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110 2nd Avenue South,#D7 Pacheco CA 94553-5560 <br /> McCampbell Analytical, Inc. Telephone 925-798-1620 Fax 925-798 1622 <br /> _Wobgtte www mceampbell corn E mail Tmtn@mccatnpbetl cam==— <br /> Advanced GeoEnvironmcntal, Inc Client Project ID Flag City Chevron Date Sampled 01/20/04-01/22/04 <br /> 837 Shaw Road Date Received 01/23/04 <br /> Stockton, CA 95215 Client Contact Tim Cuellar Date Extracted 01/23/04 <br /> Client P O Date Analyzed 01/24/04-01/28/04 <br /> Semi-Volatile Organics by GC/MS(Basic Target List)* <br /> ExtiactionMethod SW3550C Analytical Method SW8270D Work Order 0401260 <br /> Lab ID 040 t 260-019A <br /> _ = Client ID_ -- - - - P41-45' <br /> Matrix Sol] <br /> Compound Concentration* DF Reportms * �ttii g <br /> iumt Compound Concentration DF <br /> Acena hthene ND 1 0 033 Acenaphthylene I ND 1 0 -033 <br /> Acetochlor ND 1 0 033 Anthracene ND ! 0 0 33 <br /> Benzidine ND 1 0 1 6 Benzoic Acid ND 1 0 1 6 <br /> Benzo a anthracene ND 1 0 033_ Benzo b fluotanthene ND 1 0 033 <br /> Benzo(k)fluoranthene I ND 1 0 033 Benzo( ,h i)pe lene ND 1 0 0 33 <br /> Benzo(a)pyrene ND 1 0 033 Benzyl Alcohol ND 1 0 0 66 <br /> Bis(2-chloroethox Ivtethane ND 1 0 03 Bis 2-chloroeth !)Ether ND 1 0 0 33 <br /> - Bis(2-chioroiso ro ])Ether ND - 1 0 033 Bis(2-eth lhex 1)Adipate ND 1 0 0 33 <br /> Bis 2-ethylhexyl)Phthalate ND 1 0 0 33 4-Bromo hen i Phenyl Ether ND 1 0 033 <br /> Bu lbenz I Phthalate ND 1 0 0 33 4-Chloroanilme ND 1 0 066 <br /> Nitrobenzene ND 1 0 1 6 4-Chloro-3-methylphenot ND 1 0 033 <br /> 2-Chlorona hthalene ND 1 0 0 33 —2-Chlor ND 1 0 03-1 <br /> 4-Chlorohenyl Phenyl Ether ND 1 0 033 Ch gene ND 1 0 033 <br /> Dibenzo a,h anthracene ND 1 0 033 Dibenzofuran ND 1 0 033 <br /> Di-Ti-but l Phthalate ND 1 0 033 1,2-Dichlorobenzene ND 1-0 —033 <br /> 1 3-Dichlorobenzene ND 1 0 033 1,4-Dichlorobenzene ND 1 0 10 33 <br /> 3 3-Dichlorobenzidine I ND 10 0 66 2,4-Dichloro henol ND 1 0 033 <br /> Diethyl Phthalate ND 1 0 033 2,4-Dimeth 1 henol ND 1 0 033 <br /> Dimethyl Phthalate ND 1 0 033 4,6-Dtnitro-2-methyl henol ND 1 0 16 <br /> 2,4-Dinitry henol ND 1 0 16 12,4-Dinitrotoluene ND _10 033 <br /> 2,6-Dimtrotoluene ND 1 0 033 Di-n-act I Phthalate ND l 0 033 <br /> 1,2-Diph drazme ND 1 0 0 33 Fluoranthene ND 1 0 0 33 <br /> Fluorene ND l 0 10 33 Hexachlorobe-nzene ND 1 0 033 <br /> Hexachlorobutadiene �ND <br /> 1 0 033 Hexaehloroc cl0 entadiene ND 10 1 6 <br /> Hexachloroethane 1 0 0 33 Indeno(1,2,3,d) ene ND 1 0 033 - <br /> Iso horone 1 0 033 2-Methylnaphthalene ND __1_O_ 033 <br /> 2-Meth I henol(o-Cresol) ND to 033 3&lor 4-Meth 1 henol m, -Cresol ND 1 0 033 <br /> Naphthalene ND l 0 10 33 1 2-Nitroamlme ND 10 1 6 <br /> 3-Nitroamlme ND 10 t 6 1 4-Nitroantlme ND 10 16 <br /> 2-Nttro henol ND 10 16 4-Nitrophenol I ND l 0 0 33 <br /> N-Nitrosodi hen lamme ND 10 033 N-Nttrosodt-n-prop /amine ND 1 0 0 33 <br /> Pentachlorophenol ND 10 1 6 Phenanthrene ND 10 1 033 <br /> Phenol ND 10 0 33 Pyrene ND ! 0 0.33 <br /> 1,2,4-Trichlorobenzene ND 1 0 1 033 2,4,5-Trichlorophenol ND 1 0 0 33 <br /> 2 4 6-Tnchlorohenol ND 16- 1-033 <br /> Surrogate Recoveries{%) <br /> °/aSS! 95 9 %SS2 858 <br /> %SS3 884 %SS4 <br /> 850 <br /> %SSS <br /> 858 °/6556 gq 2 <br /> Comments <br /> *water samples and all TCLP&SPLP extracts are reported inµg/L,soil/sludgelsohd samples to mg/kg,wipe samples in gg/wipe,product/od/non- <br /> aqueous liquid samples in mg/L <br /> ND means not detected above the reporting;.t,NIA means analyte not applicable to this analysis <br /> #)surrogate diluted out of range,&)low or no surrogate due to matrix interference <br /> h)lighter than water immiscible sheen/product is present,t)liquid sample that contains greater than–2 vol %sediment,J)sample diluted due to high <br /> organic content,k)reporting limit raised,benzoic acid found in LCS/LCSD samples Benzote acid found in the method blank ata detectable <br /> concentration but under the RL for this compound <br /> DHS Certification No 1644 'Angela Rydehus, Lab Manager <br />