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110 2nd Avenue Soutli #D7,Pacheco CA 94553-5560 <br /> McCampbell Analytical, Inc. Telephone 925-798 1620 Fax 925-798 1622 <br /> Website www mccarnpbeileom E mail-main(arweampbell corn-""—" <br /> Advanced GeoEnvironmental, Inc Client Project ID Flag Clty Chevron Date Sampled 01/20/04-01/22/04 <br /> . 837 Shaw Road Date Received 01/23/04 <br /> Stockton, CA 95215 <br /> Client Contact 1 im CueIlar Date Extracted 01/23/04 <br /> - _ <br /> Client P O Date Analyzed 01124104-01/28/04 <br /> Serra-Volatile Organics by GUMS(Basic Target List)* <br /> Extraction Method SW3510C Analytical Method SW8270D <br /> Work Order 0401260 <br /> 040I260-OIOD <br /> P;:Ml <br /> - - - P43-13toIg <br /> Water <br /> Concentration DF Rcporung * Rep°rt°�g <br /> I...tet Compound Concentration DF Lmut <br /> Acenaphthene ND 1 0 10 Acenaphthylene ND l 0 10 <br /> Anthracene ND 10 10 Benzidine ND 10 50 <br /> Benzoic Acid ND 1 0 50 Benzo(a)anthracene ND 10 10 <br /> Benzo b fluoranthene ND 1 0 10 Benzo(k)fluoranthene ND 1 0 10 <br /> Benzo ,h,i a lene ND 1 0 10 Benzo(a)pyrene ND to 10 <br /> Bcnzyl Alcohol ND 1 0 20 Bis(2-chloroethox Methane ND 1 0 10 <br /> Bis(2�hloroeth 1)Ether ND 1 0 10 Bis(2-chlorotsopro yl)Ether ND 1 0 10 <br /> Bis(2-eth lhexyl)Phthalate ND 1 0 10 4-Bromo hen 1 Phenyl Ether ; ND 1 0 10 <br /> But lbenz ly Phthalate ND 1 0 10 4-Chloroanilme ND —1-07 20 <br /> 4-Chloro-3-meth 1phenol ND 1 0 10 2-Chloronaphthalene ND to 10 <br /> 2-Chlorophenol ND 1 0 10 4-Chloro hen 1 Phenyl Ether ND to 10 <br /> Chrysene ND 1 0 10 Dibenzo a,h anthracene ND lo 10 <br /> Dibenzoturan ND 1 D 10 Di-n-butyl Phthalate ND 1 0 10 <br /> 1,2-Dichlorobenzene ND 10 10 1 1,3-Dichlorobenzene ND 10 10 <br /> 1,4-Dichlorobenzene ND I 0 IO 3,3-Dichlorobenzidme ND ! 0 20 <br /> • 2,4-Dichloro henol ND i 1 0 10 Diethyl Phthalate ND __100_ 1 10 <br /> 2,4-Dimethylphenol ND 1 0 10 Dimethyl Phthalate ND 1 0 10 <br /> 4 6-Dmitro-2-meth 1 henoi ND 1 0 50 2,4-Dmttro henol ND ] 0 50 <br /> 2 4-Dinitrotoluene ND 1 0 10 2,6-Dimtrotoluene ND 11 0 10 <br /> Di-n-octyl Phthalate ND l 0 10 1,2-Dt hen lh drazme ND l 0 14 <br /> Fluoranthene ND 10 10 Fluurene ND 10 10 <br /> Hexachloroberizene ND 10 10 Hexachlorobutadiene ND 10 10 <br /> Hexachloroeyclo entadiene ND 1 0 50 Hexachloroethane ND 1 0 10 <br /> indeno 12,3-cd)pyrene ND 1 0 10 Isophorone NA 10 10 <br /> 2-Meth Naphthalene ND 10 10 2-Meth l henol(o-Cresol) ND l0- 10 - <br /> 3&lor 4-Meth 1 henol m, -Cresol) ND 1 0 10 Naphthalene ND 1 0 10 <br /> 2-Nitroaniline ND 10 50 3-Nitroanihne ND 10 50 <br /> 4-Nrtroamlme ND 10 50 Nitrobenzene ND 1 0 50 <br /> 2-Nitrophenol ND 10 50 4-Nitrophenol ND [0 10 <br /> N-Nitrosodi hen lamitte ND 1 0 10 N-Nitrosodi-n-propylamme ND 1 0 10 <br /> Pentachlorophenol ND 1 0 50 Phenanthrene ND to 10 <br /> Phenol ND 10 10 Pyrene � ND11 <br /> 10 <br /> 1,2,4-Trtchlorobenzene ND to 10 2,4,5-Tnehloro henol ND 1-0) <br /> 10 <br /> 2 4 6-Tnchloro henol NO 10 10 <br /> Surrogate Recoveries(%) <br /> %SSI 83 3 %SS2 <br /> 867 <br /> %SS3 <br /> %SS3 832 %SS4 817 <br /> 79 3 %SS6 720 <br /> Comments i <br /> "water samples and all TCLP&SPLP extracts are reported inµg/L,soil/sludge/solid samples in mg/kg wipe samples in Ag/wipe,product/oil/non- <br /> aqueous ltquid samples in mg/L <br /> ND means not detected above the reporting)emit,NIA means analyte not applicable to this analysis <br /> #)surrogate diluted out of range,&)low or no surrogate due to matrix interference <br /> • h)lighter than water immiscible sheen/product is present,t)liquid sample that contains greater than-2 vol %sediment,3)sample diluted due to high <br /> organic content,k)reporting limit raised,benzoic acid found in LCSILCSD samples Benzoic acid found in the method blank at a detectable <br /> concentration but under the RL for this compound <br /> DHS Certification No 1644 Angela Rydeltus, Lab Manager <br />