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110 2nd Avenue South,t1D7 Pacheco CA 94553 5560 <br /> Inc.McCampbell Analytical, Telephone 925-798 1620 Fax 925 798-1622 <br /> —Website www McCampbell Com E Mail Matti@mccampbell wm - _— <br /> Advanced GeoEnvironmental, Inc Chent Project ID Flag City Chevron Date Sampled 01/20104-01/22/04 <br /> . 837 Shaw Road Date Received 01/23/04 <br /> Stockton, CA 95215 <br /> Client Contact Tim Cuellar Date Extracted 01/23/04 <br /> - - <br /> Client P O LDateAnalyzed 01124104-01/28/04 <br /> Senu-Volatile Organics by GUMS(Basic Target List)* <br /> Extmcnon Method SW3550C Analytical Method SW8270D Work Order 0401260 <br /> Lab ID 0401260-020A <br /> - = Client ID - - P42-10' <br /> Matrix Soil <br /> Compound Concentration * DF xeLum Compound Concentration* DF Re <br /> Lmut porung <br /> Acenaphthene ND 1 0 033 J Acenaphthylene ND 1 0 033 <br /> Acetochlor ND 1-0.. 033 Anthracene ND 1 0 033 <br /> Benzidine ND 1 0 16 Benzoic Acid ND 1 0 16 <br /> Benzo(a)anthracene ND 1 0 033 Benzo(b)fluoranthene ND l 0 0 33 <br /> Benzo(k)fluoranthene ND 1 0 0 33 Benzo( ,gi)pctylcne ND 10 0 33 <br /> Benzo(a)p e ND 1 0 033 Benzyl Alcohol ND 1 0 066 <br /> Bis(2-chloroethox )Methane ND 1 0 033 Bis 2-chloroethyl Ether ND 1 0 033 <br /> Bis 2-chlorotso ro yl Eiher ND 1 0 033 Bis 2-eth /hexyl)Adipate ND 1 0 033 <br /> Bis(2-ethyl he—xi Phthalate ND 1 0 033 4-Bromo hen 1 Phenyl Ether ND 1 0 033 <br /> Bu (benzyl Phthalate ND 1 0 033 4-Chioroanrlme ND1 0 0 66 <br /> Nitrobenzene ND 1 0 16 14-Chloro-3-methyl henoi ND 1 0 033 <br /> 2-Chlorona hthalene ND 1 0 033 2-Chloro henoi ND l 0 033 <br /> 4-Chlora hen 1 Phenyl Fther ND 1 0 033 Chrysene ND 1 0 033 <br /> Dibenzo(a,h)anthracene ND 1 0 033 Dibenzofuran ND 1 0 033 <br /> Di-n-butyl Phthalate ND 1 0 033 1,2-Dichlorobenzene ND 1 0 033 <br /> 1,3-Dichlorobenzene ND 1 0 033 1,4-Dichlorobenzene ND 10 0 33 <br /> 3,3-Dichlorobenzidme ND l 0 0 66 2 4-Dichloro henoi ND 1 0 033 <br /> Diethyl Phthalate ND 1 0 033 2 4-Dimethylph ND 1 0 033 <br /> Dimethyl Phthalate ND 1 0 0 33 4,6-Dmitro-2-methyl henol ND to 1 6 <br /> 2,4-Dmitrohenol ND 10 16 12,4-Dinitrotoluene ND 1 0 033 <br /> 2,6-Dmitrotoluene ND 1 0 033 Di-n-oct 1 Phthalate ND 1 0 033 <br /> 1,2-Diphen lh drazme ND 1 0 033 Fluoranthene ND 1 0 033 <br /> Fluorene ND 1 0 033 Hexachlorobenzene ND 1 0 033 <br /> Hexachlorobutadiene ND i 0 0 33 Hexachloroc clo entadiene ND 1 0 1 6 <br /> Hexachloroethane ND 1 0 0 33 Indeno(1,2,3�dpyrene ND 1 0 033 - <br /> Iso horone ND 1 0 0 33 2-Meth ina hthalene ND 10 033 <br /> 2-Meth 1 henoi(o-Cresol) ND 1 0 033 3&/or 4-Meth I henoi m, -Cresol) ND 1 0 033 <br /> Naphthalene ND 1 0 0 33 2-Nitroanilme ND 1 0 1 6 <br /> 3-Nnroamlme ND 10 16 4-Nitroanihne ND l0 16 <br /> 2-Nitrophenol ND 1 0 1 6 4-Nitro henoi ND 10 033 <br /> N-Nitrosodi hen ]amine ND 10 0 33 N-Nitrosodi-n- ro ylamme ND 10 033 <br /> Pentachlorophenol ND 1 0 1 6 Phenanthrene ND 10 033 <br /> Phenol ND 1 0 033 Pyrene ND 1 0 033 <br /> 1,2,4-Tnchlorobenzene ND 1 0 033 2,4,5-Tnchlorohenol ND !0 0 33 <br /> 2 4 6-Tnchloro henoi ND 10 1 033 <br /> Surrogate Recoveries(%) <br /> %SS1 181 8 1 %SS2 84 2 <br /> %SS3 81 1 %SS4 78 8 <br /> %SS5 800 %SS6 797 <br /> Comments <br /> water samples and all TCLP&SPLP extracts are reported inµg/L,soil/sludge/solid samples to mg/kg,wipe samples in itg/wipe,product/oil/non- <br /> aqueous liquid samples in mg/L <br /> ND means not detected above the reporting limit,NIA means analyte not applicable to this analysis <br /> r� #)Surrogate diluted out of range,&)low or no surrogate due to matrix interference <br /> h}lighter than water immiscible sheen/product is present,i)liquid sample that contains greater than--2 vol %sediment,j)sample diluted due to high <br /> organic content,k)reporting limit raised,benzotc acid found in LCS/LCSD samples Benzoic acid found in the method blank ata detectable <br /> concentration but under the RL for this compound <br /> DHS Certification No 1644 Angela Rydelius,Lab Manager <br />