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110 2nd Avenue South #D7 Pacheco,CA 94553-5560 Inc.McCampbell Analytical, Telephone 925 798-1620 Fax 925-798-1622 µ Web4ite www mecampbell corn F mail main@mccanipbell com------ --- - Advanced GeoEnvironmental, Inc Client Project ID FIag City Chevron Date Sampled 01/20/04-01/22/04 837 Shaw Road Date Received 01/23/04 Stockton, CA 95215 Client Contact Tim Cuellar Date Extracted 01/23/04 - ,- Client P O Date Analyzed 01/24/04-01/28104 Senn-Volattle Organics by GC/MS(Basic Target List)* Extracuon Method SW3550(. Analytical Method SW82701) Work Order 0401260 Lab ID �� 0401260-023A _ a --Client ID - - _ P42-50' ~ - Matrix Soil Compound Concentration DF U Compound Concentration * DF Repo* Renmg Law Compound Acenaphthene ND 1 0 0 33 Acenaphthylene ND 1 0 033 Acetochlor ND 1 0 033 Anthracene NI) 1 0 033 Benzidine ND 1 0 1 6 Benzoic Acid ND 10 1 6 Benzo(a)anthracene ND 1 0 033 Benzo b tluoranthene ND 1 0 033 Henzo(k)fluoranthene ND 1 0 033 Benzo( ,h,i erylene ND 1 0 033 Benzo(a)pyrene ND E 1 0 033 Benzyl Alcohol ND l 0 066 Bis(2-chloroethoxy)Methane ND l 0 033 Bis 2-i hloroethyl)Ether ND 1 0 033 Bis(2-chloro tso ro yl)Ether ND 1 0 0 33 His(2-ethylhexyl Adipate ND '-1 0 I 0 33 Bis 2-eth lhex 1)Phthalate ND 1 0 033 4-Bromo hen 1 Phenyl Ether ND 1 0 033 Bu ]ben 1 Phthalate ND 1 0 0 33 4-Chloroamline ND 1 0 066 Nitrobenzene ND 1 0 16 4-Chloro-3-meth 1 henol ND 1 6 033 2-Chloronaphthalene ND 1 0 033 2-Chlorol2henol ND 1 0 10 33 4-Chloro hen l Phen l Ether ND 1 0 033 Ch sene ND l 0 033 Dibenzo(a,h)anthracene ND 1 0 033 Dibenzofuran ND 10 1 033 Di-n-but 1 Phthalate ND 1 0 033 1,2-Dichlorobenzene ND 1 0 0 33 1,3-1)ichlorobenzene ND 1 0 033 1,4-Dichlorobenzene ND 1 0 033 3,3-Dichloroben7tdine ND 1 0 066 2 4-Dichloro henol ND 1 0 033 Dieth1 Phthalate ND 1 0 033 2,4-Dameth 1 henol ND 1 0 033 Dimethyl Phthalate ND 1 0 033 1 4 6-Dinitro-2-methyl henot ND 1 0 l 6 2,4-Dmitrohenol ND 1 0 1 6 2,4-Dinitrotoluene ND 1 0 033 2,6-Dinitrotoluene ND 10 033 Di-n-octyl Phthalate ND 1 0 033 1,2-Diphen lh drazine ND 1 0 033 Ftuoranthene ND 1 10 033 Fluorene ND 1 0 033 Hexachlorobenzene ND 1 0 033 Hexachlorobutadiene ND 1 0 033 Hexachlorocyclo entadiene ND 1 0 --16 Hexachloroethane ND l 0 033 Indeno(1,2,3-cd)pyrene - ND 1 0 033 -- Iso horone ND 1 0 033 2-Methylnaphthalene ND 1 0 0 33 2-Meth 1 henol(o-Cresol) ND 10 033 3&/or 4-Meth I henol(m, -Cresol) ND 1 0 033 Naphthalene ND 1 0 033 2-Nitroaniline ND 10 16 3-Nitroaniline ND 10 16 4-Nnroanilme ND 10 16 2-Nitro henol ND 1 0 1 6 4-Nitrophenol ND 1 0 033 N-Nitrosodi hen famine ND to 033 N-Nitrosodi-n- ropylamine ND 10 033 Pentachlorophenol ND 1 0 1 6 Phenanthrene ND 1 0 033 Phenol ND 10 033 Pyrene ND 1 0 033 1,2,4-Tnchlorobenzene ND 10 033 2,4,5-Tnchlorohenol ND 1 0 033 2 4 6-Trichlorohenol ND i 1 0 033 Surrogate Recoveries(%) %SS 1 95 5 %SS2 870 %SS3 884 %S S4 861 %SS5 796 %SS6 862 Comments *water samples and all TCLP&SPLP extracts are reported in pg/L,soil/sludge/solid samples in mg/kg,wipe samples in pg/wipe,product/oil/non- aqueous liquid samples in mg/L ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis • #)surrogate diluted out of range &)low or no surrogate due to matrix interference h)lighter than water immiscible sheen/product is present,i)liquid sample that contains greater than—2 vol %sediment,j)sample diluted due to high organic content,k)reporting limit raised,benzoic acid found in LCS/LCSD samples Benzoic acid found in the method blank at a detectable concentration but under the RL for this compound DHS Certification No 1644 r\JU-ht.F[��Angela Rydelius, Lab Manager