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110 2nd Avenue South #137 Pacheco,CA 94553-5560 <br /> McCampbell Analytical, Inc. Telephone 925-798-1620 Fax 925-798 1622 <br /> - - -Website www mcca:atpbcll coni Email main@mccampbell cam �= - - -- -- — <br /> Advanced GeciEnvironmental, Inc Client Project ID Flag City Chevron Date Sampled 01/20104-01/22/04 <br /> 837 Shaw Road Date Received 01/23/04 <br /> Stockton,CA 95215 Client Contact Tim Cuellar Date Extracted 01/23/04 <br /> _ <br /> Client P O Date Analyzed 01/24/04-01128104 <br /> Semi-Volatile Organics by GC/MS(Basic TargLt List)* <br /> Extmcuon Method. SW3510C Analyacal Method SW8270D Work Order 0401260 <br /> Lab ID 1 040126 0-011 D <br /> Client ID d P43-37to41 - - <br /> Matrix Water <br /> DF Pepog < i <br /> gCompound Concentration I.= Compound Concentration* DF Lima <br /> Acenaphthene ND 1 0 10 Acena hth leve ND 1 0 10 <br /> Anthracene ND 10 l0 Benzidine ND 10 50 <br /> Benzoic Acid ND 1 0 50 Benzo a anthracene ND 1 0 10 <br /> Benzo b fluoranthene ND 1 0 10 Benzo fluoranthene ND 1 0 10 <br /> Benzo(g,h,i)pe ]enc ND 1 0 10 Benzo(a)pyrene ND l 0 10 <br /> Benzy]Alcohol ND 1 0 20 Bis(2-chicroethoxy)Methane ND 1 D to <br /> Bis(2-Lhloroeth 1)Ether ND 1 0 10 Bos(2-chlorolsopropyl)Ether ND i lo 10 <br /> Bis 2-eth ]hex 1 Phthalate ND 10 10 4-Bromo hen I Phenyl Ether ND 1 0 10 <br /> Bu Ibenz ]Phthalate ND 1 0 10 4-Chloroamlme ND I lo 20 <br /> 4-Chloro-3-meth (phenol ND 1 0 10 2-Chlorona hthalene ND 1 0 10 <br /> 2-Chlorophenol ND 1 0 10 4-Chloro hen i Phenyl Ether ND lo 10 <br /> Chrysene ND 10 10 Dibenzo(a,h)anthracenc ND 10 10 <br /> Dlbenzofuran ND 1 0 10 Di-n-butyl Phthalate ND 10 10 <br /> 1,2-Dichlorobenzene ND 10 10 1,3-13tchlorobenzenc ND 10 10 <br /> 1,4-Dichi xobenzene ND 1 0 10 3,3-Dichlorobenzidine ND 1 0 20 <br /> . 2,4-Dwhloro henol ND 1 0 10 I Diethyl Phthalate ND 1 0 10 <br /> 2,4-Dimethylphenol <br /> ND 1 0 10 Dimethyl Phthalate ND 7 0 10 <br /> ND 1 0 50 2,4-Dinitro henoi ND t 0 50 <br /> Dmitrotoluene ND 1 0 10 2 6-Dmotrotoluene ND l U 10 <br /> Di-n oc I Phthalate ND l 0 10 1,2-Di hen ]h drazine ND 10 10 <br /> Fluoranthene ND 10 10 Fluorene ND 10 10 <br /> Hexachlorobenzene ND 1 0 10 Hexachlorobutadiene ND 1 0 10 <br /> Hexachloroc clo entadiene ND 1 0 50 Hexachloroethane ND 1 0 10 <br /> indeno 1,2,3-cd pyrene ND 1 0 10 Iso horone ND 1 0 l0 <br /> 2-Meth ]naphthalene ND 1 0 10 2-Meth l henoI(o-Cresol ND - 1 0 10 <br /> 3&!or 4-Methylphenol(m, -Cresol) ND 1 0 10 Naphthalene ND 1 0 10 <br /> 2-Nitroanillne ND l0 50 3-Nitroantline ND 10 50 <br /> 4-Nitroaniline ND 10 50 1 Nitrobenzene ND 10 50 <br /> 2-Nitro henoi ND 1 0 50 4-Nitrophenol ND i 10 ]0 <br /> N-Nltrosodr hen lamine ND 1 0 10 N-Nitrosodi-n-propylamine ND 1 0 10 <br /> Pentachlorophenol ND 1 050 Phenanthrene ND 10 10 <br /> Phenol ND 10 Ell <br /> 0 Pyrene ND 10 10 <br /> 1,2,4-Tnchlorobenzene ND 1 0 0 2,4,5-Tnehloro henoI ND 1 0 10 <br /> 2,4.6-Trichlorophenol ND 1 0 0 <br /> Surrogate Recoveries(%) <br /> %S31 92 0 %SS2 93 1 <br /> %SS3 897 %SS4 867 <br /> %SS5 796 %SS6 101 <br /> Comments i <br /> 'water samples and all TCLP&SPLP extracts are reported in Itg/L,soil/studge/sohd samples in mg/kg,wipe samples in}Ig/wipe,product/oil/non- <br /> aqueous liquid samples in mg/L <br /> ND means not detected above the reporting]emit,NIA means analyte not applicable to this analysis <br /> #)surrogate diluted out of range,&)low or no surrogate due to matrix interference <br /> h)lighter than water immiscible sheen/product is present,i)liquid sample that contains greater than--2 vol %sediment,j)sample diluted due to high <br /> organic content,k)reporting limit raised,benzoic acid found in LCS/LCSD samples Benzoic acid found in the method blank at a detectable <br /> concentration but under the RL for this compound <br /> DHS Certification No 1644 Angela Rydebus, Lab Manager <br />