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110 2nd Avenue South,#D7,Pacheco CA 94553-5560 <br /> McCampbell Analytical, Inc. Telephone 925 798-1620 Fax 925-798-1622 <br /> _ __ - __ — _ _ _ -_ _-_ _ _- _-�- _ —Website www mccampbell corn E-mail niaw@mccampbell corn�- _- T --�_- <br /> Advanced GeoEnvironmental,Inc Client Project 1D Flag City Chevron Date Sampled 01/20/04-01/22/04 <br /> 4 <br /> 837 Shaw Road Date Received 01/23/04 <br /> Client Contact Tun Cuellar Date Extracted 01/23/04 <br /> Stockton,CA 95215 __ <br /> Client P O Date Analyzed 01/24/04-01/28/04 <br /> Semi-Volatile Organics by GUMS(Basic Target List)* <br /> Fxtracnon Method SW3550C Analytical Method SW8270D Work Order 0401260 <br /> Lab ID 0401260-021A <br /> - Client ID - - - P42-15' - - - - <br /> Matrix Soil <br /> Compound Concentration * DF L=t Compound_s Compound Concentration * DF �s <br /> Acenaphthene ND 1 0 033 Acenaphthylene ND 1 0 033 <br /> Acetochlor ND 1 0 033 Anthracene ND 1 0 033 <br /> Benzidine ND 1 0 16 Benzoic Acid ND 1 0 1 6 <br /> Benzo(a)anthracene ND 1 0 033 Benzo b fluoranthene ND 1 0 033 <br /> Benzo fluoranthene ND 1 0 033 Benzo(g,h i) a ]ene ND 1 0 033 <br /> Benzo(a)pyrene ND 1 0 033 Benzyj Alcohol ND 1 0 066 <br /> Bis 2-chloroethoxy Methane ND 1 0 033 Bis(2-chloroeth ])Ether ND 1 0 033 <br /> Bts 2-chloroiso ro yl Ether ND 1 0 033 Bis(2-ethylhex l)Adipate ND 1 0 033 <br /> Bis 2-eth lhex 1)Phthalate ND 1 0 033 4-Bromo hen I Phenyl Ether ND E 1 0 033 <br /> Butylben l Phthalate ND 1 0 033 4-Chloroaniline ND l 0 066 <br /> Nitrobenzene ND E 1 0 16 4-Chloro-3-meth1phenol ND 1 0 033 <br /> 2-Chlorona hthalene ND l 0 033 2-Chloro henoi ND 1 0 033 <br /> 4-Chloro hen l Phenyl Ether ND 1 0 0 33 Ch scne ND 1 0 033 <br /> Dibenzo a h anthracene. ND 1 0 033 ; Dibenzofuran ND 1 0 033 <br /> D:-n-bu i Phthalate ND 1 0 033 1,2-Dichlorobenzene ND 10 033 <br /> 1,3-Dichlorobenzene ND 1 0 1 033 1,4-Dtchlorobenzene ND l 0 033 <br /> 4P3,3-Dichlorobenzidme ND 1 0 066 2,4-Dichloro henol ND 1 0 033 <br /> Diethyl Phthalate ND 10 033 2 4-Dimethylphenol ND 1 0 033 <br /> Dimethyl Phthalate ND 1 0 0 33 4,6-Dinitro-2-meth I henoi ND 1 0 16 <br /> 2,4-Dinitrohenol ND 1 0 1 6 2,4-Dmitrotoluene ND 1 0 033 <br /> 2 6-Dinitrotoluene ND 1 0 033 Dt-n-octyl Phthalate ND 1 0 033 <br /> 1,2-Dt hen lh drazine ND 1 0 033 Fluoranthene ND 1 0 J 033 <br /> Fluorene ND 1 0 033 Hexachlorobenzene ND 1 0 033 <br /> Hexachlorobutadiene ND 1 0 033 Hexachloroc cla entadiene ND 10 1 6 <br /> Hexachloroethane ND 10 033 Indeno(1,2,3-cdpyrene ND 1 0 033 <br /> Iso horone ND 10 033 2-Meth ina hthalene ND 1 0 033 <br /> 2-Meth 1phenol{o-Cresol ND 1 0 033 3&/or 4-Meth [ henoi m, -Cresol) ND 10 033 <br /> Naphthalene ND 10 033 2-Nitroamhne ND 10 16 <br /> 3-Nitroanilme ND l0 16 4-Nitroanthne ND 10 16 <br /> 2-Nitrophenol ND 1 0 1 6 4-Nitrophenol ND 1 10 033 <br /> N-Nitrosodt hen lamine ND to 0.33 N-Nitrosodi-n-eropylamine ND 10 033 <br /> Pentachloro henoi ND 1 0 1 6 Phenanthrene ND ] 0 033 <br /> Phenol ND 1 0 0 33 P ene ND 1-0 0 33 <br /> 1,2,4-Trichlorobenzene ND to 033 2,4,5-Trichlorophenol ND 10 033 <br /> 2 4 6-Tnchloro henoi I ND 1 0 033 <br /> Surrogate Recoveries <br /> %SSZ 97 9 %SS2 <br /> 856 <br /> %SS3 88 3 %SS4 90 5 <br /> %SS5 81 0 E 0/.SS6 <br /> 908 <br /> Comments <br /> "water samples and all TCLP&SPLP extracts are reported in pg/L,soil/sludge/solid samples in mg/kg,wipe samples inµg/wipc,product/oil/non- <br /> aqueous liquid samples in mg/L. <br /> ND means not detected above the reporting limit,NIA means analyte not applicable to this analysis <br /> #)surrogate diluted out of range,&)low or no surrogate due to matrix interference <br /> h)lighter than water immiscible sheeniproduct is present,i)liquid sample that contains greater than—2 vol %sediment j)sample diluted due to high <br /> organic content,k)reporting limit raised,benzoic acid found in LCS/LCSD samples Benzoic acid found in the method blank at a detectable <br /> cumentration but under the RL for this compound <br /> DHS Certification No 1644 ' Angela Rydelius, Lab Manager <br />