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110 2nd Avenue South #D7 Pacheco CA 94553-5560 <br /> Inc.McCampbell Analytical, Telephone 925-798-1620 Fax 925-798-1622 i <br /> _Webgne wwwmccampbell com-E-mail main@mccampbell com= - - --=---- <br /> Advanced GeoEnvironmental, Inc Client Project ID FIag City Chevron Date Sampled 01/20/04-01/22/04 <br /> • 837 Shaw Road Date Received 01/23/04 <br /> Stockton,CA 95215 Client Contact Tim CueIIar Date Extracted 01/23/04 <br /> _ <br /> [Client P O Date Analyzed 01/24/04-01128/04 <br /> Sena-Volatile Organics by GUMS(Basic Target List)'* <br /> Extraction Method SW3550C Analytical Method SW8270D York Order 0401260 <br /> Lab ID 0401260-025A <br /> Client 117 --- -P43-30' _ - Y <br /> Matrix Soil <br /> Compound Concentration * DF Reio=�t„s Compound Concentration * DF R`P�,,"',g <br /> Acenaphthene ND 10 033 Acenaphthylene ND 1 0 033 <br /> Acetoehlor ND 1 0 033 Anthracene ND 10 033 <br /> Benzidine ND t 0 1 6 Benzoic Acid ND 1 0 1 6 <br /> Benzo a anthracene ND 1 0 03 Denzo(b)fluoranthene ND 1 0 033 <br /> Benzo(k)fluoranthene ND 1 0 03 Benzv ,h,t lene ND 1 0 -0-3-3 <br /> Benzo a ene ND 10 0 33 Benzyl Alcohol ND 11 0 066 <br /> Bis(2-chloraethoxy Methane ND 1 0 0 33 Bis 2-chloroethyl)Ether ND 1 0 6,113 <br /> Bis 2-chloro1sopro yl)Ether ND 1 0 033 Bis(2-eth lhex 1)Adipate ND 1 0 033 <br /> Bis 2-ethylhexyl)Phthalate ND i 1 0 033 4-13mmo henyl Phenyl Ether ND 1 0 033 <br /> But lbenz 1 Phthalate ND ] 0 0 33 4-Chloroanihne ND l 0 066 <br /> Nitrobenzene ND �1 ,0 �03 <br /> 4-Gliloro-3-meth 1 henoE ND 1 0 0 33 <br /> 2-Chlarona hthalene i ND 2-Chloro henol ND 1 0 033 <br /> 4-Chlvrophen I Phenyl Ether ND Ghryseno ND ] 0 033 <br /> Dibenzo(a,h)anthracene ND 1 0 033 Dibenzofuran ND 10 033 <br /> Di-n-but 1 Phthalate ND 1 0 033 1,2-Dichlorobenzene ND l 0 033 <br /> 1,3-Dichlorobenzene ND ! 0 0 33 1,4-Dichlorobenzene ND 1 0 033 <br /> 3,3-Dichlorobenzidine ND 1 0 0 66 2 4-Dichlorophen] ND 1 0 033 <br /> Diethyl Phthalate ND 1 0 0 332,4-Dimeth ]phenol ND 1 0 033 <br /> Dimethyl Phthalate ND til <br /> 0 33 �Di-n-octyl <br /> Dimtro-2-meth ] henol ND 1 0 16 <br /> 2,4-Dmitra henol ND 1 6 Dmitrotoluene ND 10 033 <br /> 2,6-Dinitrotoluene ND 0 33 Phthalate ND l 0 033 <br /> 1,2-Di hen ih drazme ND 1 0 033 Fluoranthene ND 1 0 033 <br /> Fluorene ND 1 00 33 H—x-. hlombenzene ND 10 033 <br /> Hexachlorobutadiene ND 1 0 033 Hexachlorocyclo entadtone ND 1 0 16 <br /> Hexachloroethane ND 1 0 033 Indeno 1,2,3-edpyrene ND 10 033 - <br /> Iso horone ND 1 0 033 2-Mcthylna hthalene ND l 0 033 <br /> 2-Methyl henol(o-Cresol) ND 1 0 033 3&/or 4-Meth [phenol m, -Cresol) ND l 0 033 <br /> Naphthalene ND 1 0 033 2-Nitroamline ND 10 1 6 <br /> 3-Nitroaniline ND W64-Nitroanilinc Nitroaniline ND ] 016 <br /> 2-Nitrohenol ND Nitro hent ND 10 033 <br /> N-Nitrosodi hen lamme ND Nitrosodi-n- ro ylamme ND t0 033 <br /> Pentachloro henol ND enanthrene ND l 0 033 <br /> Phenol ND rene ND 1 0 033 <br /> 1,2,4-Trichlorohenzene ND ,5-Trichlorophenol ND 1 0 033 <br /> 2 4 6-Tnchloro henol ND 10 033 <br /> Surrogate Recoveries <br /> %SSI 107 °/x552 927 <br /> %SS3 928 %SS4 983 <br /> %SS5 81 1 %SS6 <br /> 106 _ <br /> Comments <br /> *water samples and all TCLP&SPLP extracts are reported in kg(L soil/sludge/solid samples in mg/kg,wipe samples in gg/wipe,product/oil/non- <br /> aqueous liquid samples in mg/L <br /> ND means not detected above the reporting limit,NIA means analyte not applicable to this analysis <br /> #)surrogate diluted out of range,&)low or no surrogate due to matrix interference <br /> h)lighter than water immiscible sheen/product is present,i)liquid sample that contains greater than--2 vol %sediment j)sample diluted due to high <br /> organic content,k)reporting limit raised,benzoic acid found in LCS/LCSD samples Benzoic acid found in the method blank at a detectable <br /> concentration but under the RL for this compound <br /> DHS Certification No 1644 Angela Rydelius,Lab Manager <br />