 Di-n-octyl Phthalate ND l 0 033 <br /> 1,2-Di hen lh drazine ND 1 0 033 Fluoranthene ND 10 033 <br /> Fluorene ND 1 0 033 Hexachlorobenzene ND 1 0 033 <br /> Hexachlorobutadiene ND 1 0 033 Hexachloroc clo entadiene ND 1 0 16 <br /> Hexachloroethane ND l 0 033 Indeno 1,2,3-cd)12yrene _RD 1 0 033 <br /> Iso horone ND 1 0 033 2-Methylnaphthalene ND 1 0 033 <br /> 2-Meth 1 henol(o-Cresol) ND 1'0 033 3&/or 4-Meth 1 henol(m,p-Cresol) ND 10 033 <br /> Naphthalene ND 10 033 2-Nitroanilme ND l 0 i G <br /> 3 Nitrganihne ND ] 0 l 6 4-Nitroanilme ND l 0 1 6 <br /> 2-Nitro henol ND 1 0 1 6 4-Nitrophenot ND 10 033 <br /> en <br /> N-Nitrosodi hlamine ND 10 033 N-Nitrosodi-n-pLopylamme ND 10 033 <br /> Pentachloro henol ND 10 1 6 Phenanthrene ND E10 033 <br /> Phenol ND 10 033 Pyrene ND 0 33 <br /> 1,2,4-Tnchlorobenzene ND 1 0 0 33 2,4,5-Tnchloro henol ND 1 0 0 33 <br /> 2 4 6-Tnchloro henol ND l 0 0 33 <br /> Surrogate Recoveries(%) <br /> %SSI 104 %S S2 104 <br /> %SS3 876 %SS4 889 <br /> %SS5 828 %SS6 938 <br /> Comments <br /> water samples and all TCLP&SPLP extracts are repotted inµg/L,soiUsludge/solid samples in mg/kg,wipe samples in jig/wipe,product/oLUnon- <br /> aqueous liquid samples in mg1L <br /> ND means not detected above the reporting limit NIA means analyte not applicable to this analysis <br /> #)surrogate diluted out of range,&)low or no surrogate due to matrix interference <br /> h)lighter than water immiscible sheen/product is present i)liquid sample that contains greater than--2 vol %sediment,j)sample diluted due to high <br /> organic content k)reporting limit raised,benzoic acid found in LCS/LCSD samples Benzoic acid found in the method blank at a detectable <br /> concentration but under the RL for this compound <br /> DHS Certification No 1644 Angela Rydelius, Lab Manager <br />