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110 2nd Avenue South,#177,Pacheco,CA 94553-5560 <br /> McCampbell Analytical, Inc. Telephone 925-798-1620 rax 925-798 1622 <br /> Web�Lte_www mccampbell coin ]-mail mainQmccampbe11 coin -- - - _-- <br /> Advanced GeoEnvironmental, Inc Client Project ID Flag City Chevron Date Sampled 01/20/04-01/22/04 <br /> . 837 Shaw Road Date Received 01/23/04 <br /> Stockton,CA 95215 Client Contact Tim Cuellar Date Extracted 01/23/04 <br /> r <br /> rc—Itent P O Date Analyzed 01/24/04-01/28/04 <br /> Semi-Volatile Organics by GC/MS(Basic I'arget List)* <br /> Extraction Method SW3550C Analytical Method SW8270D Work Order 0401260 <br /> Lab ID 7777 0401260-026A <br /> - - _ - Client ID - P43-45' <br /> Matrix Soil <br /> xc <br /> Compound Concentration * DF L-1 Compound Concentration s e�orr�,g <br /> i.orti DF <br /> Acenaphthene ND 10 033 Acenaphthylene ND 10 0 33 <br /> Acetochlor ND 10 I 033 Anthracene ND ! 0 033 <br /> Benzidine ND 1 0 1 6 Benzoic Acid ND 1 0 l 6 <br /> Benzo(a anthracene ND 1 0 033 Benzo b fluoranthene ND 1 0 0 33 <br /> Benzo(k)fluoranthene ND 1 0 033 Benzo( ,h,i}pe ]ene ND 1 0 033 <br /> Benzo(a)pyrene ND 1 0 033 Benzyl Alcohol ND ] 0 066 <br /> Bas(2-chloroethox Methane ND l 0 033 Bis 2-chloroeth i)Ether ND ! 1 0 033 <br /> Bis(2-chlorolsopropyl)Ether ND 1 0 033 Bis(2�th lhex I)Adipate - ND 1 0 0 33 <br /> Bis 2-ethylhex 1 Phthalate ND 1 0 033 4-Bromo henyl Phenyl Ether ND 1 0 033 <br /> Bu lbenz 1 Phthalate ND 1 0 033 4-Chloroanihne ND 1 0 066 <br /> Nitrobenzene ND 1 0 1 64-Chloro-3-meth l heno] ND 10 033 <br /> 2 Ch]ornna ltthalene ND 1 0 0 33 2-Chlorophenol ND 1 0 033 <br /> 4-Chlorohen 1 Phenyl Ether ND 1 0 0 33 Chrvsene ND t 0 033 <br /> Dibenzo(a,h)anthracene ND 1 0 033 Dibenzofuran ND 1 0 033 <br /> Di-n-but l Phthalate ND 1 0 033 1,2-Dichlorobenzene ND 1 0 033 <br /> 1,3-Dichlorobenzene ND 1 0 033 1,4-Dichlorobenzene ND 10 033 <br /> 3,3-Dichlorobenzidme ND 1 0 066 2,4-Dichlorohenol ND 1 0 033 <br /> Diethyl Phthalate ND 1 0 033 2,4-Dmethil heno[ ND l 0 033 <br /> Dimethyl Phthalate ND 1 0 033 4,6-Dinitro-2-meth i henoi ND 1 0 l 6 <br /> 2,4-Dinitro henoi ND 1 0 16 2,4-Dimtrotoluene ND 1 0 033 <br /> 2,6-Dinitrotoluene ND 1 0 033 Di-n-octyl Phthalate ND 1 0 033 <br /> 1,2-Di henyihydrazine ND 1 0 033 Fluoranthene ND 1 0 033 <br /> Fluorene ND 1 0 033 Hexacblorobenzene ND l 0 033 <br /> Hexachlorobutadiene ND 1 0 033 Hexachlorocycloperitadiene ND 1 0 l 6 <br /> Hexachloroethane ND 1 0 033 lndeno(1,2,3-cdpyrene - ND _10 033 �- <br /> lso horone ND 1 0 033 2-Meth Ina hthalene ND 1 0 033 <br /> 2-Methyl henol(o-Cresol) ND 1 0 033 3 Wor 4-Meth i heno! m, -Cresol) ND 1 0 033 <br /> Naphthalene ND l 0 033 2-Nitroanihne NQ L 0 1 6 <br /> 3-Nitroaniline ND 10 16 4-Nttroandine ND 10 16 <br /> 2-Nitrophenol ND l 0 1 6 4-Nitro heno] ND 1 0 033 <br /> N-Nitrosodi henylamine ND 1 0 033 N-Nitrosodi-n- roylamine ND 1 0 033 <br /> Pentachlorophenol ND 1 0 16 Phenanthrene ND 10033 <br /> Phenol ND ] 0 033 Pyrene ND 1 0 0 33 <br /> 1,2,4-Trichlorobenzene ND 1 0 033 2 4,5-Trichlorophenol ND 10 0 33 <br /> 2 4 6-Trichlorohenol ND to 0 33 <br /> Surrogate Recoveries(%) <br /> %SSI 93 2 %SS2 <br /> 863 <br /> %SS3 <br /> 932 %SS4 837 <br /> %SS5 806 %SS6 909 <br /> Comments <br /> •water samples and all TCLP&SPLP extracts are reported inµg/L,soil/sludge/solid samples in mg/kg,wipe samples in 4g/wipe,product/oillnon- <br /> aqueous liquid samples in mg/L <br /> ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis <br /> #)surrogate diluted out of range,&)low or no surrogate due to matrix interference <br /> h)lighter than water immiscible sheen/product is present,i)liquid sample that contains greater than-2 vol %sediment,l)sample diluted due to high <br /> organic content,k)reporting limit raised,benzoic acid found in L.CS/LCSD samples Benzoic acid found in the method blank at a detectable <br /> concentration but under the RL for this compound <br /> DHS Certification No 1644 Angela Rydelius, Lab Manager <br />