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110 2nd Avenue South,#D7,Pacheco CA 94553-5560 <br /> McCampbelI Analytical, Inc. Telephone 925-798-1620 Fax 925-798-1622 <br />-_ w- -- — -- ---- _- W— ------- — -Web5ite www mccampbell com E-mat]. mainQenccampbell com-- -_ - ---- <br /> Advanced GeoEnvironmental, Inc Client Project ID Flag City Chevron Date Sampled 01/20/04-01122/04 <br /> 837 Shaw Road Date Received 01/23/04 <br /> Stockton,CA 95215 Client Contact Tun Cuellar Date Extracted 01/23/04 <br /> Client P Q Date Analyzed 01/24/04-01/28/04 <br /> Semi-Volatile Organics by GC/MS(Basic Target List)* <br /> Extraction Method SW3550C Analytical Method SW8270D Work Order 0401260 <br /> Lab ID 0401260-018A <br /> _ - - Client ID _ _ P41-30' <br /> Matrix Soil <br /> Compound Concentrahon* DF R`pmmg * Reporting <br /> r P Ltron Compound Concentration DF L=t <br /> Acena hthene ND 1 0 033 ' Acena hth lene ND 1 0 0 33 <br /> Acetochlor ND 1 0 033 Anthracene ND 1 0 033 <br /> Benzidine ND 10 1 6 Benzoic Acid ND 1 0 16 <br /> Benzo(a) nthracene ND 1 0 033 Benzo(b)fluoranthene ND 1 0 033 <br /> Benzo(k)fluoranthene ND 1 0 0 33 Benzo ,h8 i)perylene ND 10 1 033 <br /> Benzo(a)2yrene ND 1 0 033 Benzyl.Alcohol ND 1 0 0 66 <br /> Bis(2-chloroethox )Methane ND 1 0 033 Bis(2-chloroeth 1)Ether NI) 10— 033 <br /> i Bis(2-chloroiso ro 1)Ether ND 1 0 033- Bis(2�thylhex i Adi ate ND 1 0 1 033 <br /> Bis(2-eth lhex l)Phthalate ND 1 0 033 4-13romo hen 1 Phenyl Ether ND 1 0 033 <br /> Bu ]benzyl Phthalate ND 1 0 033 4-Chloroantline ND 1 0 066 <br /> Nitrobenzene ND 1 0 1 6 4-Chloro-3-meth 1 henol ND 10 033 <br /> 2-Chlorona hthalene ND 1 0 033 2-Chlorophenol ND l 0 033 <br /> 4-Chlorophenyl Phenyl Ether ND 1 0 0 33 Ch Bene ND 1 0 033 <br /> Dibenzo(a h)anthracene ND 1 0 033 Dibenzoluran ND 1 0 033 <br /> Di-n-butyl Phthalate ND 1 0 033 1,2-Dichlorobenzene ND 1 0 033 <br /> 1,3-Dichlorobenzene ND 1 0 033 1 4-Dtchlorobenzene ND1 0 0 33 <br /> . 3,3-Dichlorobenzidine ND 1 0 066 2,4-Dichlorophen] ND 1 0 03.1 <br /> Diethyl Phthalate ND 1 0 033. 2,4-Dimeth 1 henol ND 10 033 <br /> Dimethyl Phthalate ND 1 0 033 4,6-Dinitro-2-meth 1 henol ND 1 0 1 6 <br /> 2 4-Dinitro henot ND 1 0 16 2,4-Dinitrotoluene E]FND 1 0 033 <br /> 2,6-Dmitrotoluene ND 1 0 033 Di-n-oc 1 Phthalate 1 0 033 <br /> 1 2-Di hen lh drazine ND 1 0 033 Fluoranthene 1 0 033 <br /> Fluorene ND l 0 0 33 Hexaehlorobenzene ND 1 0 033 <br /> Hexachlorobutadiene ND 1 0 033 Hexachloroc clo entadiene ND 10 i 1 6 <br /> Hexachloroethane ND 1 0 03-3 Indeno 1,2,3-cd)pyrene ND 10 033 <br /> Iso horone ND 10 033 2-Meth lna hthaleneND 1 0 0 33 <br /> 2-Meth 1 henol o-Cresol) ND ] 0 0 33 3&/or 4-Meth 1 henol(m, -Cresol ND 1 0 033 <br /> Naphthalene ND 1 0 033 2-Nitroanilme ND 1 0 l 6 <br /> 3-Nitmamline ND l0 16 4-Nitroanehne ND 10 16 <br /> 2-Nitrophenol ND 1 0 16 4-Nitro henol ND t 0 033 <br /> N-Nitrosodi hen lamine ND 1 0 1 033 N-Nrtrosodi-n- rop ]amine ND l 0 0 33 <br /> Pentachlorophenol ND 1 0 1 6 Phenanthrene ND E�O <br /> 0 33 <br /> Phenol ND 1 0 033 Pyrene ND 0 33 <br /> 1 2 4-Tnchlorobenzene ND 1 0 033 2,4,5-Tnchlora henoi ND 0 33 <br /> 2 4 -Tnchlorol2henol ND 1 0 033 <br /> Surrogate Recoveries{%) <br /> %SS 1 110 °/.SS2 100 <br /> %SS3 953 %SS4 990 <br /> %S-S-5 — 95 1 %SS6 985 <br /> Comments <br /> *water samples and all TCLP&SPLP extracts are reported in Ng/L,soillsludge/solid samples in mg/kg,wipe samples in pg/wipe,product/orl/non- <br /> aqueous liquid samples in mg/L <br /> ND means not detected above the reporting lima,N/A means analyte not applicable to this analysis <br /> ##)surrogate diluted out of range,&)low or no surrogate due to matrix interference <br /> h)lighter than water immiscible sheen/product is present,t)liquid sample that contains greater than–2 vol %sediment i)sample diluted due to high <br /> organic content,k)reporting limit raised,benzoic acid found in LCS/LCSD samples Benzoic acid found in the method blank at a detectable <br /> concentration but under the RL for this com ound <br /> DHS Certification No 1644 Angela Rydelius,Lab Manager <br />